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Forgeabilité des aciers inoxydables austéno-ferritiques

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tel-00672279, version 1 - 21 Feb 2012<br />

54 Chapter III. HOT CRACKING RESISTANCE<br />

III.2.3.4.3 Comparison between both methods<br />

The two methods appear to be very complementary. The main advantages and disadvantages relative<br />

to each technique are summarized in Table III.1.<br />

Manual method � Location of the inclusions<br />

Automatic method<br />

Advantages Disadvantages<br />

� Automatic counting<br />

� Surface analyzed: 20mm² (950<br />

pictures at a magnification of<br />

700x)<br />

� Information about the nature and<br />

size of the particles<br />

� Manual counting<br />

� Surface analyzed: 2mm² (50 pictures<br />

at a magnification of 500x)<br />

� No information about the nature<br />

and size of the particles<br />

� No location of the inclusions<br />

� Impossible to discriminate Mo and<br />

S<br />

Table III.1. Summary of the advantages and disadvantages of both techniques used to determine the<br />

inclusion content.<br />

III.2.3.5 Micro-hardness<br />

Micro-hardness Vickers measurements were carried out on DENT specimens in both phases from the<br />

fracture surface down to the undeformed region. Then, it is possible to plot the evolution of the hard-<br />

ness as a function of the equivalent strain. These measurements provide information concerning the<br />

hardening/softening mechanisms involved in the investigated gra<strong>des</strong>.<br />

III.3 Comparison between as-cast D1 and D2<br />

III.3.1 Results<br />

D1 and D2 differ in chemical composition, especially in terms of nickel and molybdenum content<br />

(Table I.3). These two gra<strong>des</strong> were selected because of a known very different degree of hot worka-<br />

bility (section I.2.1). Comparing these two gra<strong>des</strong> should allow unravelling the key parameters involved<br />

in the hot workability of duplex stainless steels.<br />

The DENT specimens were machined in the as-cast slab of each duplex stainless steel with the liga-<br />

ment located in the columnar zone as shown schematically in Figure III.10.<br />

RD<br />

ND<br />

TD<br />

L<br />

t 0<br />

As-cast slab<br />

Figure III.10. Schematic the as-cast slab showing where the DENT specimens were machined.

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