Shodex Catalogue 2013-2015.pdf - Analytics Shop

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Sample PretreatmentColumnsPretreatment Columns for Column SwitchingMethodPKFeaturesEffective for both hydrophilic and hydrophobic substancesThe high protein removal rate enables efficient pretreatmentNewsNo.9, 11, 22Pretreatment Columns for Column Switching MethodGF-4AHigher protein removal rate than PK columns* GF-4A column removes proteins well but is not suitable for trapping hydrophilic substances.Use PK columns for this purpose.NewsNo.9, 11, 22Cartridge columns and holder for column switching methodProduct CodeF8700000F8700012F8700001Product NameMSpak PK-2A 2pMSpak PK-4A 2pMSpak HLDColumn for column switching methodParticle Size(µm)3030−Pore Size(Å)3030−Column Size(mm)I.D. x Length2.0 x 104.0 x 10(Holder for PK)Shipping SolventH 2 OH 2 O−Pcs/boxBase Material : Hydrophilic copolymers containing N-vinyl acetoamide* PK series are cartridge columns and thus should be installed in a column holder "MSpak HLD" before use.221Product CodeProduct NameParticle Size(µm)Pore Size(Å)Column Size(mm)I.D. x LengthShipping SolventF8700015 MSpak GF-4A 9 400 4.6 × 10H 2 OBase Material : Polyvinyl alcohol64*Contact <strong>Shodex</strong> or our distributors near you for customized columns.
System diagram for column switchingPretreatment columnAnalytical columnInjectorDetectorPump 1Protein removal rate using pretreatment columnsColumnPK-2AGF-2A*Company-AProtein removalrate99.62%99.80%97.68%Residual BSA (μg)500400300200100Sample PretreatmentColumnsEluent 1Proteins etc.in sampleRecovery rate of medical compounds using PK-2ASampleAcetaminophenAcetylpheneturideAconitineAlprazolamAmitriptylineAmobarbitalBarbitalBenzoylaconitineBenzoylhypaconineBiperidenBromazepamBromocriptineBromperidolBromvalerylureaBrotizolamCaffeineCarbamazepineCarpipramineChlordiazepoxideChlormezanoneChlorpheniramineChlorpromazineClocapramineClofedanolClomipramineClonazepamPump 2Recovery(%)1159211099939394968399102808994971069799133921117795919596Eluent 2SampleCloxazolamDesipramineDiazepamDiphenhydramineEstazolamEthenzamideEtizolamFludiazepamFlumazenilFlunitrazepamFlurazepamGlutethimideHaloperidolHaloxazolam1-Hydroxymethyltriazolam4-HydroxytriazolamHydroxyzineHypaconitineImipramineIndomethacinLevomepromazineLofepramineMaprotylineMedazepamMephobarbitalMesaconine0PK-2A(Pretreatment)Eluent : 10mM Ammonium acetate buffer(pH7.0)Flow rate : 0.5mL/minColumn temp. : Room temp.GF-2A Company-A(Analysis)Column : <strong>Shodex</strong> PROTEIN KW-604S**Eluent : 0.1% TFA in (H 2 O/CH 3 CN=50/50)Flow rate : 0.5mL/minDetector : UV(280nm)*GF-2A: Custom-made column ofColumn temp. : Room temp.GF-4A (2.0mm I.D. x 10mm)Switching time : 5min**KW-604S is phase-out product.Recovery(%)911099793101981059793971069399939091999797939665909199118SampleMianserinNimetazepamNitrazepamNortriptylineOxazepamOxazolamPentobarbitalPerfenazinePhenacetinPhenobarbitalPhenytoinPrimidonePromethazinePropericiazinePropranololSecobarbitalSildenafil citrateThioridazineTimiperoneTriazolamTrihexyphenidylTrimethadioneTrimipramineWarfarinZotepineRecovery(%)92909786979993861089699919290979795978896911371078192Pretreatment Columns for Column Switching MethodClotiazepam96Metharbital94(Adsorption)Eluent : 10mM Ammonium acetate buffer (pH7.0)Flow rate : 0.5mL/min(Elution)Eluent : 10mM Ammonium acetate buffer (pH7.0)/CH 3 CNFlow rate : 0.5mL/minDetector : UV(220nm)Switching time : 5min65
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TMWe provide a wide range of produc
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BiotechnologyGenomicsProteomicsGlyc
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Comparison between ODP2 HP and ODP-
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AlkylalcoholsC8C6C4EGC6C10C12C14C8C
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Separation and recovery rate of sta
Page 15 and 16: Fructooligosaccharide syrup2Sample
Page 17 and 18: Hippuric acids in urineStandards2Sa
Page 20 and 21: Standard AnalysisColumnsColumns for
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Page 30 and 31: Standard AnalysisColumnsAqueous SEC
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Page 34 and 35: Standard AnalysisColumnsMultimode C
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Page 38 and 39: Standard AnalysisColumnsOrganic SEC
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Page 68 and 69: Application FieldsPharmaceuticals a
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Page 74 and 75: Semi-micro andMicro ColumnsSemi-mic
Page 80 and 81: PreparativeColumnsPreparativeColumn
Page 86 and 87: InformationPhase-out ProductsPhase-
Page 88 and 89: InformationColumn Cleaning Procedur
Page 90 and 91: InformationColumn Trouble ShootingC
Page 92 and 93: IndexIndex by Product NameColumns a
Page 94 and 95: Technical InformationTechnical Note
Page 96: Please contact a Shodex support off
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