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Forgeabilité des aciers inoxydables austéno-ferritiques

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tel-00672279, version 1 - 21 Feb 2012<br />

Chapter III. HOT CRACKING RESISTANCE 71<br />

Figure III.28 gives an estimation of the Ni-diffusion length in the ferrite for different duration of anneal-<br />

ing at 1050°C.<br />

l δ Ni, T = 1050°C (μm)<br />

100<br />

80<br />

60<br />

40<br />

20<br />

0<br />

�<br />

DNi ( 1050<br />

25.1 μm<br />

12.6 μm<br />

�14<br />

�1<br />

�C) � 4.<br />

39.<br />

10 m².<br />

s<br />

61.6 μm<br />

87.1 μm<br />

0 10 20 30 40 50<br />

t (h)<br />

Figure III.28. Evolution of the Ni-diffusion length in the ferrite as a function of time at T = 1050°C.<br />

III.4.4 Conclusions<br />

Proper control of phase transformation mechanisms has allowed the generation of a variety of micro-<br />

structures with different phase morphologies. By controlling the temperature, the duration of annealing<br />

sequences and the cooling rate, alloys with a <strong>des</strong>ired phase proportion, and <strong>des</strong>ired size and shape of<br />

the microstructure constituents have been produced. Figure III.29 summarizes, for both gra<strong>des</strong>, the<br />

resulting microstructures generated with appropriate heat treatments.<br />

Widmanstätten<br />

(W)<br />

Equiaxed<br />

(E)<br />

e γ = 22 µm<br />

D1 D2<br />

γ δ<br />

e γ = 29 µm<br />

% γ = 45 ± 3 %<br />

% γ = 50 ± 3 %<br />

a) b)<br />

γ<br />

ø γ = 50 µm<br />

δ<br />

% γ = 47 ± 3 %<br />

c) d)<br />

γ<br />

ø γ = 59 µm<br />

% γ = 52 ± 3 %<br />

δ<br />

γ δ<br />

Figure III.29. Summary of the model microstructures obtained with the appropriate heat treatments; a)<br />

D1 Widmanstätten microstructure after HTW.1; b) D2 Widmanstätten microstructure after HTW.1; c) D1<br />

equiaxed microstructure after HTE.2; d) D2 equiaxed microstructure after HTE.2.

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