SAF-RC-047 100 & 300 Area Component of the ... - Hanford Site

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8. One hundred twenty-two (122) of one hundred twenty-eight (128) matrix spike recoveries were outside acceptance criteria. A copy of the Sample Discrepancy Report (SDR) has been enclosed. 9. Sixty-three (63) of sixty-four (64) blank spike recoveries were outside acceptance criteria. A copy of the Sample Discrepancy Report (SDR) has been enclosed. 10. The method blank contained the common laboratory contaminant Bis (2-Ethylhexyl) phthalate at a level less than the CRQL. 11. Internal standard area criteria were not met for sample JllKK8 MSD. The analysis of associated matrix spike sample fulfills the reanalysis requirement. 12. Manual integrations are performed according to SOP QA-125 to produce quality data with the utmost integrity. All manual integrations are required to be technically valid and properly documented. Appropriate technical flags are defined in the Glossary ("Technical Flags For Manual Integration"). 13. LvLI is NELAP accredited by the state of Pennsylvania and holds over 20 additional state accreditations. For a complete listing of accrediting authorities and the corresponding analytes/methods, please contact your Project Manager. 14. I certify, that this sample data package is in compliance with SOW requirements, both technically and for completeness, other than the conditions detailed above. Release of the data, contained in this hard-copy data package, has been authorized, by the Laboratory Manager or a designee, as verified by the following signature. am `l Iai aniel La ratory Manager Lionville Laboratory Incorporated som\gomp\data\bna\mu-hanford\0604-904.doa 208 Welsh Pool Road • Exton, PA 19341- 1313 • (610) 280-3000 • Fax (610) 280-3041 ate V •raasuswxat4u
_WrrvurV r..duvrdtory -)ampie Initiator. Orlette Johnson Batch: ^ Date: §117106 Samples: Client: dQt Method: RCoLi7 1. Reason for SDR ncy Keport (ZwK) 111 - ' to o rr Parameter: Matrix: i] A Prep Batch: a. COC Disc repancy , Tech P rofile Error Client Request Sampler Error on C-O-C Transc ri ption Error _ Wrong Test Code _ Other b. General Discrepancy Missing Sample/Extract _ Container B roken Wrong Sample Pulled _ Label ID's Illegible Hold Time Exceeded Insufficient Sample Preserva ti on Wrong _ Received Past Hold _ Imp roper Bottle Type _ Not Amenable to Analysis X Other Note`: Verified by (Logan] or [Prep Group] (circle) ... signaturelcI ta: c. Problem (Include all relevant spe cific results; attach data if necessa ry) On 5/10106 sample storage refrigerator ID# R003 malfunctioned and was not holding the required sample storage temperature of 4°C +/- 2°C 2. Known or P robable Causes(s) B ro ken motor 3-Discussion and Proposed Action Other Desc ri ptions _ Re-log At the time of malfur ^tion R003 was used for storage of samples received _ En tire Batch for extractable organics, metals and wet chemist ry (except TOG) analyses. Following Samples: All samples we re removed from R003 to another refrigerator on 5110/06. _ Re-leach R003 was tagged out on 5/10106, repaired on 5112/06, and we have _ Re-extractcertified fiat R003 is maintaining the required sample storage temperatu re. _ Re-digest Revise EDD _ Change Test Code to _ Place On/Take Off Hold (circle) 4. Project Manager Instructions ... signaturerdate: Concur with Proposed Ac ti on ag ree with Proposed Action; See Instruc ti on nclude In Case Narrative Client Conta ^'' Date/Person t3 G`40 _ Add Cancel 5. Final Action ... s4nature/dau Other Explanation: _ VoRed rei4][leach][e ][digest][ n lysisJ clil eluded in Case Narrative _ Hard Copy COC Revised Elect ro nic COC Revised _ EDD Cor rections Completed When Final Action has been recorded, forward original to QA Specialist for distribution and filing. Route Distribu ti on of Completed SDR Route Distribution of Completed SDR X Ini ti ator_ Metals: Welsh X Lab Manager. I. Dan' _ _ Inorganic: Perrone X P roject Mgr. Ston ohnso GC/LC: Kiger _ Data Management MS: Schnsider/Beley C6t r0(C rL _ Sample P rep: Beegle/Kiger — _— Login: Per ry b, Admin: O ther. c `^r6^`' QA-105-A-0805 13 00000004
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SAF-RC-047 100 & 300 Area Component
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Lionville Laboratory, ry, Inc. PEST
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7. Two (2) of twenty (20) blank spi
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Lionville Laboratory, Inc. Extract.
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I Lionville Laborato ry Use Only b
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Washington Closure Hanford CHAIN OF
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Washin)Iton Closure Hanford CHAIN O
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Washington Closure Hanford " " CHAI
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SR-002-B 13. VOA, TOC, TOX free of
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Case Narrative Client: TNU-I IANFOR
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Lionville Laborato ry Sample Discre
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19 rNnn1r L10oFAIOF'r /^' DATA QUAL
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PCBs by GC Report Date: 07/10/06 11
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Lionville Laborato ry Use Only Cust
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Washineton Closure Hanford CHAIN OF
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Washington Closure Hanford Collect"
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Lionville Laboratory, Inc_ INORGANI
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Lionville Laboratory, Inc. INORGANI
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Page 135 and 136: RFW Batch Number: 0604L904 Semivola
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w EBERLINE VSERVICES May 30, 2006 M
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E B E R L I N E S E R V I C E S/ R
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E B ERLINE SERVICES/RICHMOND SAMPLE
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EBERLINE SERVICES/RICHMOND SAMPLE D
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SDG 7420 EBERLINE SERVICES/RICHMOND
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R604093-19 SDG 7420 Contact Melissa
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EBER L INE SER V ICES / RICHMOND SA
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EBERLINE SERVICES/RICHMON D SAMPLE
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Test TH Matrix SOLID EBERLINE SERVI
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EBER L INE SERVI CES / RI CHMOND SA
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EBERLINE SERVI CES / RI C HM O ND S
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DATE RECEIVED: 04/12/06 CLIENT ID L
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11. The continuing calibration stan
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VLY=LM=1W DATA OUALIF'IERS GLOSSARY
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Lionville Laboratory Use Only Custo
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Client: TNU-HANFORD RC-047 W.O.#: 1
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METALS METHOD GLOSSAR Y The followi
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SAF-RC-047 100 & 300 Area Component of the ... - Hanford Site

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