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BROOKFIELD DV-II+ PROGRAMMABLE VISCOMETER Operating ...

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A.4 VERIFYING CALIBRATION1. Determine the appropriate sample volume.Refer to Table A6 to determine the correctsample volume required for the spindle tobe utilized.2. Select a Brookfield Viscosity Standard fluidthat will give viscosity readings between10% and 100% of full scale range. Refer toAppendix B for viscosity ranges of conespindles; ranges listed apply to CPE cones.ConePart No.CPE-40CPE-41CPE-42CPE-51CPE-52Table A1Sample Volume0.5 ml2.0 ml1.0 ml0.5 ml0.5 mlDo not use a silicone viscosity standard fluidwith a viscosity value greater than 5000 cPwith a Cone/Plate. Brookfield offers acomplete range of mineral oil viscositystandards suitable for use with Cone/Platesfor viscosities above 5,000 cP or shear ratesabove 500 sec -1 ; see Table E2 inAppendix E for a list of available fluids.It is best to use a viscosity standard fluidthat will be close to the maximum viscosityfor a given cone spindle/speed combination.Example:LV<strong>DV</strong>-<strong>II+</strong> Viscometer, ConeSpindle CPE-42, BrookfieldSilicone Viscosity Standardhaving a viscosity of 9.7 cP at25°CAt 60 RPM, the full scale viscosity range is10.0 cP. Thus, the Viscometer readingshould be 97% torque and 9.7 cP viscosity ±0.197 cP. The allowable error (±0.197 cP)is a combination of Viscometer accuracyand fluid tolerance (refer to Interpretationof Calibration Test Results inAppendix E).4. Attach the sample cup to the Viscometerand allow sufficient time for thesample, cup and cone to reach temperatureequilibrium.5. Turn the motor on. Set the desiredspeed(s). Measure the viscosity andrecord the reading in both % torqueand centipoise (cP).Note: The cone spindle must rotateat least five (5) times before a viscosityreading is taken.6. Verify that the viscosity reading iswithin the allowable 1% deviation, asexplained earlier, for the specificviscosity standard fluid(s) that you areusing.* The CPE designation on the conespindle indicates use with ElectronicGap Setting Cone/Plate Viscometers/Rheometers only.3. With the motor off, remove the sample cupand place the viscosity standard fluid intothe cup.Brookfield Engineering Labs., Inc. Page 45 Manual No. M/97-164-F1 102

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