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100638<br />

E-BILLING TO SIMPLIFY AND SPEED THE MANUAL<br />

INVOICE HANDLING PROCESS,<br />

IN PERFECT COMPLIANCE WITH THE EC LAW<br />

FASTER, LEGALLY CONFORM<br />

AND PAPERLESS!<br />

Reducing the time spent on invoice<br />

handling, avoiding errors and integrating<br />

the electronic processes: that is what the<br />

introduction of electronic billing sets out to<br />

achieve. And it will save around 600 000 sheets<br />

of paper into the bargain. This project<br />

coincides with the entry into force of the<br />

European directive on electronic billing and<br />

the transposal of this regulation into national<br />

law. Based on an estimated 200 000 annual<br />

invoices, the project claims to generate a<br />

cost-saving of EUR 300 000. Taking into<br />

account both the cost of the programmes<br />

and the setting up of the new system, the<br />

investment pays for itself in only three<br />

months! The electronic invoice, a “pdf”<br />

document is completed by the certified<br />

electronic signature, according to the legal<br />

requirements. Both are sent to the client by<br />

e-mail. The software of Authentidate AG,<br />

was selected in September 2005 and the<br />

server and the software were set up during<br />

the first quarter of 2006. The project is being<br />

tested in Spain with the Solvay Chemicals<br />

and SolVin clients. It will then be rolled out<br />

in all for all the European customers and for<br />

the 3S entity for the ‘self-billing’ to suppliers.<br />

Solvay is thus joining the select circle of the<br />

five chemical companies in the world to offer<br />

such a service to its clients.<br />

> Haimo Zekoll; Bernadette Hislaire; Chantal Liesse;<br />

Christophe Pariset; Montserrat Paulos;<br />

Richard Verlaque.<br />

> CHEMICALS SECTOR<br />

105231<br />

MAJOR BREAKTHROUGH IN THE EXTRACTION<br />

AND OPTIMIZATION OF FLUORSPAR<br />

RECOVERY AT THE SOLVAY OKORUSU<br />

FLUORSPAR MINE - NAMIBIA<br />

A MINE OF GOOD<br />

IDEAS AT OKORUSU<br />

Since the acquisition of the Okorusu<br />

mine (Namibia) by Solvay in 1997,<br />

constant efforts have been made to improve<br />

the production of fluorspar concentrates<br />

(CaF2). The ore contains between 30 and<br />

40% of CaF2. The mine, which carries out the<br />

flotation of the ore on site to extract sterile<br />

gangue, supplies its concentrates to the<br />

Solvay plants of Bad Wimpfen (Germany)<br />

and Porto Marghera (Italy). Production<br />

increased gradually from 23 000 tonnes<br />

in 1997 to 80 000 tonnes in 2003. The main<br />

difficulties lied in producing a 97%<br />

concentrate of CaF2 while maintaining the<br />

presence of the other elements in line<br />

with the required specifications. A first<br />

breakthrough was achieved through the use<br />

of a new reagent, which saw production<br />

spiral to 104 000 tonnes in 2004. However,<br />

the process developed called for specific ores<br />

with a very low carbonate content and<br />

consequently, thousands of tonnes of ore<br />

with an excessive carbonate content were<br />

building up as they were unsuitable<br />

for production. On the initiative of Dr<br />

Gerstenberg, the research concentrated on<br />

treating the concentrates with an acid. Under<br />

the supervision of Roy Verburgt, the team<br />

made further progress by using NH4FHF<br />

(ammonia bifluoride), which made it possible<br />

to improve the safety and management of<br />

the leaching process. The technology was<br />

immediately rolled out at industrial level<br />

in August of 2005. These improvements<br />

restored the profitability of the mine, which<br />

had been endangered by the appreciation<br />

of the local currency. The possibility of<br />

exploiting a poorer ore and obtaining a<br />

richer concentrate considerably increased the<br />

mine’s lifetime. It has set itself a production<br />

goal of 127 000 tonnes in 2007.<br />

> Rolf Gerstenberg; Mark Dawe; Willem Nependa;<br />

Roy Verburgt.<br />

> SBU FLUOR<br />

Performance improvement<br />

101361<br />

A REVOLUTION IN HEAT TRANSFER AT HIGH<br />

PRESSURE: THIN WALL REACTOR<br />

ONE INNOVATION<br />

AFTER THE OTHER<br />

In chemical processes that require the use<br />

of pressurized, heated or refrigerated reactors,<br />

the heat is transferred via a double jacket<br />

through the wall of the reactor. Generally,<br />

the thickness of the reactor is increased<br />

in line with the pressure and the diameter,<br />

which, at the same time, reduces the transfer<br />

of heat. Several technological attempts have<br />

therefore been made to reduce the thickness<br />

of the wall, in particular through a special,<br />

complicated and thus costly design.<br />

The SolVin teams thought along other lines<br />

to break the dependency between the<br />

internal pressure and the thickness of the<br />

wall involved in the heat transfer. They<br />

worked on the idea of a very thin laser<br />

welded internal wall, formed through<br />

hydrodeformation at high pressure. To<br />

achieve this result, it was necessary to tackle<br />

the process itself, by balancing the pressures<br />

of the reactor and of the cooling water. The<br />

thickness of the internal wall could thus be<br />

drastically reduced (from 27 to 1.5 mm) and<br />

the heat transfer was doubled. A first<br />

application of the process has proven<br />

successful in Jemeppe (Belgium) on a reactor<br />

of 100 litres. Various modelling<br />

and engineering studies have demonstrated<br />

the industrial feasibility of the process.<br />

The development prospects are quite broad,<br />

as the process can be applied to all high<br />

pressure heat transfer procedures.<br />

> Jean-Paul Bindelle; Jean-Marie Blairon;<br />

Daniel Borremans; Olivier Brulard;Thierry Cartage;<br />

Manuel de Francisco; Stéphane Ghislain;<br />

Maryse Granville; Philippe Guiche; Claude Laugel;<br />

Dominique Martinez.<br />

> SBU VINYLS<br />

J U L Y 2 0 0 6<br />

49

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