SAF-RC-047 100 & 300 Area Component of the ... - Hanford Site

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8. All laboratory control samples (LCS) were within the 80-120% control limits with the exception of Silicon at 31.2%. Refer to the Inorganics Laboratory Control Standards Report. Associated sample results may be biased low. 9. The matrix spike (MS) recoveries for 4 analytes were outside the 75-125% control limits. Refer to the Inorganics Accuracy Report. 10. For analytes where the ICP MS is out-of-control, a post-digestion MS (PDS) and serial dilution are performed. A PDS was not performed for Zinc. A PDS was prepared at meaningful concentration level for the following analytes: PDS PDS Sample ID Element Concentration (onb) % Recovery J11KV6 Iron 22,000 101.9 Phosphorous 4,000 110.5 Zirconium 200 100.4 11. The duplicate analyses for 8 analytes were outside the 201/6 Relative Percent Difference (RPD) control limits. Refer to the Inorganics Precision Report. 12. For the purposes of this report, the data has been reported to the Instrument Detection Limit (IDL). Values between the IDL and the Practical Quantitation Limit (PQL) are acquired in a region of less-certain quantification. 13. LvLI is NELAP accredited by the state of Pennsylvania and holds over 20 additional state accreditations. For a complete listing of accrediting authorities and the corresponding analytes/methods, please contact your Project Manager. 14. I certify that this sample data package is in compliance with SOW requirements, both technically and for completeness, other than the conditions detailed above. Release of the data contained in this hard-copy data package has been authorized by the Laboratory Manager or a designee, as verified by the following signature. aniel rrrr Laboratory Manager Lionville Laboratory Incorporated jjw/m04750 vLl 4u Date
METALS METHOD GLOSSAR Y The following methods are used as'reference for the digestion and analysis of samples contained within f Lot#: pbo y L^5-v s Leaching Procedure: _1310 _1311 _1312 _Other: CLP Metals _Digestion and _ Analysis Methods: "03.0 _ILMO4.0 Metals Digestion Methods: _3005A _3010A _3015 _3020A Zo3050B _3051 _200.7 _SS17 Other. Aluminum Antimony Arsenic Ba SW846 -)C 601 OR )c601 0B _7041' ^C 601 OR `7060A ri Metals Analysis Methods EPA um Beryllium Bismuth Boron Cadmium Calcium Chromium Cobalt Copper Iron Lead Lithium Magnesium Manganese Mercury Molybdenum Nickel Potassium Rare Earths Selenium Silicon Silica Silver Sodium Stron tium Thallium Tin Titanium Uranium Vanadium Zinc Zirconium EPA STD MTD _200.7 _200.7 204.2 200.7 206.2 311313 -f- 601 OR _200.7 *C6010B _200.7 Y-6010B' _200.7' 6010B _200.7 16010B _7131A' _200.7 _213.2 7r-6010B _200,9 ^C6010B _7191' 200.7 218.2 --ewlw _200.7 r 6010 _7211' _200.7 _220.2 r6010B 200.7 35601013 _7421' _200.7 _239.2 3113B ^J6010B _7430' 200;7 Zc6OIOB 200.7 -f-6010B ::200.7 7470A'r-7471 245.1 '_245.5 2 -jC 6010B _200.7 f- 601 _200.7 ^EWJOB _7610' _200.7 _258.1' _601013 ' 200.7 1 6010B _7740' 200.7 270.2 3113B 1601 OR 200.7 _6010B _200.7 601013 _7761 _200.7 _272.2 601013 _7770' _200.7 273.14 ^601 OR 200.7 •,f6010B _7841' 200.7!279.2_200.9 JG60IOB _200.7 _601 OR _200.7 5&OlOB' 200.7' 6010B -200,7 601013 200.7 ^6010B' 200,7' OSWR _1620 _1620 _1620 _1620 _1620 _1620 _1620 USATHAMA 99 _99 99 99 99 _SS17 _99 _99 _99 _99 _99 -^• _99 _99 99 99 _99 99 99 99 99 99 99 99 99 -^ 99 99 99 99 Other: p Method• 4moQ 4m, . 000000021
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SAF-RC-047 100 & 300 Area Component
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Lionville Laboratory, ry, Inc. PEST
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7. Two (2) of twenty (20) blank spi
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Lionville Laboratory, Inc. Extract.
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I Lionville Laborato ry Use Only b
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Washington Closure Hanford CHAIN OF
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Washin)Iton Closure Hanford CHAIN O
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Washington Closure Hanford " " CHAI
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SR-002-B 13. VOA, TOC, TOX free of
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Case Narrative Client: TNU-I IANFOR
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Lionville Laborato ry Sample Discre
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19 rNnn1r L10oFAIOF'r /^' DATA QUAL
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PCBs by GC Report Date: 07/10/06 11
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Lionville Laborato ry Use Only Cust
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Washineton Closure Hanford CHAIN OF
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Washington Closure Hanford Collect"
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Lionville Laboratory, Inc_ INORGANI
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Client: TNU-HANFORD RC-047 WON: 113
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METALS METHOD GLOSSARY The followin
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CLIENT: TNUHANFORD RC-047 K0303 WOR
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Lionville Laboratory, Inc, INORGANI
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SAMPLE SITE ID LCS1 06L0324-LC1 ANA
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Lionville Laboratory Use On ly Cust
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v Washington Closure Hanford CHAIN
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Washington Closure Hanford " CHAIN
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Lionville Laboratory Incorporated S
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Case Narrative Client: TNU-HANFORD
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_WrrvurV r..duvrdtory -)ampie Initi
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Lionville Laborato ry Sample Discre
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ABBREVIATIONS GLOSSARY BS — Indic
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uivuviaio ueuaaa.n wa.]i, aau. Semi
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--------- ----------- r-.-- Semivol
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Semivolatiles by GC/MS, HSL List Re
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RFW Batch Number: 0604L904 Semivola
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IF CLiENT SAMPLE NO. SEMIVOLATILE O
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1F SEMIVOLATILE ORGANICS ANALYSIS D
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1F CLIENT SP.MPLE NO. SEMIVOLATILE
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Injection Volume: 2_0(uL) GPC Clean
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IF CLTENT SAMPLE NO. SEMIVOLATILE O
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IF SEMIVOLATILE ORGANICS ANALYSIS D
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1F SEMIVOLATILE ORGANICS ANALYSIS D
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Lionville Lanoratory, inc. SAMPLE E
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Lionville Laboratory Use On ly Clie
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Washineton Closure Hanford CHAIN OF
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w EBERLINE VSERVICES May 30, 2006 M
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E B ERLINE SERVICES/RICHMOND SAMPLE
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EBERLINE SERVICES/RICHMOND SAMPLE D
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SDG 7420 EBERLINE SERVICES/RICHMOND
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R604093-19 SDG 7420 Contact Melissa
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EBER L INE SERVI CES / RI CHMOND SA
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EBERLINE SERVI CES / RI C HM O ND S
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