Shodex Catalogue 2013-2015.pdf - Analytics Shop

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Standard AnalysisColumnsColumns for LC/MS AnalysisColumns for Polymer-based Reversed Phase ChromatographyProductCodeProduct NamePlate Number(TP/column)FunctionalGroupBase MaterialParticleSize(µm)PoreSize(Å)Column Size(mm)I.D. x LengthShipping SolventF7622004ODP2 HP-2B≥ 3,000−Polyhydroxymethacrylate5402.0 × 50H 2O/CH 3CN=55/45F7622005ODP2 HP-2D≥ 7,000−Polyhydroxymethacrylate5402.0 × 150H 2 O/CH 3 CN=55/45Columns for Polymer-based Hydrophilic Interaction Chromatography (HILIC) Aqueous/Organic SEC Columns Organic SEC (GPC) Columns[Columns for LC/MS Analysis] Columns for Polymer-based Reversed Phase ChromatographyF6714011F7620009F6713001F7001007F6700151F7008160F7008220ODP2 HPG-2AAsahipak ODP-50 2DAsahipak ODP-50G 2ARSpak DE-213RSpak DE-SGRSpak NN-414RSpak JJ-50 2D(guard column)≥ 5,000(guard column)≥ 8,000(guard column)≥ 6,000≥ 3,500−OctadecylOctadecyl−−SulfoAqueous/Organic SEC ColumnsPolyhydroxymethacrylatePolyvinyl alcoholPolyvinyl alcoholPolymethacrylatePolymethacrylatePolyhydroxymethacrylatePolyvinyl alcohol55546105−250−25−2001002.0 × 102.0 × 1502.0 × 102.0 × 1502.0 × 104.6 × 1502.0 × 150H 2 O/CH 3 CN=55/45H 2 O/CH 3 CN=35/65H 2 O/CH 3 CN=35/65H 2 O/CH 3 CN=50/50H 2 O/CH 3 CN=50/500.1M Sodium phosphatebuffer(pH3.0)H 2 O/CH 3 CN=40/60Columns for Polymer-based Hydrophilic Interaction Chromatography(HILIC)ProductCodeF7630008F7630009F7630010F7630006F6713000Asahipak NH2P-40 2BAsahipak NH2P-40 2DAsahipak NH2P-40 2EAsahipak NH2P-50 2DAsahipak NH2P-50G 2AQuaternaryammonium* Asahipak NH2P-40 2B, Asahipak NH2P-40 2D, and Asahipak NH2P-40 2E are the new names for the NH2P40-2B, NH2P40-2D, and NH2P40-2E, respectively.ProductCodeF7600100F7600110F7600024F7600120Organic SEC (GPC) ColumnsProductCodeF6028111Product NameProduct NameMSpak GF-310 4BMSpak GF-310 4DMSpak GF-310 4EMSpak GF-310 2DProduct NameGPC KF-401HQPlate Number(TP/column)≥ 2,000≥ 5,500≥ 7,000≥ 3,500(guard column)Plate Number(TP/column)≥ 3,000≥ 10,000≥ 16,000≥ 5,500PlateNumber(TP/column)≥ 25,000FunctionalGroupAminoAminoAminoAminoAminoExclusion Limit(Pullulan)1,50040,00040,00040,00040,000ExclusionLimit(Polystyrene)Base MaterialPolyvinyl alcoholPolyvinyl alcoholPolyvinyl alcoholPolyvinyl alcoholPolyvinyl alcoholBase MaterialPolyvinyl alcoholPolyvinyl alcoholPolyvinyl alcoholPolyvinyl alcoholBase MaterialParticleSize(µm)Styrene divinylbenzene copolymer44455ParticleSize(µm)5555PoreSize(Å)3100100100100−ParticleSize(µm)Column Size(mm)I.D. x Length2.0 × 502.0 × 1502.0 × 2502.0 × 1502.0 × 10MaximumPore Size(Å)400400400400MaximumPore Size(Å)50Shipping SolventCH 3 CNCH 3 CNCH 3 CNH 2 O/CH 3 CN=25/75H 2 O/CH 3 CN=25/75Column Size(mm)I.D. x Length4.6 × 504.6 × 1504.6 × 2502.0 × 150Column Size(mm)I.D. x Length4.6 × 250ShippingSolventH 2 OH 2 OH 2 OH 2 OShippingSolventTHFF6028112GPC KF-402HQ≥ 25,0005,000Styrene divinylbenzene copolymer31504.6 × 250THFF6028114GPC KF-402.5HQ≥ 25,00020,000Styrene divinylbenzene copolymer33004.6 × 250THF58F6700300GPC KF-G(guard column)−Styrene divinylbenzene copolymer8−4.6 × 10THF*Contact Shodex or our distributors near you for customized columns.
Barbital recovery rate comparison of ODP2 HP-2B and ODS in the presence of BSAODP2 HPBarbital 500ng/mLBarbitalPeak Area : 100%ODSBarbital 500ng/mLBarbitalPeak Area : 100%For the LC/MS analysis of drug samplescontaining protein as a matrix, using ODScolumns generally exhibit ion suppressionof the target drugs. Since proteins are notretained by ODP2 HP column, they eluteseparate (as a void) from the targetcomponents. Thus, using ODP2 HP columnexhibits less ion suppression influence.Standard AnalysisColumns0.0 1.0 2.0 3.0 4.0 min 0.00 2 4 6 8 100 1into MS2Barbital 500ng/mL in BSA 7.0mg/mL1BarbitalPeak Area : 99%LC/MS analysis of drugs in control serumSample : 5μLDrugs 500ng/mL each in Control serumUV(280m)12 minLC/MS analysis of basic drugs0Lidocaine2 4 6 8 10 12 14 min3 4 5 6 7 8 9 min21.0 2.0 3.0 4.0 minm/z 235Chlorpheniraminem/z 275VerapamilPropranololm/z 260Diphenhydraminem/z 256BupivacaineImipramineColumn : Shodex ODP2 HP-2BEluent : 10mM Ammonium acetate aq./CH 3 CN=70/30Flow rate : 0.2mL/minDetector : UV(280nm), ESI-MS(SIM Positive)Column temp. : 40˚Cm/z 304 m/z 290m/z 289m/z 455m/z 281ODP-50 2D, a polymer-based reversed phase column, is capable of analyzingbasic drugs at low concentration or without salt. This is preferred for ESI-MSanalysis, since the presence of salt causes ion suppression, and thus influencesthe analysis performance.Column : Shodex Asahipak ODP-50 2DEluent : H 2 O/CH 3 CN=40/60Flow rate : 0.2mL/minDetector : ESI-MS(SIM Positive)Column temp. : 30˚CSample : 10ng/mL each, 5μL1. Scopolamine2. AtropineBarbital 500ng/mL in BSA 7.0mg/mLBarbitalPeak Area : 71%LC/MS analysis of statinsPravastatin0 1 2 3 4 5 6 7 8 9Glyoxylic acidPyruvic acidGlycolic acidLactic acidPitavastatinFluvastatinAtorvastatinMevastatin10 11 12 13 14 15 16 17 18 19 20 21 minMaleic acidLovastatinSuccinic acidFumaric acidSimvastatinLC/MS analysis of organic acidsColumn : Shodex ODP2 HP-2BODS from other manufacturerEluent : 10mM Ammonium acetate aq./CH 3 CN=70/30Flow rate : 0.2mL/minDetector : ESI-MS(SIM Negative : m/z 183)Column temp. : 30˚CInjection vol. : 10μLAdipic acid0 1 2 3 4 5 6 7 8 9 minSample : 100ng/mL each, 5μLm/z 423m/z 422m/z 412m/z 559m/z 391m/z 405m/z 419Column : Shodex ODP2 HP-2BEluent : (A); 10mM Ammonium formate aq. (B); CH 3 CNLinear gradient;B%; 10%(0min) 10%(3min) 35%(13min) 35%(20min)Flow rate : 0.2mL/minDetector : ESI-MS(SIM)Column temp. : 40˚CSample : 50ng/mL each, 10μLm/z 73m/z 87m/z 75m/z 89m/z 115m/z 117m/z 115m/z 145Column : Shodex RSpak DE-213Eluent : (A); 0.1%(v/v) Formic acid aq. (B); CH 3 CNLinear gradient;B%; 5%(0min) 5%(2min) 15%(2.5min) 15%(10min)Flow rate : 0.2mL/minDetector : ESI-MS(SIM Negative)Column temp. : 30˚CColumns for Polymer-based Hydrophilic Interaction Chromatography (HILIC) Aqueous/Organic SEC Columns Organic SEC (GPC) Columns[Columns for LC/MS Analysis] Columns for Polymer-based Reversed Phase Chromatography59
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TMWe provide a wide range of produc
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BiotechnologyGenomicsProteomicsGlyc
Page 9 and 10: Comparison between ODP2 HP and ODP-
Page 11 and 12: AlkylalcoholsC8C6C4EGC6C10C12C14C8C
Page 13 and 14: Separation and recovery rate of sta
Page 15 and 16: Fructooligosaccharide syrup2Sample
Page 17 and 18: Hippuric acids in urineStandards2Sa
Page 20 and 21: Standard AnalysisColumnsColumns for
Page 28 and 29: Standard AnalysisColumnsColumn Sele
Page 30 and 31: Standard AnalysisColumnsAqueous SEC
Page 32 and 33: Standard AnalysisColumnsAqueous SEC
Page 34 and 35: Standard AnalysisColumnsMultimode C
Page 36 and 37: Standard AnalysisColumnsAqueous/Org
Page 38 and 39: Standard AnalysisColumnsOrganic SEC
Page 52 and 53: Standard AnalysisColumnsApplicabili
Page 62 and 63: Standard AnalysisColumnsLC/MS analy
Page 64 and 65: Sample PretreatmentColumnsColumns f
Page 66 and 67: Sample PretreatmentColumnsPretreatm
Page 68 and 69: Application FieldsPharmaceuticals a
Page 70 and 71: Application FieldsBiotechnology Ana
Page 72 and 73: Application FieldsWater quality[Ani
Page 74 and 75: Semi-micro andMicro ColumnsSemi-mic
Page 80 and 81: PreparativeColumnsPreparativeColumn
Page 86 and 87: InformationPhase-out ProductsPhase-
Page 88 and 89: InformationColumn Cleaning Procedur
Page 90 and 91: InformationColumn Trouble ShootingC
Page 92 and 93: IndexIndex by Product NameColumns a
Page 94 and 95: Technical InformationTechnical Note
Page 96: Please contact a Shodex support off
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