SAF-RC-047 100 & 300 Area Component of the ... - Hanford Site

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A.ionv", a a,auuracury, iuc. Pesticide/PCBs by GC, CLP List Report Date: 07/07/06 15:01 RFW Batch Number: 0604L904 Client: THURANFORD RC-047 X0303 work Order: 11343606001 Page: 2 Cust ID: J11KM4 J11KN5 J11KM6 JllKV1 JllKV2 J11L21 Sample RFW#: 007 008 009 010 011 012 Information Matrix: SOLID SOLID SOLID SOLID SOLID SOLID D.F.: 4.00 4.00 4.00 4.00 4.00 4.00 Units: UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG Surrogate: Tetrachloro-m-xylene 122 * t 104 t 173 * t 177 * t 200 * t 124 * k Decachlorobiphenyl 101 t 92 t 143 * t 140 * t 155 * t 96 t ---__...... °__ ......... _________ .......... ___f1 ...... _===== f1=====__=====fl=====_...... fl ...........= f1=====__=====f1 Alpha-BHC 20 U 15 U 14 U 18 U 14 U 19 U gamma-BHC (Lindane) 20 U 15 U 7.3 J 18 U 15 J 19 U Beta-BHC 46 19 .1 44 51 38 .I 16 J.I Heptachlor 20 U 15 U 14 U 18 U 14 U 19 U Delta-BHC 12 J 15 U 14 U 40 14 U 19 U Aldrin 12 J 15 J 14 U 14 28 19 U Heptachlor epoxide 20 U 15 U 14 U 18 U 14 U 19 U gamma-Chlordane 20 U 15 U . 14 D 18 U 14 U 19 U Endosulfan I 20 U 15 U 14 U 18 U 9.8 J 19 U. alpha-Chlordane 20 U 15 U 14 U 18 U 14 U 19 II, 4,4'-DDE 20 U 15 U 14 U 12 J 14 U 19 U. Dieldrin, 20 U i5 II 14 II 18 U 14 U 19 U: Endrin 20 U 15 U 14 U 18 U 14 U 19 U 4,4'-DDD 20 U 15 II .". 14 II _18 U I 19 U. Endosulfan II 20 U 15 U 14 U 18 U 14 U 19 U 4,4'=DDT 20 U 10 J 14 U 18 U 19 19 U Endrin aldehyde 20 U 15 U 14 U 18 U 14 J.I 19 U Endosulfan sulfate 20 U 15 U 14 U 18 U 14 U 19 U Methoxychlor 20 U 15 U 14 U 32 14 U 19 U Endrin ketone 20 U 15 U 14 U 18 U 14 U 19 U Toxaphene 200 U 150 U 140 U 180 U 140 U 190 U U- Analyzed, not detected. J. Present below detection limit. B= Present in blank. NR= Not reported. NS= Not spiked. V- Percent recovery. D- Diluted out. I. interference. NA. Not Applicable. *= Outside of EPA CLP QC 4 m M M m
uiuura W ua Wv 06Vcy, auc. Pesticide/PCBs by GC, CLP List Report Date: 07/07/06 15:01 RFW Batch Number • 0604L904 Client-, TNUHANFORD RC-047 K0303 Work Order- 11343606001 Page-, 3 Sample Information Cust ID: RFW#: Matrix: D.F.: JIIL23 013 SOLID 4.00 JIIL25 014 SOLID 4.00 J11L36 015 SOLID 4.00 J11L36 015 MS SOLID 4.00 J11L36 015 MSD SOLID 4.00 PBLKJM 06LE0455 -MIDI SOIL 1.00 m mm m Units: UG/KG UG/KG UG/KG UG/KG UG/KG UG/KG Surrogate: Tetrachloro-m-xylene 81 % 133 * $ 116 % 117 $ 149 * $ 113 $ Decachlorobiphenyl 67 $ 109 $ 87 $ 90 $ 135 * $ 97 $ ............................................. fl== ---------- fl ..... __=.... fl ... ==__=====fl== = ......... fl ............ fl Alpha-BHC 16 U 16 U 17 U 76 t 91 $ 0.33 U gamma-BHC (Lindane) 7.9 J.I 16 U 17 U 91 $ 112 $ 0.33 U Beta-BHC 46 .I 14 J 17 U 91 % 119 $ 0.33 U Heptachlor 16 U 16 U 17 U 99 $ 116 $ 0.33 U Delta-BHC 16 U 16 U 17 U 68 $ 64 $ 0.33 U Aldrin 16 U 16 U 17 U 90 $ 119 % 0.33 U Heptachlor epoxide 16 U 16 U 17 U 93 $ 113 $ 0.33 U gamma-Chlordane 16 U 16 U 17 U 84 $ 119 $ 0.33 U .. Endosulfan I 16 U 16 U 17 U 94 $ 136 * $ 0.33 U alpha-Chlordane 16 U 16 U 17, U 94 $ 132 * $ 0.33 U 4,4'-DDE 16 U 16. U 17 U 95 V 141 * $ 0.33 U Dieldrin 16 U 16 U 17 U 91 $ 132 * % 0.33 T ... Endrin 16 U 16 U 17 U 111 _ $ 157 * $ 0.33 U 4;4'-DDD 16 U 16 U 17 ,U 102 t 197 *. % 0.33 U Endosulfan II 16 U 16 U 17 II 94 $ 134 *$ 0.33 U 4,4'-DDT 16 U 16 U 17 U 79 $ 43 $ 0.33 U Endrin aldehyde 16 U 16 U 17 U 10 * % 5 * $ 0.33 U Endosulfan sulfate 16 U 16 U 17 U 58 * t 28 * $ 0.33 U Methoxychlor 16 U 16 U 17 U 107 $ 75 $ 0.33 U Endrin ketone 16 U 16 U 17 U 79 $ 72 $ 0.33 U Toxaphene 160 U 160 U 170 U 180 U 180 U 3.3 U U- Analyzed, not detected. J- Present below detection limit. B- Present in blank. NR. Not reported. NS= Not spiked. $. Percent recovery. D. Diluted out. I= Interference. NA. Not Applicable. *- Outside of EPA CLP QC m CD
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Client: TNU-HANFORD RC-047 WON: 113
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METALS METHOD GLOSSARY The followin
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CLIENT: TNUHANFORD RC-047 K0303 WOR
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Lionville Laboratory, Inc, INORGANI
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SAMPLE SITE ID LCS1 06L0324-LC1 ANA
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Lionville Laboratory Use On ly Cust
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Washington Closure Hanford CHAIN OF
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v Washington Closure Hanford CHAIN
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Washington Closure Hanford " CHAIN
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Lionville Laboratory Incorporated S
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Case Narrative Client: TNU-HANFORD
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_WrrvurV r..duvrdtory -)ampie Initi
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Lionville Laborato ry Sample Discre
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ABBREVIATIONS GLOSSARY BS — Indic
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uivuviaio ueuaaa.n wa.]i, aau. Semi
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--------- ----------- r-.-- Semivol
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Semivolatiles by GC/MS, HSL List Re
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RFW Batch Number: 0604L904 Semivola
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IF CLiENT SAMPLE NO. SEMIVOLATILE O
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1F SEMIVOLATILE ORGANICS ANALYSIS D
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1F CLIENT SP.MPLE NO. SEMIVOLATILE
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Injection Volume: 2_0(uL) GPC Clean
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IF CLTENT SAMPLE NO. SEMIVOLATILE O
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IF CLIENT SAMPLE NO. SEMIVOLATILE O
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IF SEMIVOLATILE ORGANICS ANALYSIS D
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1F SEMIVOLATILE ORGANICS ANALYSIS D
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Lionville Lanoratory, inc. SAMPLE E
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Lionville Laboratory Use On ly Clie
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Washineton Closure Hanford CHAIN OF
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Washin>;ton Closure Hanford CHAIN O
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w EBERLINE VSERVICES May 30, 2006 M
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E B E R L I N E S E R V I C E S/ R
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E B ERLINE SERVICES/RICHMOND SAMPLE
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EBERLINE SERVICES/RICHMOND SAMPLE D
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SDG 7420 EBERLINE SERVICES/RICHMOND
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R604093-19 SDG 7420 Contact Melissa
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EBER L INE SER V ICES / RICHMOND SA
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EBE RL INE SERVICES /R ICHMOND SAMP
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EBERLINE SERVICES/RICHMON D SAMPLE
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Test TH Matrix SOLID EBERLINE SERVI
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EBER L INE SERVI CES / RI CHMOND SA
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EBERLINE SERVI CES / RI C HM O ND S
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EBERLINE SE RV I CES /RI CHMOND SAM
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DATE RECEIVED: 04/12/06 CLIENT ID L
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11. The continuing calibration stan
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VLY=LM=1W DATA OUALIF'IERS GLOSSARY
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Lionville Laboratory Use Only Custo
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usaueueuaa^- ^^1 Washington osure I
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s - Washington Closure Hanford CHAI
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Client: TNU-HANFORD RC-047 W.O.#: 1
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METALS METHOD GLOSSAR Y The followi
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CLIENT: TNURANPORD RC-047 X0303 WOR
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CD 0 0 0 CD 9 6 A W Lionville Labor
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