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DESENVOLVIMENTO E CARACTERIZAÇÃO FÍSICO ... - UFSM

DESENVOLVIMENTO E CARACTERIZAÇÃO FÍSICO ... - UFSM

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49<br />

43 1651 - γ-butyrolactone 0.061 ± 0.013 - - -<br />

44 1654 - 1-nonanol 0.002 ± 0.001 - - -<br />

-<br />

45 1658 - Isovaleric acid 0.012 ± 0.003 - -<br />

Peak<br />

IK-Wax a<br />

IK-<br />

RTX5-<br />

ms b<br />

(conclusão)<br />

Compounds mg.Lc IK-GC-O d Odor descritor e Frequency f<br />

46 1707 1188 Diethyl Succinate 0.004 ± 0.001 - - -<br />

47 1723 - alpha-Terpineol 0.002 ± 0.001 1722 Flower 1<br />

48 1728 - γ-caprolactone 0.008 ± 0.003 - - -<br />

49 1756 - Prenyl isobutyrate 0.008 ± 0.001 - - -<br />

50 1763 - Citronellol 0.002 ± 0.001 - Citronella 1<br />

51 1802 - 3-Methyl-2-butenoic acid 0.004 ± 0.003 - - -<br />

52 1813 - 3-Methyl-3-butenoic acid 0.001 ± 0.001 - - -<br />

53 1819 - Ethyl 4-hydroxybutyrate 0.008 ± 0.002 - - -<br />

54 1825 1258 2-Phenylethyl acetate 0.008 ± 0.011 - - -<br />

55 1841 1111 Hexanoic acid* 10.7± 0.039 1821<br />

rancidity, sheepskin,<br />

sour<br />

8<br />

56 1870 1324 Ethyl hydrocinnamate 0.012 ± 0.021 1871 Burnt sugar, coffee 3<br />

57 1900 1120 Phenylethyl alcohol 0.086 ± 0.039 1940 Rose, strawberry gum 5<br />

58 1918 1123 2-Ethyl-hexanoic acid 0.009 ± 0.001 - - -<br />

59 1972 1193 Octanoic acid 0.113 ± 0.060 1996 Sweet 1<br />

60 >2000 1443 Ethyl cinnamate 0.009 ± 0.001 >2000 Floral, sweet 3<br />

a<br />

Experimental linear retention index on capillary column DB-Wax<br />

b<br />

Experimental linear retention index on capillary column RTX5-ms.<br />

c<br />

Mean ± standard deviation of three repetitions of each two production batches.<br />

d<br />

Experimental linear retention index on capillary column DB-Wax by GC-O<br />

e<br />

Aroma descriptor of the consensual aromagram<br />

f<br />

Detection frequency of the judges in GC-O analysis of jelly palm wine<br />

* Volatile compounds quantified by GC-HS

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