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NAMS 2002 Workshop - ICOM 2008

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Ultra- and Microfiltration III - Membranes – 5<br />

Friday July 18, 4:30 PM-5:00 PM, Honolulu/Kahuku<br />

Acoustic Investigation of Porous and Membrane Structures<br />

S. Léoni, Ecole Centrale Marseille, Marseille, France<br />

J. Bonnet, Université Paul Cézanne Aix Marseille, Provence, France<br />

Y. Wyart (Speaker), Université Paul Cézanne Aix Marseille, Provence, France -<br />

yvan.wyart@univ-cezanne.fr<br />

J. Allouche, Ecole Centrale Marseille, Marseille, France<br />

P. Moulin, Université Paul Cézanne Aix Marseille, Provence, France<br />

The processes of membrane filtration are in the heart of actual and future<br />

environmental challenges. Nevertheless, in order to increase the impact of<br />

membrane separation techniques in industrial field, the phenomenon of<br />

membrane fouling must be more understood. The membrane fouling can be<br />

monitored by measuring the increase of transmembrane pressure when the<br />

filtration is made at a constant flow rate. This procedure is a good indicator to<br />

estimate the frequency of backwashes or chemical cleanings; but gives no<br />

information about the kinetic of the fouling phenomenon, the fouling location (on<br />

membrane surface or in the membrane bulk), the structure of the cake&<br />

Moreover, it is well known that the membrane fouling depends on the structural<br />

characteristics of the membrane. The aim of the study is to develop an acoustic<br />

method to characterize first new membranes and secondly fouled membranes.<br />

This method must be non- invasive to avoid the destructuration of the cake and<br />

simple for an easy use.<br />

The present work deals with acoustic characterisation of porous media and<br />

membrane using impedance tube. This kind of materials is widely used<br />

throughout industry to measure the sound absorption coefficient and other<br />

acoustic properties of materials. Low frequency acoustic method is used to<br />

determine porosity from acoustic sample properties. The experimental setup is<br />

composed of a sound source, two microphones and a sample holder. The sound<br />

source (speaker), placed at an extremity of a rigid walled tube, generates<br />

incident plane waves which are partially reflected by the material sample, located<br />

at the other extremity of the tube (sample holder). The incident and reflected<br />

waves interfere and create a system of standing waves. For sufficiently low<br />

frequencies, it is a plane wave which is propagated along the tube axis. The<br />

lower limit frequency is dependent on the microphones limitation and on the<br />

spacing between microphones. The higher limit is given by the cut off frequency<br />

of the tube. Placed at the end of the tube, two microphones measure the acoustic<br />

pressure in order to calculate the frequency response function (FRF). This FRF is<br />

used to determine the complex acoustic surface impedance Z of the sample. The<br />

method presented in this paper is based on the theories of Lafarge- Allard which<br />

are based on a low frequency approximation. Using this assumption, porosity Phi

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