Standard AnalysisColumnsOrganic SEC (GPC) Columns (General Analysis) :ChloroformK-800FeaturesStandard organic solvent SEC (GPC) columnSupports a wide range of applications from low to high molecular weight compoundsPreparativeColumnsp.83Standard columnsOrganic SEC (GPC) Columns (General Analysis) : ChloroformK-800 series : Shipping solvent ChloroformProduct CodeF6028110F6028120F6028125F6028130F6028194F6028140F6028195F6028150F6028196F6028160F6028190F6028197F6028170F6028198F6700401F6709450Product NameGPC K-801GPC K-802GPC K-802.5GPC K-803GPC K-803LGPC K-804GPC K-804LGPC K-805GPC K-805LGPC K-806GPC K-806MGPC K-806LGPC K-807GPC K-807LGPC K-GGPC K-800DPlate Number(TP/column)≥ 18,000≥ 18,000≥ 18,000≥ 18,000≥ 18,000≥ 18,000≥ 18,000≥ 11,000≥ 11,000≥ 11,000≥ 13,000≥ 11,000≥ 6,000≥ 6,000(guard column)solvent-peakseparation columnExclusion Limit(Polystyrene)1,5005,00020,00070,00070,000400,000400,0004,000,0004,000,000(20,000,000)*(20,000,000)*(20,000,000)*(200,000,000)*(200,000,000)*−* See page 40 for details of the solvent-peak separation columns. The columns with ‘L’ or ‘M’ atthe end of column names are mixed-gel column capable of analyzing samples over a wide rangeof molecular weight distribution.−Particle Size(µm)666667710101010101818810MaximumPore Size(Å)501503005005001,5001,5005,0005,00010,00010,00010,00020,00020,000−−Column Size(mm)I.D. x Length8.0 × 3008.0 × 3008.0 × 3008.0 × 3008.0 × 3008.0 × 3008.0 × 3008.0 × 3008.0 × 3008.0 × 3008.0 × 3008.0 × 3008.0 × 3008.0 × 3004.6 × 108.0 × 100Base Material : Styrene divinylbenzene copolymer( )* Estimated value* See page 50 for applicability of SEC (GPC) columns to solvent replacement.Molecular weight range with polystyrene (eluent : chloroform)Molecular weight (Polystyrene)10 10 210 3 10 4 10 5 10 6 10 7 10 8 10 9K-801K-802K-802.5K-803K-804K-805K-806K-807K-803LK-804LK-805LK-806MK-806LK-807L38CalibrationStandardsSee page 51 forCalibration Standards*Contact <strong>Shodex</strong> or our distributors near you for customized columns.
Epoxy resinSample : Epikote ® 1001 0.1%, 100μLLow molecular polydimethylsiloxanesSample : 0.1% each, 100μL1. Polydimethylsiloxane (MW:770)2. Polydimethylsiloxane (MW:237)3. Hexamethyldisiloxane (MW:162)23Standard AnalysisColumns10 15 20 minColumn : <strong>Shodex</strong> GPC K-803L x 2Eluent : ChloroformFlow rate : 1.0mL/minDetector : UV(254nm)Column temp. : Room temp.Silicon oilSample : Silicone oil 0.1%, 200μLSilicone oil0 510Column : <strong>Shodex</strong> GPC K-801 x 2Eluent : ChloroformFlow rate : 1.0mL/minDetector : RI(Polarity : negative)Column temp. : 40˚CBionolle TM(Polybutylene succinate/adipate)115 20 25minSample : Polybutylene succinate/adipate 0.2%, 100μLOrganic SEC (GPC) Columns (General Analysis) : Chloroform10 152025 min15 20 25 30 minColumn : <strong>Shodex</strong> GPC K-806M x 2Eluent : TolueneFlow rate : 1.0mL/minDetector : RIColumn temp. : 45˚CColumn : <strong>Shodex</strong> GPC K-806M x 2 + K-801Eluent : ChloroformFlow rate : 1.0mL/minDetector : RIColumn temp. : 40˚CRecycling fractionation of lauryl stearyl thiodipropionateSample : 5%, 500μL1. Distearyl thiodipropionate2. Lauryl stearyl thiodipropionate3. Dilauryl thiodipropionateCYCLE1CYCLE2 CYCLE6 CYCLE10123Column : <strong>Shodex</strong> GPC K-LG + K-2001Eluent : ChloroformFlow rate : 3.0mL/minDetector : RI(preparative type)Column temp. : 50˚C0 10 20 min* See page 83 for K-200139