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Forgeabilité des aciers inoxydables austéno-ferritiques

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tel-00672279, version 1 - 21 Feb 2012<br />

2 Table of contents<br />

II.2.3 Strain partitioning ..............................................................................................33<br />

II.2.4 Influence of the deformation mode ....................................................................35<br />

II.2.5 Influence of the phase morphology ...................................................................36<br />

II.3 Damage during hot working .................................................................... 37<br />

II.3.1 Influence of the chemical composition ...............................................................37<br />

II.3.1.1 Influence of the major elements .............................................................................. 38<br />

II.3.1.2 Influence of the minor elements .............................................................................. 39<br />

II.3.2 As-cast microstructures .....................................................................................40<br />

II.3.3 Influence of temperature and strain rate ............................................................41<br />

II.3.4 Origin of damage...............................................................................................42<br />

II.4 Conclusions .............................................................................................. 43<br />

Chapter III. Hot cracking resistance .................................................. 45<br />

III.1 Literature review about the Essential Work of Fracture concept ......... 45<br />

III.2 Experimental procedure .......................................................................... 49<br />

III.2.1 High temperature testing ...............................................................................49<br />

III.2.2 Dimensions of the DENT specimens .............................................................50<br />

III.2.3 Characterization tools ....................................................................................51<br />

III.2.3.1 Observation of the fracture surfaces ....................................................................... 51<br />

III.2.3.2 Microstructural characterizations ............................................................................ 52<br />

III.2.3.3 Damage characterization ........................................................................................ 52<br />

III.2.3.4 Inclusion content ..................................................................................................... 53<br />

III.2.3.5 Micro-hardness ....................................................................................................... 54<br />

III.3 Comparison between as-cast D1 and D2 ............................................... 54<br />

III.3.1 Results ..........................................................................................................54<br />

III.3.1.1 EWF results ............................................................................................................. 55<br />

III.3.1.2 Fracture observations ............................................................................................. 56<br />

III.3.1.3 Damage ................................................................................................................... 58<br />

III.3.2 Discussion .....................................................................................................60<br />

III.3.2.1 Origin of the differences between D1 and D2 in the as-cast conditions ................. 60<br />

III.3.2.2 Origin of the dispersion of the results ..................................................................... 63<br />

III.3.3 Conclusions...................................................................................................65<br />

III.4 Generation of model microstructures .................................................... 65<br />

III.4.1 Materials and characterizations .....................................................................66<br />

III.4.2 γ-Widmanstätten microstructure ....................................................................66<br />

III.4.2.1 Understanding of the as-cast slab microstructure .................................................. 66<br />

III.4.2.2 Generation of a γ-Widmanstätten microstructure ................................................... 68<br />

III.4.3 γ-Equiaxed microstructure .............................................................................69<br />

III.4.4 Conclusions...................................................................................................71<br />

III.5 Comparison between D1 and D2 γ-Widmanstätten microstructures ... 72<br />

III.5.1 Results ..........................................................................................................72<br />

III.5.1.1 EWF results ............................................................................................................. 72<br />

III.5.1.2 Fracture and damage observations ........................................................................ 74<br />

III.5.2 Discussion .....................................................................................................76

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