paraffin wax deposition and fouling

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Oil Gas J., 58 (38), 87—91 (Sept. 1960). 32. Perry, J.H., “Chemical Engineers Handbook”, Cole, R.J., Jezzcn, F.W., ‘Paraffin Deposition”, (1971), (In Russian). 33. Armenski, E.A., Novoselov, V.F, Tugunov, P.1., McGraw Hill, 4th ed, (‘950). 17—24 (March 9970). Wax — Solvent Systems”, Soc. Pet. Engrs. J., - 0 - “Paraffin Deposition in Short Pirelines”, Izv. Vysak. Ucheb Zaved., Heft Gas, 9- (7) 71—3w 6. Kolesnik, .0., Lukashevick, 1.?., Susanina, 0.0., 8. Zisrnan, W.A., “Influence of Constitution on Adhesion”, 57. Parks, G.E., “Chemical Inhibitors Combat Paraffin Deposi;ion 31. Patton, C.C., Caaad, B..., “Paraffin Deposition from Refined 39. Nelson, W.L., Stewart, 1.2., “Effect of Oil on Plastic ?rcser;ies 40. Shepard, J.C., “Theory and Mechanism of :iaffin Deposition”, 41. Muravev, i.X., Osk, l.A., Mishchenho, .T., 43. McAdar.:s, W.H., “Heat Transmission”, McGraw Hill, 3rd ed., (195--). 42. Nelson, W.L., “Petroleum Refining En;ineerin;”, McGraw Hill, 44. :cezso, W.L., ‘TouTh; of Ee.t :changers”, Refiner and Natural 4. Deissler, 2.0. “Thrbulent }eat Z’ansar and frioticn in Lin, Oxford University -ress, (9959). and 13 (6), 292—298, (Aust 193). 4th ed., (9958). (1949). nd. En;. Chern., 55, 99 (1953). Oil Gas J., 58, 97 (April 4th 1960). 85—8, (1971), (In Russian). — Isv. Vyssh. Uche. Zaved, Heft Gaz, 14 (2), 12 (2), 35—9, (1969), (In Russian). Deposition” Izv. Vyssh. Jcheb. Zaved., Heft Gaz, 35. Pustogov, V.1., Federov, EE., “Role of Temperature in ;ax “Effect of Temperature on Paraffin Deposition”, of Petroleum Waxes”, md. En;. Chem., 41, 2239, Short Course, University of Oklahoma, (1958). Presence of Sumerfactants”, Heft Khoz., -8 (12), ‘-8—5, (n Russian). Digest, Proc. of first Annual Paraffin Conhro Gasoiene aziufacturer, 93 (7), 279—275, (July 995--) Valume 7, Section , Convective ieat Transfer and Passages”, HiCk Seed .erodynamics and Jet Proralsion, “Crystallization of Paraffin in Solution in the friction in flow of licuids, 238—33?, falter D.C. t,
— 81 — 46. Coulson, J., Richardson, J.P., “Chcnical Engineering”, Vol. One, Pergarnon Press, Revised Second Edition, (1970) - 47. Cooper, A., “Recover More Heat with Plate Heat Exchangers”, Chern Engr., No. 285, 280—285, (May 1974). 48 Standards of the Th’oular Exchanger Manufacturers Association, 5th edition, New York, (1968). 49. Galloway, T.R., “Heat Transfer ?ouling Through Growth of Calcareous Ruin Deposits”, mt. J. Heat Mass Transfer, 16, 43—460, (1973).
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1 ci 0 Ilc (i) s_ri P4 4) •,-1 0
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ACKC’bJLED3E.:ENTS should like to
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46 iixperimental Results 461 IntroJ
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APPNNDICES 1. PHYSICal PRSPHTIES Oi
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the major unresolved problem in hea
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and time, fouling factors are usual
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o F-I 0 U J ,ij cn J ‘I—I F3 Fl
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—5— vary from less than 1 per c
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2.2.3 Solubility refined paraffin w
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-.9— whica is well novc condition
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— -ii — deposit. Tronov statej
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— 13 remain in solution and the p
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- iuctoov and dorov concluded hat t
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— 17 — a deporsiion ce:Ll in a
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— 19 - toat sur:ace. hjsima.a ot
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— 2 - S * .. -, ‘.: ,- - .-,-
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and surface proueriez reapectlvely_
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- 25 - loading to a random process
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y - F’J CD:’ C) x— Dcpoit thi
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0 C 15O— 200 From ref 2 of wax eo
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0 o3 Tb 3D 0•0 L D 2 •O— Fg.2
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2 I In 0 Tot -D -D U 16H 16 20, In
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C CE) CL) CE) () .: rJ\: - . c: CD
Page 47 and 48:
400 function of roughness factor. m
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— 2o — 3. i3:\CGRDU ND TO TI PR
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3.5 Conclusions decreases At the in
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L - A sz: CF Fo:;:NG BY SOLUTIONS O
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was designed to cut off the steam s
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• saLLy measures were tacen. oa:D
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— 34 .4 ‘mrii:ntal Solution The
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sections were ke-:t the same. fosi:
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sectaon 4- at eajt tests sections h
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These fluctuations were not reduced
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ii ID XXX 9 C-) 0 (N x S x xx< 7r-
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12— -; 11L. s 10E - 9: ‘3) 0 Ru
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(1) U) C’) C) Cl) It) 0 0 0 0 ox
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f-iq. 1.0-3.5.— Hecit trcinsfcr r
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I--i Fig. f.6.3.7. I ;ut transfer r
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0 C’) R — [feat transfer resist
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characteristc does exist and is tyt
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The ziuewor in the circulation syst
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The calibrations o the tesperature
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the solution and water o::a;es thro
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‘-- 5,5 wocrinentsl Resuts with f
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two hours, the deposits were observ
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wcr: on ara:zic: c.eposc.tion consi
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-- II 1 L1 SOLUIIOIJ C;IFCU1_/:[ION
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SCAR FE 1 DEPOSITION PLATE - - 0 C)
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M—AMOUNI DEPOSITED (mg) T1 0_i c)
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C) 0 0 0 Li.] CD - 3 0 3 0 h Iii (E
Page 101 and 102:
- II -fl M—AMOUNT DEPOSITED (rng)
Page 103 and 104: 91 9) :< C) --z 9] mc-) .;J -i ru
Page 105 and 106: .1 1• ci E 0 Ci) c) — nj
Page 107 and 108: - . O, O, I— —,-, fouling studi
Page 109 and 110: profiles at different Reynolds numb
Page 111 and 112: L Run . (°c) used to calculate tem
Page 113 and 114: Due to a concentration gradient the
Page 115 and 116: 1 I C. (1.2.2.2 \1L. I .OC[FY V [A[
Page 117 and 118: V 40 - 0 C—, lt! -— o. ---—-
Page 119 and 120: Li FIG. G.2.3./. TEMPERAI URE v RAD
Page 121 and 122: — 1 7.0 0 --Tc.=10.0°C 50 140
Page 123 and 124: — -- — -——— — -—Tb =
Page 125 and 126: Z_o_—o-- 50 l0 - yX—--X— —-
Page 127 and 128: I:302 00 50 Ito -0——— ---—-
Page 129 and 130: I 50 ;) 30c’/ / C —------------
Page 131 and 132: FIG. 6. 4.1. AN IDEEAL TEMPERATURE
Page 133 and 134: — 63 — 7. DISCUSSIOI 7.1 Introd
Page 135 and 136: — 65 — through it decreases gra
Page 137 and 138: For breakdown and removal to occur
Page 139 and 140: — 69 — the large fouling studie
Page 141 and 142: Increased flowrate and temperature
Page 143: — 72 — 8. ICOi’NDATTCNS It is
Page 146 and 147: EEfiDN2WON
Page 148 and 149: T TemDerature T = Average temperatu
Page 150 and 151: = :ieat eddy dfusivity = Xoent eddy
Page 152 and 153: in Exchar.ge: Tubes”, Chem. Engr.
Page 156 and 157: U U F--I C) (f
Page 158 and 159: The o1ubi1ity of 5i/54°Cparafin wa
Page 160 and 161: — — .‘.ti+ c:Lic gravity The
Page 162 and 163: In section Al .4 the auount of pcra
Page 164 and 165: 0 •) X S (N U ‘0 -° CD c-) ( -
Page 166 and 167: I-] H — C C) p 0’ H 0’ H CD C
Page 168 and 169: fully refined paraffin wax in keros
Page 170 and 171: — A12 — The cloud point decrens
Page 172 and 173: — A3 — Tnble A2.1 Ca1culccd c i
Page 174 and 175: calibration constants are given in
Page 176 and 177: — Al? — Table A3.3.1 Calibratio
Page 178 and 179: — A19 — APPENDIX 4 THE PRDGR’
Page 180 and 181: C NC = C C REiCS EACH SET OF RE[iJC
Page 182 and 183: 13.42 7.40 7.SC 33.90 33.10 13.8 0.
Page 184 and 185: TIME TI TO TKI TKC DPK EPW DPT V CF
Page 186 and 187: 81.15 7.45 7.7C 33.40 32.70 30.0 0.
Page 188 and 189: RUN A1C—4 TIME 1WI TWO TKI TKC DP
Page 190 and 191: RUN 82—6 TIME TiI TC TKI TKC OPK
Page 192 and 193: TIME TWI TWO TKI TKC OPK CPW OPT V
Page 194 and 195: RUN B7—1C TIME TWI TWC TKI TKO DP
Page 196 and 197: RUN B9—12 T V’E ThI TWC TKI TKC
Page 198 and 199: RUN C1—1t T1’E IWI TWO TKI TKC
Page 200 and 201: PUN C2—15 TIME T’iI T0 TK1 TKC
Page 202 and 203: }U•” C-16 TIME TWI TWO TKI TKC
Page 204 and 205:
TIME flit TC TKI TKO DPK DPW OPT V
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UN C5-18 TIME TWI TfD TKI TKO DPK C
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14.25 7.IC 10.2C 39.10 38.00 8.8 0.
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RUNJ C8-2C T[’E TWE T0 TKI (Hg) (
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TIVE M)*2 C) TWI TWO TKI TKC DPK op
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Tt’iE TWI TC TKI TKO OPK CPW DPT
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— A23 — APPENDIX 5 OALT2RATTUNS
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T—- TEI\iFERATUFE (°C) —I’ U
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d Average C Table A5.2 0.0452 0.025
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11.1 6.517 10.5 6.418 10.1 6.346 9.
Page 224 and 225:
— A27 — Tib1e A6.2 Pun Dl .irn
Page 226 and 227:
-A29- Table A6.4 Pun 1)3 ‘ Time (
Page 228 and 229:
Time — A51 — Table A6.5 Run D5
Page 230 and 231:
— A33 — APPENDIX 7 EOUNDARY LAY
Page 232 and 233:
— ;55 — 1.7.3 Dimensionless Exp
Page 234 and 235:
— = u — u = in — + ± + + or
Page 236 and 237:
I A8.21 Data 2 Subroutines usng ite
Page 238 and 239:
— ALf1 — Equations L.7.4.3 and
Page 240 and 241:
— A1i•3 — Lt Prorran Use The
Page 242 and 243:
DIM /\3.2./>. THE iJNI/E?j\I. \ELC)
Page 244 and 245:
C DF1ENSIOH VIS(2.) REAL NUWSI INTE
Page 246 and 247:
C C SUt3ROUTINE DATA INTEGER SR C C
Page 248 and 249:
LI) I Li . 0 0 X .. (1•) U.. UI
Page 250 and 251:
C C WRt 1E(6,’O) 60 FQR’AT(1HLf
Page 252 and 253:
te 4Z’Xt’9’911’XZ’ 3DNVIS
Page 254 and 255:
C C C C C )fl:O .0 DO ‘O 1=3,9,2
Page 256 and 257:
C, .4:’. 0 0 —; —s iZ fl r;
Page 258 and 259:
KINEMATIC VISCOSITY AT WALL 0.07407
Page 260 and 261:
YP UP TP Y U T VIS TC CR PR 39.00 1
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