SAF-RC-047 100 & 300 Area Component of the ... - Hanford Site

Lionville Laborato ry Sample Discrepancy Report (SDR) SDR #: 06PM002
Initiator: Orlette Johnson Batch: 06d6l,gM Parameter. G6 2S14
Date: 6/21/06 Samples: Matrix: 'td
...
Client: 1W 4vii6d A Q2_ Method: cAm1cLPr Prep Batch:
1. Reason for SDR
a. COC Discrepancy _ Tech P rofile Error Client Request Sampler Error on C-O-C
Transcription Error _ Wrong Test Code _ O ther
b. General Discrepancy .
_ Missing Sample/Extract _ Container B roken _ Wrong Sample Pulled _ Label ID's Illegible
X Hold Time Exceeded Insufficient Sample _ Preservation Wrong _ Received Past Hold
_ Improper Bottle Type _ Not Amenable to Analysis
Note: Vented by [Log4ril or (Prep Group) (drde)...algnatureddate:
c. Problem (In clude all relevant specific results; attach data if necessa ry)
Sample(s) waslwe re extracted 4^ days beyond the hold time
Sa* rt o4d to 4 js kw/ku?'^V6 &J1t.1A6
Z Known or P robable Causes(s) due to a temporary glassware shortage created by a malfunc tioning d rying kiln I.e,
much of our glassware was lost when one of the kilns overheated. We made eve ry effort to replace glassware as soon as
possible but our needs exceeded on-the-shelf vendor stocks of certain c ritical Items. This problem was exacerbated by an
unusually high number of samples received du ring this period of time for organics extraction.
3. Discussion and P roposed Action Other Description:
_ Re-log
_ Entire Batch
Following Samples: We have replenished glasswa re stocks to higher levels than those
_ Re-leach in-house before the kiln malfunction. We have also replaced the kiln.
_ Re-extract
_ Re-digest
_ Revise EDD
Change Test Code to
_ Place O rdTake Off Hold (circle)
4. P roject Manager Instructions ... smnature/date:
_ Concur with Proposed Action
Disagree with P roposed Action; See Instruction
X Include in Case Narra ti
ve
_ Client Contacted:
Date/Person
_ Add
Cancel
S. Final Action ... synatureidate: Other Explana ti
on:
Ve rified re-[log][leach][ digest][analysr ] ( rcle)
X Included in Case Narrative
_ Hard Copy COC Revised
Electronic COC Revised
_ EDD Corrections Completed
When Final Action has been recorded, forward original to OA Specialist for distribution and filing.
Route Distribution of Completed SDR
X Ini
Route Distribution of Completed SDR
ti
ator
X Lab Genera[ Man I. anrels
X P roject Mgr. Ston o' son
X Data Management
_ Sample Prep: I(iger
—
_ Metals: Welsh
_ _ Inorganic: Perrone
GC/LC: Kiger
'L `^ MS: Schne[de arclen
_ _ Log-in: Per ry
Admin:
Other.
oA-ios-A-osos
096000605