Shodex Catalogue 2013-2015.pdf - Analytics Shop

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Standard AnalysisColumnsColumns for Ligand Exchange ChromatographyAnomer separation of saccharidesAnomer separation of saccharides affects thechromatogram.When using a SUGAR column to analyze saccharides, theanalysis at high temperatures would suppress the influence ofanomer separation, resulting in proper chromatograms.29˚C70˚CGlucose Mannose Xylose Galactose Arabinose0 10 20 min 0 10 20 min 0 10 20 min 0 10 20 min 0 10 20 minGlucose Mannose Xylose Galactose Arabinose0 10 20 min 0 10 20 min 0 10 20 min 0 10 20 min 0 10 20 minColumn : Shodex SUGAR SC1011Eluent : H 2 OFlow rate : 0.7mL/minDetector : RIColumn temp. : 29˚C, 70˚CHydrolyzed starchDp-10Dp-5Dp-1Sample : 20μLHydrolyzed starch 1%Sample :0.5% each, 10μL1Calibration curves for KS-800 series using pullulan2Molecular Weight (Pullulan)Saccharides in wood (model)Sample : 5μL1. Cellobiose 1.0%2. Glucose 1.5%3. Xylose 0.5%4. Galactose 0.5%5. Arabinose 0.5%6. Mannose 1.0%10 710 610 510 410 310 246 810 12Elution volume (mL)KS-801KS-802KS-803KS-804KS-805KS-806Column : Shodex SUGAR KS-800 seriesEluent : H 2 ODetector : RIColumn temp. : 80˚CKetohexosesSample : 0.025% each, 10μL1. Sorbose2. Fructose3. Tagatose4. Psicose1263 4 5341015 20 min5 10 1520min0 5 10 1520minColumn : Shodex SUGAR KS-802 x 2Eluent : H 2 OFlow rate : 1.0mL/minDetector : RIColumn temp. : 80˚CColumn : Shodex SUGAR SP0810Eluent : H 2 OFlow rate : 0.6mL/minDetector : RIColumn temp. : 85˚CColumn : Shodex SUGAR SP0810Eluent : H 2 OFlow rate : 1.0mL/minDetector : RIColumn temp. : 80˚COligosaccharides in soybeanSaccharides related to raffinosebiosynthesisAcesulfame K and sucraloseSample : 0.1% each, 20μL1. Verbascose2. Stachyose3. Raffinose4. Sucrose5. Pinitol5Sample : 20μL, 0.1% each1. Raffinose2. Sucrose3. Galactinol4. Galactose5. myo-Inositol1235Sample : 20μL1. Acesulfame K 0.1%2. Sucrose 0.5%3. Glucose 0.5%4. Unknown from Acesulfame K5. Fructose 0.5%6. Sucralose 0.1%2423435114610 15 20 25 30min0 5 10 min0 5 10 1520min18Column : Shodex SUGAR KS-802 + KS-801Eluent : H 2 OFlow rate : 0.6mL/minDetector : RIColumn temp. : 85˚CColumn : Shodex SUGAR SC1011Eluent : H 2 OFlow rate : 1.0mL/minDetector : RIColumn temp. : 80˚CColumn : Shodex SUGAR SC1011Eluent : 10mM CaSO 4 aq.Flow rate : 0.6mL/minDetector : RIColumn temp. : 80˚C
Sucrose and turanose12Sample : 0.5% each, 10μL1. Fructose2. Glucose3. Sucrose4. Turanose5. LactoseMaltose and isomaltose1Sample : 0.5% each, 20μL1. Glucose2. Maltose3. Isomaltose4. Maltotriose5. Isomaltotriose4Saccharides and sugar alcoholsSample : 0.5% each, 20μL1. Rhamnose2. Xylose3. Arabinose4. Fructose5. Glucose6. Galactose7. Arabitol8. Xylitol9. Mannitol10. SorbitolStandard AnalysisColumns3450 5 10 15 20 25 30 350 5 10 15 20 minminColumn : Shodex SUGAR SZ5532Eluent : H 2 O/CH 3 CN=20/80Flow rate : 0.6mL/minDetector : RIColumn temp. : 60˚CSaccharides in presence of sodium salt23Column : Shodex SUGAR SZ5532Eluent : H 2 O/CH 3 CN=25/75Flow rate : 1.0mL/minDetector : RIColumn temp. : 60˚CSince DC-613 uses Na + as counter ion, it enables the analysis of saccharides insodium salt containing samples without desalting. Acid hydrolyzed sample canbe analyzed after neutralizing the remaining acid, such as hydrochloric or sulfuricacid, with sodium hydroxide.Solvent for samplepreparationSample : 0.1% each, 10μL1. Xylose2. Sucrose3. Cellobiose4. Lactose5Pinitol1 234 567 8 90 5 10 15 minColumn : Shodex SUGAR SZ5532Eluent : H 2 O/CH 3 CN=20/80Flow rate : 1.0mL/minDetector : RIColumn temp. : 65˚C10Sample : 0.1% each, 10μL1. Pinitol2. Fructose3. Glucose4. Sucrose5. chiro-Inositol6. myo-InositolColumns for Ligand Exchange Chromatography1% NaCl aq./CH 3 CN=50/50123411% Na 2 SO 4 aq./CH 3 CN=50/502345 6H 2 O/CH 3 CN=50/500 5 10 15min0510 1520minColumn : Shodex RSpak DC-613Eluent : H 2 O/CH 3 CN=30/70Flow rate : 0.8mL/minDetector : RIColumn temp. : 50˚C* High concentration of acetonitrile isused for saccharide analysis by DC-613.Pay attention to possible salt depositionwhen analyzing with high saltconcentration samples.Column : Shodex RSpak DC-613Eluent : H 2 O/CH 3 CN=25/75Flow rate : 1.0mL/minDetector : RIColumn temp. : 70˚CMoisturizing componentsMannitol analysis with USP methodSample : 0.1% each, 20μL1. 1,3-Propanediol2. Propylene glycol3. Ethylene glycol4. Glycerin5. meso-Erythritol1According to the USP (United States Pharmacopeia) method, mannitolshould be analyzed using a column which can separate mannitol andsorbitol with a resolution equal to or greater than 2.0.MN-431 is a column specially designed for mannitol analysis, whichsatisfies this criteria.14Sample : 0.5% each, 10μL1. Mannitol2. Sorbitol22350 5 10 15minColumn : Shodex SUGAR SC1211Eluent : H 2 O/CH 3 CN=60/40Flow rate : 0.6mL/minDetector : RIColumn temp. : 40˚C0 2Column : Shodex USPpak MN-431Eluent : H 2 OFlow rate : 0.5mL/minDetector : RIColumn temp. : 60˚C4 6 8min19
Page 2: TMWe provide a wide range of produc
Page 7 and 8: BiotechnologyGenomicsProteomicsGlyc
Page 9 and 10: Comparison between ODP2 HP and ODP-
Page 11 and 12: AlkylalcoholsC8C6C4EGC6C10C12C14C8C
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Page 15 and 16: Fructooligosaccharide syrup2Sample
Page 17 and 18: Hippuric acids in urineStandards2Sa
Page 22 and 23: Standard AnalysisColumnsColumns for
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Page 30 and 31: Standard AnalysisColumnsAqueous SEC
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Page 34 and 35: Standard AnalysisColumnsMultimode C
Page 36 and 37: Standard AnalysisColumnsAqueous/Org
Page 38 and 39: Standard AnalysisColumnsOrganic SEC
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Page 64 and 65: Sample PretreatmentColumnsColumns f
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Application FieldsBiotechnology Ana
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Application FieldsWater quality[Ani
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Semi-micro andMicro ColumnsSemi-mic
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PreparativeColumnsPreparativeColumn
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InformationPhase-out ProductsPhase-
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InformationColumn Cleaning Procedur
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InformationColumn Trouble ShootingC
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IndexIndex by Product NameColumns a
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Technical InformationTechnical Note
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Please contact a Shodex support off
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