SAF-RC-047 100 & 300 Area Component of the ... - Hanford Site

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EBERLINE SERVICES/RICHMOND SAMPLE DELIVERY GROUP K0303 Test PU Matrix SOLID Client Hanford SDG 7420 METHOD SUMMARY Contract No. 630 Contact Melissa C. Mannion PLUTONIUM, ISOTOPIC IN SOLIDS Contract SDG K0303 RESULTS ALPHA SPECTROSCOPY LAB RAW SUF- Plutonium Plutonium CLIENT SAMPLE ID SAMPLE ID TEST FIX PLANCHET 238 239/240 Preparation batch 7181-066 J11KK8 R604093-02 7420-002 U U J11KL5 R604093-03 7420-003 U U Jll KL6 R604093-04 7420-004 U U J11KM0 R604093-05 7420-005 U U JllKM2 R604093-06 7420-006 U U Jll KM3 R604093-07 7420-007 U U Jll KM4 R604093-OB 7420-008 U U J1lKM5 R604093-09 7420-009 U U J11KM6 R604093-10 7420-010 U U J11KV1 R604093-11 7420-011 U U J11KV2 R604093-12 7420-012 U U JIIL21 R604093-13 7420-013 U U JIIL23 R604093-14 7420-014 U U JlIL25 R604093-15 7420-015 U U JlIL36 R604093-16 7420-016 U U Method Blank R604093-18 7420-018 U U Lab Control Sample 8604093-17 7420-017 Ok Ok Duplicate (R604093-06) R604093-19 7420-019 - U - U Nominal values and limits from method RDLS (pCi/g) 1.0 1.0 100&300Area Compnt RCBRA Sediment6Ti Lab id EBRLNE Protocol Hanford METHOD SODAfARIES Version Ver 1.0 Page 1 Form DVD-CMS SUMMARY DATA SECTION Version 3.06 Page 31 Report date 05/25/06
EBERLINE SERVICES/RICHMOND SAMPLE DELIVERY GROUP K0303 Test PU Matrix SOLID Client Hanford SDG 7420 METHOD SUMMARY Contract No. 630 Contact Melissa C. Mannion PLUTONIUM, ISOTOPIC IN SOLIDS Contract SDO K0303 METHOD PERFORMANCE ALPHA SPECTROSCOPY LAB RAW SUF- MAX MDA ALIQ PREP DILU- YIELD EFF COUNT FWHM DRIFT DAYS ANAL- CLIENT SAMPLE ID SAMPLE ID TEST FIX pci/g g PAC TION k % min keV KeV HELD PREPARED YZED DETECTOR Preparation batch 7181-066 2a prep error 5.0 % Reference Lab Notebook 7181 pg. 66 J11KK8 R604093-02 0.24 0.500 49 172 J11KL5 R604093-03 0.25 0.500 55 172 J11KL6 R604093-04 0.20 0.500 58 173 J11KMO R604093-05 0.26 0.500 56 173 J11KM2 R604093-06 0.17 0.500 68 173 J11KM3 R604093-07 0.14 0.500 82 173 JIIKM4 R604093-08 0.25 0.500 49 173 JllKM5 R604093-09 0.35 0.500 44 144 J11KM6 R604093-10 0.39 0.500 '59 103 J11KV1 R604093-11 0.46 0.500 37 144 J11KV2 R604093-12 0.33 0.500 45 144 J111,21 R604093-13 0.29 0.500 61 144 J111,23 R604093-14 0.33 0.500 48 145 J11L25 R604093-15 0.29 0.500 60 114 JlIL36 R604093-16 0.33 0.500 55 114 Method Blank R604093-18 0.27 0.500 68 114 Lab Control Sample R604093-17 0.20 0.500 90 114 Duplicate (R604093-06) R604093-19 0.29 0.500 69 113 Nominal values and limits from method 1.0 0.500 20-105 100 100 180 PROCEDURES REFERENCE PUISO_PLATE_AEA CP-071 Soil Dissolution, > 1.Og Aliquot, rev 5 CP-941 Plutonium in Water and Dissolved Samples by Extraction Chromatography, rev 3 CP-008 Heavy Element Electroplating, rev 9 42 05/17/06 05/17 SS-027 42 05/17/06 05/17 SS-028 44 05/17/06 05/17 SS-029 42 05/17/06 05/17 SS-031 44 05/17/06 05/17 SS-032 44 05/17/06 05/17 SS-033 44 05/17/06 05/17 SS-034 44 05/17/06 05/17 SS-035 49 05/17/06 05/22 SS-040 42 05/17/06 05/17 SS-036 42 05/17/06 05/17 SS-038 44 05/17/06 05/17 SS-039 44 05/17/06 05/17 SS-040 42 05/17/06 05/17 SS-055 44 05/17/06 05/17 SS-056 05/17/06 05/17 SS-058 05/17/06 05/17 SS-057 44 05/17/06 05/17 SS-059 AVERAGES t 2 SO M)A 0.28 3 0.16 FOR 18 SAMPLES YIELD 58 ; 27 Lab id EBRLNE Protocol Hanford METHOD SUMMARIES Version Ver 1.0 Page 2 Form DVD-CMS SUMMARY DATA SECTION Version 3.06 Page 32 Report date 05/25/06
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SAF-RC-047 100 & 300 Area Component
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METALS METHOD GLOSSARY The followin
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SAMPLE SITE ID LCS1 06L0324-LC1 ANA
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RFW Batch Number: 0604L904 Semivola
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IF CLiENT SAMPLE NO. SEMIVOLATILE O
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1F SEMIVOLATILE ORGANICS ANALYSIS D
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Injection Volume: 2_0(uL) GPC Clean
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IF CLTENT SAMPLE NO. SEMIVOLATILE O
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