SAF-RC-047 100 & 300 Area Component of the ... - Hanford Site

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Lionville Laboratory, Inc. INORGANIC ANALYTICAL DATA PACKAGE FOR TNUHANFORD RC-047 K0303 DATE RECEIVED: 04/28/06 LVL LOT # :06041,904 CLIENT ID /ANALYSIS LVL # MTX PREP # COLLECTION EXTR/PREP ANALYSIS THALLIUM, TOTAL MB1 S 06LO324 N/A 05/25/06 05/26/06 URANIUM LABORATORY LC1 BS S 06LO324 N/A - 05/25/06 05/26/06 URANIUM, TOTAL MB1 S 06L0324 N/A 05/25/06 05/26/06 VANADIUM LABORATORY LC1 BS S 06L0324 N/A 05/25/06 05/26/06 VANADIUM, TOTAL MB1 S 06L0324 N/A 05/25/06 05/26/06 ZINC LABORATORY LC1 BS S 06LO324 N/A 05/25/06 05/26/06 ZINC, TOTAL MB1 S 06L0324 N/A 05/25/06 05/26/06 000000018
Client: TNU-HANFORD RC-047 WON: 11343-606-001-9999-00 LVL#: 0604L904 Date Received: 04-28-06 SDG/SAF4: K0303/RC-047 METALS CASE NARRATIVE The following is a summary of the QC results accomp anying the sample results. Lionville Laborato ry (LvLI) certi fi es that all test results meet the requirements of NELAC except as noted below. All soil samples are repo rted on a dry weight basis unless requested by the client, required by the method, or noted otherwise. This narrative covers the analyses of 15 solid samples. 2. The samples were prepared and analyzed in accordance with methods checked on the attached glossary. The samples are reported on a wet weight, `as received' basis. All samples were rerun for Aluminum, Be ryllium, and Copper, along with the Phosphorous analysis, due to sample matrix. The matrix spike of sample J11KK8, and samples J1 1L21 and J11L23 were rerun for Phosphorous due to high concen trations. 3. All analyses were performed within the required holding ti mes. 4. All Ini ti al and Con ti nuing Calibration Verifications (ICV/CCVs) were within the 90-110% con trol limits (80-120% for Mercury). 5. All Ini tial and Continuing Calibration Blanks (ICB/CCBs) were within con trol limits (less than the PQL). 6. The preparation/method blanks for 2 analytes were outside method c riteria (less than the Prac ti cal Quantitation Limit (3X the IDL), or samples greater than 20X MB value). Refer to the Inorganics Method Blank Data Summary . a). The MB results for Aluminum and Uranium were greater than the Prac ti cal Quantitation Limit (PQL) (3 x the (IDL) Instrument Detection Level) and al l samples read less than 20 ti mes the MB concentration for Aluminum. However, no corrective ac ti on criteria for MBs were provided in SW846 method 6010B. The sample results were repo rted herein "uncorrected" for the levels found in the MB. All samples were below the IDL for Uranium. All ICP Interference Check Standards were within con trol limits. The re su lts presented in this re port relate only to the analytical testing and conditions ofthe samples at receipt and during storage. All pages ofthis re po rt are integral pads ofthe analy tical data The re fo re , this report should only be reproduced in its entirety of ^C pages. 208 Welsh Pool Road • Exton, PA 19341- 1313 • (610) 280-3000 • Fax (610) 280-3047
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SAF-RC-047 100 & 300 Area Component
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Lionville Laboratory, ry, Inc. PEST
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ABBREVIATIONS GLOSSARY BS — Indic
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Semivolatiles by GC/MS, HSL List Re
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RFW Batch Number: 0604L904 Semivola
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IF CLiENT SAMPLE NO. SEMIVOLATILE O
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1F SEMIVOLATILE ORGANICS ANALYSIS D
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Injection Volume: 2_0(uL) GPC Clean
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DATE RECEIVED: 04/12/06 CLIENT ID L
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11. The continuing calibration stan
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VLY=LM=1W DATA OUALIF'IERS GLOSSARY
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Client: TNU-HANFORD RC-047 W.O.#: 1
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