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Neftegaz.RU #3-17 ENG

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OFS<br />

inhibitor injection. Mutual solvents<br />

(WAW85202 (Baker Petrolite),<br />

ВР-1 (Experimental plant<br />

NefteHim and others) or nonionic<br />

or cation-active surfactant water<br />

solutions are used as liquid mud.<br />

Injection is performed with<br />

maximum flow rate of injected<br />

mutual solvent without hydraulic<br />

fracture in the following sequence:<br />

• cementing unit AC-32 (CA-320),<br />

[АЦ-32 (ЦА-320)], is connected<br />

to the well tube side for injection<br />

of the solution;<br />

• when casing valve is opened,<br />

the required volume of liquid<br />

mud is injected by means of acid<br />

pumping unit. When casing valve<br />

is opened, there will occur only<br />

the borehole cleanout without<br />

affecting the formation;<br />

• delivery of the main volume of<br />

inhibitor is performed by injection<br />

of the inhibitor (lacking volume<br />

after the mutual solvent injection<br />

for displacement of well-killing<br />

fluid from the tubing), it is injected<br />

when casing valve is opened in<br />

order to fill the remaining voidage<br />

of the tubing. Then the injection<br />

is stopped, the valve is closed<br />

and the remaining solution pills in<br />

required volume are injected into<br />

the formation. The 10% inhibitor<br />

solution is used (depending on<br />

the predicted protective effect).<br />

The injection is carried out using<br />

the same unit with maximum flow<br />

rate without hydraulic fracture;<br />

• delivery of the overflush fluid<br />

volume is carried out in order to<br />

push the inhibitor deeper into<br />

the formation. For displacement<br />

of inhibitor solution it is<br />

recommended to use 2% KCl<br />

solution, when injecting water<br />

solution of inhibitor and degassed<br />

oil, when injecting organic<br />

inhibitor solution. The injection<br />

is carried out, when the casing<br />

valve is closed, with maximum<br />

flow rate without hydraulic<br />

fracture.<br />

• response – the well is shut in<br />

for 12 – 24 hours, all works are<br />

suspended in order for corrosion<br />

inhibitor to be adsorbed on the<br />

reservoir formation;<br />

• technological tubing is pulled out<br />

and underground equipment is<br />

lowered;<br />

• well is put into run, then it is put<br />

into operation.<br />

Required quantity of mutual solvent<br />

is calculated by the following<br />

equitation:<br />

where – volume of mutual<br />

solvent for formation washing, m 3 ,<br />

– penetrated-formation<br />

thickness, m.<br />

When the bottom-hole formation<br />

zone is used as a natural dosing<br />

unit, then the empirical rule of "onethird"<br />

is working (same as when<br />

applying salt inhibitors) [2]. This<br />

rule is as follows: the third part of<br />

corrosion inhibitor injected in the<br />

formation is irrevocably adsorbed<br />

on the deposit rock (during the first<br />

few treatments); the third part of<br />

corrosion inhibitor injected in the<br />

formation is subtracted during the<br />

first few days (from 3 to 15) after<br />

start of well performance; and only<br />

the remaining third part of corrosion<br />

inhibitor injected in the formation is<br />

being subtracted for long period of<br />

time.<br />

Therefore, calculation of corrosion<br />

inhibitor weight for injection in<br />

the bottom-hole formation zone<br />

is carried out using the following<br />

formula:<br />

where – concentration of this<br />

corrosion inhibitor in produced fluid<br />

that provide the required protective<br />

effect in the system or corrosion<br />

coupon, mg/l (approximately<br />

g/t); – fluid mass flow rate,<br />

m 3 /d (approximately t/d); –<br />

estimated time of corrosion inhibitor<br />

subtraction from the formation, d;<br />

1,000 – factor for conversion of<br />

grams into kilograms; 3 – coefficient<br />

of "one-third" rule.<br />

Overflush fluid volume , m 3 , is<br />

calculated by the following formula:<br />

where – effective formation<br />

porosity, unit fraction; – internal<br />

radius of ingress of burned inhibitor<br />

solution in the formation, m. It is<br />

taken as 1.5 – 2.0 m and is specified<br />

based on the results of observation<br />

over the duration of reagent<br />

subtraction; – formation<br />

thickness, m; – tubing volume,<br />

m 3 ; – volume of production casing<br />

from pump suction or tubing intake<br />

to bottom perforations, m 3 ; = 3,14.<br />

If well-killing fluid volume is 130 m 3 ,<br />

then overflush fluid volume will be<br />

0,2 · 3,14 · 1,5 2 · 500 + 130= 840 m 3 ; in<br />

this case the well protection time will<br />

be not less than 365 days.<br />

When installing the block-pills, the<br />

squeezing process is carried out till<br />

their installation by squeezing the<br />

reagent through the tubular annulus.<br />

Technology of intermittent<br />

dosing of inhibitor into the<br />

casing annulus<br />

Technology of well treatment using<br />

the method of intermittent injection<br />

of corrosion inhibitor solution into<br />

the casing annulus is simpler<br />

compared to the technology of<br />

inhibitor solution injection into<br />

the bottom-hole formation zone<br />

described above. Partly therefore,<br />

the method of inhibitor injection<br />

into the casing annulus is more<br />

common. Corrosion inhibitor is<br />

delivered to casing annulus in form<br />

of 10% solution in oil or water.<br />

The advantage of this technology<br />

compared to the technology of<br />

inhibitor solution injection into the<br />

bottom-hole formation zone is that<br />

batch treatments can be carried out<br />

during well operation, and not only<br />

when the wells are being serviced.<br />

The disadvantage of this technology<br />

is the necessity of more frequent<br />

(in average 1 time per 30 days)<br />

treatments [3].<br />

The technology of intermittent<br />

dosing of inhibitor into the casing<br />

annulus solves the following main<br />

problems:<br />

• protection of well underground<br />

equipment against corrosion with<br />

time between repairs of more than<br />

60 – 150 days.<br />

• protection of working level casing<br />

column against corrosion;<br />

• corrosion inhibitor saving (due to<br />

the absence of required adsorption<br />

on the deposit rock).<br />

30 ~ <strong>Neftegaz</strong>.<strong>RU</strong> [3]

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