SAF-RC-047 100 & 300 Area Component of the ... - Hanford Site

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8. All laboratory control samples (LCS) were within the 80-120% control limits with the ex cep ti on of Silicon at 69.6%. Refer to the Inorganics Laborato ry Control Standards Report. Associated sample results may be bi ased low. 9. The matrix spike (MS) recove ries for 5 analytes were outside the 75-125% control limits. Refer to the Inorganics Accuracy Repo rt . 10. For analytes where the ICP MS is out-of-control, a post-diges tion MS (PDS) and serial dilution are performed. A PDS w as prepared at meaningful concentration level for the following analytes: Sample ID Element PDS Concentra PDS ti on (pob) %Recovery J11KK8 C al cium 12,000 115.6 Iron 2,000 95.3 Phosphorous 6,000 104.1 Silicon 1,100 100.3 Zinc 100 117.1 11. The duplicate analyses for 16 analytes were outside the 20% Rela ti ve Percent Difference (RPD) control limits. Refer to the Inorg anics Precision Repo rt . 12. For the purposes of this report, the data has been reported to the Instrument Detection Limit (IDL). Values between the IDL and the Practical Quantitation Limit (PQL) are acquired in a region of less-certain quantification. 13. LvLI is NELAP accredited by the state of Pennsylv ania and holds over 20 addi ti onal state accreditations. For a complete listing of accredi ti ng authorities and the corresponding analytes/methods, ple ase contact your Project M anager. 14. I certify that this sample data package is in compli ance with SOW requirements, both technically and for completeness, other than the condi ti ons detailed above. Rele ase of the data contained in this hard-copy data package h as been autho rized by the Laborato ry Manager or a designee, as verified by the following signature. aniels I_JL^ovatory Manager Lionville Laboratory Incorporated ijw/m04-904 vLl c, )g1,^ Date 10 4W.
METALS METHOD GLOSSARY The following methods are used as 'reference for the digestion and analysis of samples contained within t Lot#: 66() 4L4aN r Leaching Procedure: -1310 -1311 -1312 ,_Other: CLP Metals_ Digestion and _ Analysis Methods: _ILM03 .0 -ILM04.0 Metals Digestion Methods: _3005A _3030A 3015 3020A x 3050B 3051 200.7 -SS17 __Other: Metals Analysis Methods EPA SW846 EPA STD MTD OSWR USATHAM , Aluminum 46010B _200.7 -99 Antimony Arsenic Ba rium Beryllium Bismuth Boron Cadmium Calcium Chromium Cobalt Copper f 6010 -7041' -200.7 -204.2 )oC 6010B -7060A -200.7 _206.2 -3113B )r, 6010B -200.7 )^- 6010B 200.7 --106010B' _200.7' )C6010B -200.7 -IC 6010B -7131A' 200.7 213.2 )C6010B -200.7 ^6010B _7191' -200.7 218.2 40010B 200.7 6010B -7211 -1620 99 -99 99 99 99 -99 -99 -99 -SSI7 -99 :200.7 Iron Lead Lithium Magnesium Manganese Mercu ry Molybdenum Nickel Potassium Rare Earths Selenium Silicon Silica Silver 220.2 ZC 6010B _200.7 6010B -7421 5 200.7 -239.2 -3113B 6030$ _7430' _200.7 6010B 200.7 6010B ll 200.7 7470A 3_)(7471A3 -245.1?2455' -y601 0B -200.7 60101 -200.7 1,60101 -7610' 200.7 _258.1' _6010B' _200.7' )C6010B -7740' -200.7 -270-23113B )L4010B' 200.7 _6010B 200.7 ^C 6010B -7761 -1620 -1620 -1620 -1620 -99 -^ -99 99 99. -99 -99 -99 -99 _99 -99 -99 -99 _99 S Sodium Strontium Thallium Tin Titanium Uranium Vanadium Zinc Zirconium 200.7 -272.2 6010B _7770' _200.7 -273.1' ^6010B 200.7 K6010B -7841' 200.7 279.2-200.9 Y 6010B -200.7 6010B 200.7 6010B' 200.7' 6010B _200.7 6010E 200.7 -6010B' 200.7' -1620 -1620 99 99 -99 99 -99 99 -99 -99 _99 Other. W d / Method: 60/06 4m.mws.om . 000000021
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SAF-RC-047 100 & 300 Area Component
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Lionville Laboratory, ry, Inc. PEST
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7. Two (2) of twenty (20) blank spi
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Lionville Laboratory, Inc. Extract.
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I Lionville Laborato ry Use Only b
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Washington Closure Hanford CHAIN OF
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Washin)Iton Closure Hanford CHAIN O
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uivuviaio ueuaaa.n wa.]i, aau. Semi
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--------- ----------- r-.-- Semivol
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Semivolatiles by GC/MS, HSL List Re
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RFW Batch Number: 0604L904 Semivola
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IF CLiENT SAMPLE NO. SEMIVOLATILE O
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1F SEMIVOLATILE ORGANICS ANALYSIS D
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1F CLIENT SP.MPLE NO. SEMIVOLATILE
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Injection Volume: 2_0(uL) GPC Clean
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IF CLTENT SAMPLE NO. SEMIVOLATILE O
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IF CLIENT SAMPLE NO. SEMIVOLATILE O
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IF SEMIVOLATILE ORGANICS ANALYSIS D
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1F SEMIVOLATILE ORGANICS ANALYSIS D
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Lionville Lanoratory, inc. SAMPLE E
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Lionville Laboratory Use On ly Clie
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Washineton Closure Hanford CHAIN OF
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Washin>;ton Closure Hanford CHAIN O
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w EBERLINE VSERVICES May 30, 2006 M
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E B E R L I N E S E R V I C E S/ R
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E B ERLINE SERVICES/RICHMOND SAMPLE
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EBERLINE SERVICES/RICHMOND SAMPLE D
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SDG 7420 EBERLINE SERVICES/RICHMOND
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R604093-19 SDG 7420 Contact Melissa
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EBER L INE SER V ICES / RICHMOND SA
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EBE RL INE SERVICES /R ICHMOND SAMP
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EBERLINE SERVICES/RICHMON D SAMPLE
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Test TH Matrix SOLID EBERLINE SERVI
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EBER L INE SERVI CES / RI CHMOND SA
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EBERLINE SERVI CES / RI C HM O ND S
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EBERLINE SERVI CES /RI CHMOND SAMPL
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EBERLINE SE RV I CES /RI CHMOND SAM
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EBERLINE SE RV ICES/RICHMOND SAMPLB
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DATE RECEIVED: 04/12/06 CLIENT ID L
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11. The continuing calibration stan
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VLY=LM=1W DATA OUALIF'IERS GLOSSARY
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Lionville Laboratory Use Only Custo
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s - Washington Closure Hanford CHAI
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Washington Closu re Hanford CHAIN O
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Client: TNU-HANFORD RC-047 W.O.#: 1
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METALS METHOD GLOSSAR Y The followi
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CLIENT: TNURANPORD RC-047 X0303 WOR
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CD 0 0 0 CD 9 6 A W Lionville Labor
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SAF-RC-047 100 & 300 Area Component of the ... - Hanford Site

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