SAF-RC-047 100 & 300 Area Component of the ... - Hanford Site

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Case Narrative Client: TNU-HANFORD RC-047 W.O. #: 11343-606-001-9999-00 LVL #: 0604L750 Date Received: 04-12-2006 SDG/SAF # K0303/RC-047 CHLORINATED PESTICIDES One (1) solid samples was collected on 04-03-2006. The sample and it's associated QC samples were extracted on 04-23-2006 and analyzed according to Lionville Laboratory SOPS based on SW846, 3rd Edition procedures on 05-03,07-2006. The extraction procedure was based on method 3540C and the extracts were analyzed based on method 8081. All soil samples are reported on a dry weight base unless requested by the client, required by the method or noted otherwise. The following is a summary of QC results accompanying the sample results. Lionville Laboratory Inc (LvLI) certifies that all test results meet the requirements of NELAC except as noted below: 1. The sample was analyzed within required holding time. 2. The sample was extracted 20 days outside of recommended hold time. A copy of the Sample Discrepancy Report has been enclosed. The sample and it's associated QC samples received Copper-Sulfur cleanups according to Lionville Laboratory SOPS based on SW846 methods 3660A respectively. 4. The method blank was below the reporting limits for all target compounds. Two (2) of six (6) surrogate recoveries were outside acceptance criteria. A copy of the Sample Discrepancy Report (SDR) has been enclosed. 6. The blank spike recoveries were within acceptance criteria. 7. Matrix spike analyses are associated with LvLi lot 0604L748. 8. The results for soil samples were reported on a wet-weight basis. 9. The sample 011 required a 4-fold instrument dilutions due to matrix. Reporting limits have been adjusted to reflect the necessary dilutions. 10. The initial calibrations associated with this data set were within acceptance criteria. The results presented in this report relate only to the analytical testing and wnditiona of the samples at receipt mid dining storage. All pages of this report are integral pans of the analytical data. Therefore, flus report should only be reproduced in its entirety of 42 7 pages. 208 Welsh Pool Road • Exton, PA 19341- 1313 • (610) 280-3000 • Fax (610) 280-3041 MGMG88Z
11. The continuing calibration standards analyzed prior to sample extracts were within acceptance criteria. 12. LvLI is NELAP accredited by the state of Pennsylvania and holds over 20 additional state accreditations. For a complete listing of accrediting authorities and the corresponding analytes/methods, please contact your Project Manager. 13. I certify that this sample data package is in compliance with SOW requirements, both technically and for completeness, other than the conditions detailed above. Release of the data contained in this hard-copy data package has been authorized by the laboratory Manager or a designee, as verified by the following signature. Laboratory Manager Lionville Laboratory Incorporated Idmtr:\VoupWata\pest\mu ha,ifotd\0604-750.pst vLl ,-511(10P Date
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SAF-RC-047 100 & 300 Area Component
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Lionville Laboratory, ry, Inc. PEST
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7. Two (2) of twenty (20) blank spi
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Lionville Laboratory, Inc. Extract.
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I Lionville Laborato ry Use Only b
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Washington Closure Hanford CHAIN OF
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Washin)Iton Closure Hanford CHAIN O
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Washington Closure Hanford " " CHAI
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SR-002-B 13. VOA, TOC, TOX free of
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Case Narrative Client: TNU-I IANFOR
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Lionville Laborato ry Sample Discre
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19 rNnn1r L10oFAIOF'r /^' DATA QUAL
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PCBs by GC Report Date: 07/10/06 11
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Lionville Laborato ry Use Only Cust
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Washineton Closure Hanford CHAIN OF
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Washington Closure Hanford Collect"
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Lionville Laboratory, Inc_ INORGANI
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Client: TNU-HANFORD RC-047 WON: 113
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METALS METHOD GLOSSARY The followin
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CLIENT: TNUHANFORD RC-047 K0303 WOR
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Lionville Laboratory, Inc, INORGANI
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CLIENT: TNUMANPORD RC-047 K0303 MOR
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CLIENT: TNUHANFORD RC-047 K0303 WOR
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CLIENT: T14URANFORD RC-047 K0203 WO
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CLIENT: TNUNANFORD RC-047 K03O3 WOR
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SAMPLE SITE ID LCS1 06L0324-LC1 ANA
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Lionville Laboratory Use On ly Cust
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v Washington Closure Hanford CHAIN
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Washington Closure Hanford " CHAIN
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Lionville Laboratory Incorporated S
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Case Narrative Client: TNU-HANFORD
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_WrrvurV r..duvrdtory -)ampie Initi
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Lionville Laborato ry Sample Discre
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ABBREVIATIONS GLOSSARY BS — Indic
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uivuviaio ueuaaa.n wa.]i, aau. Semi
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--------- ----------- r-.-- Semivol
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Semivolatiles by GC/MS, HSL List Re
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RFW Batch Number: 0604L904 Semivola
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IF CLiENT SAMPLE NO. SEMIVOLATILE O
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1F SEMIVOLATILE ORGANICS ANALYSIS D
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1F CLIENT SP.MPLE NO. SEMIVOLATILE
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Injection Volume: 2_0(uL) GPC Clean
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IF CLTENT SAMPLE NO. SEMIVOLATILE O
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IF CLIENT SAMPLE NO. SEMIVOLATILE O
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IF SEMIVOLATILE ORGANICS ANALYSIS D
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1F SEMIVOLATILE ORGANICS ANALYSIS D
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Lionville Lanoratory, inc. SAMPLE E
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Lionville Laboratory Use On ly Clie
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Washineton Closure Hanford CHAIN OF
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Washin>;ton Closure Hanford CHAIN O
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w EBERLINE VSERVICES May 30, 2006 M
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E B E R L I N E S E R V I C E S/ R
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E B ERLINE SERVICES/RICHMOND SAMPLE
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EBERLINE SERVICES/RICHMOND SAMPLE D
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SDG 7420 EBERLINE SERVICES/RICHMOND
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R604093-19 SDG 7420 Contact Melissa
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EBER L INE SER V ICES / RICHMOND SA
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