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Forgeabilité des aciers inoxydables austéno-ferritiques

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tel-00672279, version 1 - 21 Feb 2012<br />

34 Chapter II. STATE OF THE ART<br />

An example [19] of a strain map obtained at 950°C with the modified microgrid method is given Figure<br />

II.14. The strain map showed that deformation is localized at the vicinity of the δ/γ interfaces.<br />

δ<br />

γ<br />

a) b) c)<br />

δ<br />

γ<br />

Figure II.14. Highlighting of strain partitioning via the microgrid technique in a laboratory 29.6%Cr-<br />

11.6%Ni-0.27%Mn duplex steel deformed at 950°C and 1s -1 ; a) undeformed state of a relatively<br />

small area; b) deformed configuration of the same area; c) distribution of the Green-Lagrange<br />

equivalent Von Mises strain [19].<br />

The development of the modified microgrid technique could be a good way to provide quantitative data<br />

about strain partitioning at high temperature. However, up to now, only a few results are available and<br />

only small areas were analyzed (3-4 grains). In addition, the available results were most of the time<br />

obtained on model ferrite-austenite microstructures. The lack of quantitative data concerning more<br />

realistic alloys and the influence of different parameters on the strain partitioning (temperature, phase<br />

morphology…) is clear.<br />

In order to fully understand the mechanical behaviour of duplex stainless steels, an essential piece of<br />

the puzzle is missing: the rheology of both ferrite and austenite, i.e. the stress-strain behaviour of the<br />

single phases. Duprez et al. [48] have intended to determine the rheology of each phase in a duplex<br />

steel. The authors have measured accurately the composition of the ferrite and the austenite in a<br />

commercial 2205 duplex stainless steel. Then, they have elaborated single-phase alloys with, respec-<br />

tively, the composition of the austenite and the ferrite. Finally, specimens from each alloy were de-<br />

formed under hot torsion at 1200°C. The stress strain curve revealed a large difference of yield stress<br />

and flow stress between the ferrite and the austenite, which resulted in an austenite-ferrite steady<br />

stress ratio (σ γ /σ δ )steady state ≈ 3.5 (Figure II.15). Nevertheless, this method presents a few disadvantag-<br />

es. First of all, this method is very time consuming. Indeed, as the composition and the phase ratio<br />

evolve with temperature, a different casting is required for each temperature and for each phase. In<br />

addition, such method gives the rheology of each phase at different temperatures but it does not take<br />

into account the possible interaction between both phases.<br />

δ<br />

γ

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