SAF-RC-047 100 & 300 Area Component of the ... - Hanford Site

Case Narrative
Client: TNU-HANFORD RC-047 W.O. #: 11343-606-001-9999-00
LVL #: 06041,904 Date Received: 04-28-2006
SDG/SAF # K0303/RC-047
SEMIVOLATILE
Fifteen (15) soil (mice) samples were collected on 04-03,05-2006.
The samples and their associated QC samples were extracted according to Lionville Laboratory
SOPs based on SW 846 method 3540C on 06-02-2006 and analyzed according to criteria set forth
in Lionville Laboratory SOPS based on SW 846 Method 8270C for TCL Semivolatile target
compounds on 06-29,30-2006 and 07-02-2006.
The following is a summary of QC results accompanying the sample results. Lionville Laboratory
Inc (LvLI) certifies that all test results meet the requirements of NELAC except as noted below:
1. All results presented in this report are derived from samples that met LvLI's sample
acceptance policy with the exception of some discrepancies, which were documented on the
Sample Receipt Checklist.
2. All samples were stored in a refrigerator (ID# R003) that malfunctioned and failed to
maintain the required sample storing temperature (4°C +/- 2°C) on 05-10-2006. A copy of
the Sample Discrepancy Report (SDR) has been enclosed.
3. Samples were extracted outside required holding time. A copy of the Sample Discrepancy
Report (SDR) has been enclosed.
4. Due to the nature of the sample matrix, approximately 2g initial sample volume for the
extraction and reduced final volume was used for the analysis. A copy of the Sample
Extraction Record has been enclosed for detail information.
5. All sample results were reported on a wet-weight basis.
6. Non-target compounds were detected in the samples.
7. Seventy-seven (77) of one hundred fourteen (114) surrogate recoveries were outside
acceptance criteria. A copy of the Sample Discrepancy Report (SDR) has been enclosed.
The results presented in this report relate only to the analytical testing and conditions of the samples at receipt and during storage. All pages of this report are integral parts of
the analytical data. Therefore, this report should only be reproduced in its entirety of 5 3 pages.
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