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SAF-RC-047 100 & 300 Area Component of the ... - Hanford Site

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Lionville Laboratory Sample Discrepancy Report (SDR) SDR #: 06PM001<br />

Initiator. Odette Johnson Batch: T Parameter: AW AVA, Y°^<br />

Date: /1706 Samples: Mat ri<br />

x:<br />

Client: Method: swaesnacAVVwrcm P rep Batch:<br />

1. Reason for SDR<br />

a. COC Disc repancy _ Tech Pr<strong>of</strong>ile Error _ C li<br />

ent Request Sampler Error on C-O-C<br />

Transcription Error _ Wrwg Test Code _ O<strong>the</strong>r<br />

b. General Discrepancy<br />

_ Missing Sample/Extract _ Container B roken Wrong Sample Pulled _ Label ID's Illegible<br />

Hold Time Exceeded<br />

Improper Bot<br />

Insufficient Sample Preservation Wrong _ Received Past Hold<br />

tl<br />

e Type _ Not Amenable to Analysis X O<strong>the</strong>r<br />

Note: Verified by [Log-In) or [Prep amp[ (drde) ... signeture/daw.<br />

c. Problem (Include all relevant specific results; attach data If necessa ry)<br />

On 5110/06 sample storage refrigerator ID# R003 malfunctioned and was not holding <strong>the</strong> required sample storage<br />

temperature <strong>of</strong> 4'C +/- 2°C<br />

2. Known or P robable Causes(s)<br />

Broken motor<br />

3..Discuss[on and P roposed Action.... O<strong>the</strong>r Description:<br />

_ Re-log At <strong>the</strong> time <strong>of</strong> malfunction R003 was used for storage <strong>of</strong> samples received<br />

_ Entire Batch for extractable organics, metals and wet chemist ry (except TOC) analyses.<br />

Following Samples: All samples were removed from R003 to ano<strong>the</strong>r refrigerator on 5/10/06.<br />

_ f e-Ieach R003 was tagged out on 5/10106, repaired on 5/12/06, and we have<br />

_ Re-extract certified that R003 is maintaining <strong>the</strong> required sample storage temperature.<br />

_ Re-digest<br />

_ Revise EDD<br />

Change Test Code to<br />

_ Place On/Take Off Hold (circle)<br />

4. Project Manager Instructions ... signaturefdate:<br />

Concur with P ro posed Action<br />

gree with Proposed Action; See Instruc<br />

r<br />

ti on<br />

^/ nclude in Case Narrative<br />

Client Conte<br />

Date/Person ^i del l.t^ fGy^D^p<br />

_ Add<br />

Canoel<br />

S. Fine -Acdon..sgnatureaate:<br />

nfied re-[log][leach][extract]<br />

K^Ihcluded in Case Narrative<br />

_ Hard Copy COC Revised<br />

Electronic CDC Revised<br />

_ EDD Co<br />

est)[analysi ] circi )<br />

O<strong>the</strong>r Explanation:<br />

rr ec ti<br />

ons Completed<br />

When Final Action has been recorded, forward original to OA Specialist for dis tribu tion and filing.<br />

Route Distribution <strong>of</strong> Completed SDR Route Distribution <strong>of</strong> Completed SDR<br />

X Initiator _ _ Metals: Welsh<br />

X Lab Manager. I. Daniels Inorganic: Perrone<br />

X Project Mgr. Stone/Johnson _ GC/LC: IQger<br />

Data Management: Stilwell _ MS: Schneider/Daley<br />

_ Sample Prep: BeegleNger _ Log-in: Per ry<br />

Admin:<br />

O<strong>the</strong>r.<br />

oA-105-A-DW5<br />

069960005

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