Shodex Catalogue 2013-2015.pdf - Analytics Shop
Shodex Catalogue 2013-2015.pdf - Analytics Shop
Shodex Catalogue 2013-2015.pdf - Analytics Shop
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Calibration curves for KF-800 seriesusing polystyreneMolecular weight (Polystyrene)10 810 710 610 510 410 310 2105 6 7 8 9 10 11 12 13Elution volume (mL)KF-802KF-801KF-806KF-804KF-803KF-802.5KF-807KF-8051 2KF-806MColumn : <strong>Shodex</strong> GPC KF-800 seriesEluent : THFFlow rate : 1.0mL/minDetector : RIColumn temp. : Room temp.Standard polystyrenes3457Calibration curves for KF-800L (linear type)series using polystyreneMolecular weight (Polystyrene)10 810 710 610 510 410 310 2105 6 7 8 9 10 11 12 13Elution volume (mL)KF-807LKF-806LKF-805LKF-804LKF-803LColumn : <strong>Shodex</strong> GPC KF-800L seriesEluent : THFFlow rate : 1.0mL/minDetector : RIColumn temp. : Room temp.Sample : 50μL1. Polystyrene (Mw : 133,000) 0.1%2. Polystyrene (Mw : 55,100) 0.1%3. Polystyrene (Mw : 19,600) 0.1%4. Polystyrene (Mw : 7,210) 0.1%5. Polystyrene (Mw : 3,070) 0.1%6. Polystyrene (Mw : 580) 0.1%7. Toluene (Mw: 92) 0.15%2345Fat-soluble vitamins56123Sample : 100μL1. Vitamin A palmitate500μg/mL2. Vitamin E 50μg/mL3. Vitamin D3 50μg/mL4. Vitamin K3 50μg/mL410 15 20 25minColumn : <strong>Shodex</strong> GPC KF-801 x 2Eluent : THFFlow rate : 1.0mL/minDetector : UV(280nm)Column temp. : 40˚CSample : 50μL1. Polystyrene (Mw : 19,825,000) 0.05%2. Polystyrene (Mw : 1,320,000) 0.1%3. Polystyrene (Mw : 133,000) 0.1%4. Polystyrene (Mw : 7,210) 0.1%5. Polystyrene (Mw : 580) 0.1%6. Toluene (Mw : 92) 0.1%Standard AnalysisColumnsOrganic SEC (GPC) Columns (General Analysis) : THF610 5 10 15 20 25 30 min 0 5 10 15 20 25 30 minColumn : <strong>Shodex</strong> GPC KF-803L x 2Eluent : THFFlow rate : 1.0mL/minDetector : UV(254nm)Column temp. : 40˚CColumn : <strong>Shodex</strong> GPC KF-807L x 2Eluent : THFFlow rate : 1.0mL/minDetector : UV(254nm)Column temp. : 40˚CStyrene isoprene ABA block copolymerPolycarbonate resinRaw rubberSample : Styrene isoprene ABA block copolymerSample : Polycarbonate resin 0.1%, 100μLSample : Rubber 0.1%, 300μLCH3O C O CCH3 O n15 20 25 min15 20 25min0 10 20 30 minColumn : <strong>Shodex</strong> GPC KF-806M x 2Eluent : THFFlow rate : 1.0mL/minDetector : RIColumn temp. : 30˚CColumn : <strong>Shodex</strong> GPC KF-806L x 2Eluent : THFFlow rate : 1.0mL/minDetector : RIColumn temp. : 40˚CColumn : <strong>Shodex</strong> GPC KF-806M x 2+ KF-802Eluent : TolueneFlow rate : 1.0mL/minDetector : RIColumn temp. : Room temp.37
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