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Shodex Catalogue 2013-2015.pdf - Analytics Shop

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Epoxy resinSample : Epikote ® 1001 0.1%, 100μLLow molecular polydimethylsiloxanesSample : 0.1% each, 100μL1. Polydimethylsiloxane (MW:770)2. Polydimethylsiloxane (MW:237)3. Hexamethyldisiloxane (MW:162)23Standard AnalysisColumns10 15 20 minColumn : <strong>Shodex</strong> GPC K-803L x 2Eluent : ChloroformFlow rate : 1.0mL/minDetector : UV(254nm)Column temp. : Room temp.Silicon oilSample : Silicone oil 0.1%, 200μLSilicone oil0 510Column : <strong>Shodex</strong> GPC K-801 x 2Eluent : ChloroformFlow rate : 1.0mL/minDetector : RI(Polarity : negative)Column temp. : 40˚CBionolle TM(Polybutylene succinate/adipate)115 20 25minSample : Polybutylene succinate/adipate 0.2%, 100μLOrganic SEC (GPC) Columns (General Analysis) : Chloroform10 152025 min15 20 25 30 minColumn : <strong>Shodex</strong> GPC K-806M x 2Eluent : TolueneFlow rate : 1.0mL/minDetector : RIColumn temp. : 45˚CColumn : <strong>Shodex</strong> GPC K-806M x 2 + K-801Eluent : ChloroformFlow rate : 1.0mL/minDetector : RIColumn temp. : 40˚CRecycling fractionation of lauryl stearyl thiodipropionateSample : 5%, 500μL1. Distearyl thiodipropionate2. Lauryl stearyl thiodipropionate3. Dilauryl thiodipropionateCYCLE1CYCLE2 CYCLE6 CYCLE10123Column : <strong>Shodex</strong> GPC K-LG + K-2001Eluent : ChloroformFlow rate : 3.0mL/minDetector : RI(preparative type)Column temp. : 50˚C0 10 20 min* See page 83 for K-200139

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