SAF-RC-047 100 & 300 Area Component of the ... - Hanford Site

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TECHNICAL FLAGS FOR MANUAL INTEGRATION Manual quan modifications or integrations are performed routinely to improve the data quality for a variety of technical reasons. Documentation of these modifications should be clear and concise. The following `flags' are used to indicate the technical reasons for quan modifications: MP - Missed Peak: Manually added peak not found by automatic quan program. PA - Peak Assignment: Quan report was changed to reflect correct peak assignment. RI - Routine Integration: Routine integrations are performed for some analytes that are consistently integrated improperly by the automatic integration programs. Examples are the Dichlorobenzene isomers on the VOA packed column and Benzo (b) fluoranthene /Benzo (k) fluoranthene which are poorly resolve on the BNA column. SP - Split Peak: The automatic integration improperly split the peak; a manual integration was performed to get the correct area. CB - Co-elution/ Background: Peak was manually integrated to eliminate contribution from co-eluting compounds, background signal, or other interference. PI - Proper Integration: A peak with poor or inconsistent integration (i.e., excessive tail) was properly integrated manually. LV -21-21-035/AZM 909099009
uivuviaio ueuaaa.n wa.]i, aau. Semivolatiles by GC/MS, HSL List Report Date: 07/13/06 13:42 RFW Batch Number: 06041,904 Client: TNUHANFORD RC-047 K0303 Work Order: 11343606001 Pane, la Cust ID: JllKKS J11KK8 J11KK8 J11KL5 J11KL6 1T11KM0 Sample RFW#: 001 001 MS 001 MSD 002 003 004 Information Matrix: SOLID SOLID SOLID SOLID SOLID SOLID D.F.: 0.800 0.800 0.800 0.800 0.800 0.800 Units: ug/Kg ug/Kg ug/Kg ug/Kg ug/Kg ug/Kg Nitrobenzene-d5 0 * % 11 * t Surrogate 2-Fluorobiphenyl 6 * % 13 * t Recovery Terphenyl-d14 17 * % 16 * % Phenol-d5 2 * % 12 * 2-Fluorophenol 1 * % 10 * 2,4,6-Tribromophenol 15 * t 17 * Phenol 4000 U 14 * t bis(2-Chloroethyl)ether 4000 U 12 * 2-Chlorophenol 4000 U 13 * °s 1,3-Dichlorobenzene 4000 U 11 * jr 1,4-Dichlorobenzene 4000 U 11 * % 1,2-Dichlorobenzene 4000 U 11 * t 2-Methylphenol 4000 U 14 * 2,2'-oxybis(1-Chloropropane) 4000 U 12 * 4-Methylphenol 4000 U 15 * t N- Nitroso-di-n-propylamine 4000 U 15 * t Hexachloroethane 4000 U 10 * % Nitrobenzene 4000 U 12 * % Isophorone 4000 U 13 * t 2-Nitrophenol 4000 U 13 * t 2,4-Dimethylphenol 4000 U 15 * t bis(2-Chloroethoxy)methane 4000 U 13 * t 2,4-Dichlorophenol 4000 U 14 * 1,2,4-Trichlorobenzene 4000 U 12 * t Naphthalene 4000 U 12 * t 4- Chloroaniline 4000 U 13 * % Hexachlorobutadiene 4000 U 14 * 4- Chloro-3-methylphenol 4000 U 14 * 2-Methylnaphthalene 4000 U 14 * Hexachlorocyclopentadiene 4000 U 7 * t 2,4,6-Trichlorophenol 4000 U 15 2,4,5-Trichlorophenol 9900 U 14 * *= Outside of EPA CLP QC limits. 24 t 14 * 0 7 * % 17 * % 30 % 25 * % 14 * t 21 * t 37 % 31 1 22 % 31 % 25 21 * 1 13 * % 21 * t 21 * % 14 * t 7 * t 16.* % 42 % 30 21 % 26 t 29 * % 540 J 3700 U 640 J 26 * % 3700 U 3700 U 3400 U 28 * % 3700 U 3700 U 3400 U 24 *s 3700 U 3700 U 3400 U 24 * 3700 U 3700 U 3400 U 25 * % 3700 U 3700 U 3400 U 28 * t 3700 U 3700 U 3400 U 25 * t 3700 U 3700 U 3400 U 32 * t 230 J 3700 U 3400 U 31 * % 3700 U 3700 U 3400 U 22 * t 3700 U 3700 U 3400 U 26 * t 3700 U 3700 U 3400 U 29 * t 3700 U 3700 U 3400 U 29 * % 3700 U 3700 U 3400 U 31 * % 3700 U 3700 U 3400 U 29 * t 3700 U 3700 U 3400 U 30 * % 3700 U 3700 U 3400 U 27 * % 3700 U 3700 U 3400 U 27 * % 3700 U 3700 U 3400 U 26 t 3700 U 3700 U 3400 U 30 * t 3700 U 3700 U 3400 U 28 * % 3700 U 3700 U 3400 U 29 * % 3700 U 3700 U 3400 U 24 t 3700 U 3700 U 3400 U 32 t 3700 U 3700 U 3400 U 30 * t 9200 U 9200 U 8600 U m m
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SAF-RC-047 100 & 300 Area Component
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Lionville Laboratory, ry, Inc. PEST
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7. Two (2) of twenty (20) blank spi
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Lionville Laboratory, Inc. Extract.
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I Lionville Laborato ry Use Only b
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Washington Closure Hanford CHAIN OF
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Washin)Iton Closure Hanford CHAIN O
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Washington Closure Hanford " " CHAI
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SR-002-B 13. VOA, TOC, TOX free of
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Case Narrative Client: TNU-I IANFOR
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Lionville Laborato ry Sample Discre
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19 rNnn1r L10oFAIOF'r /^' DATA QUAL
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PCBs by GC Report Date: 07/10/06 11
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Lionville Laborato ry Use Only Cust
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Washineton Closure Hanford CHAIN OF
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Washington Closure Hanford Collect"
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Lionville Laboratory, Inc_ INORGANI
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Page 135 and 136: RFW Batch Number: 0604L904 Semivola
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EBERLINE SERVICES/RICHMOND SAMPLE D
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SDG 7420 EBERLINE SERVICES/RICHMOND
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R604093-19 SDG 7420 Contact Melissa
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EBER L INE SER V ICES / RICHMOND SA
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EBE RL INE SERVICES /R ICHMOND SAMP
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EBERLINE SERVICES/RICHMON D SAMPLE
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Test TH Matrix SOLID EBERLINE SERVI
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EBER L INE SERVI CES / RI CHMOND SA
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EBERLINE SERVI CES / RI C HM O ND S
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EBERLINE SERVI CES /RI CHMOND SAMPL
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EBERLINE SE RV I CES /RI CHMOND SAM
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EBERLINE SE RV ICES/RICHMOND SAMPLB
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iIL7 I-lien- tC, Il ri t"T-u ^`y Ri
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DATE RECEIVED: 04/12/06 CLIENT ID L
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11. The continuing calibration stan
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VLY=LM=1W DATA OUALIF'IERS GLOSSARY
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Lionville Laboratory Use Only Custo
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usaueueuaa^- ^^1 Washington osure I
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s - Washington Closure Hanford CHAI
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Client: TNU-HANFORD RC-047 W.O.#: 1
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METALS METHOD GLOSSAR Y The followi
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