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Forgeabilité des aciers inoxydables austéno-ferritiques

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tel-00672279, version 1 - 21 Feb 2012<br />

Chapter I. Introduction 15<br />

D1<br />

Edge-crack < 5 mm 10 cm<br />

a) b)<br />

D2<br />

Edge-crack > 50 mm 10 cm<br />

Figure I.4. Coils at the end of the hot rolling process showing different levels of edge-cracking depending<br />

on the grade; a) coil of the D1 grade with edge-cracks < 5mm; b) coil of the D2 grade with<br />

edge cracks > 50mm.<br />

I.2.2 Microstructures after continuous casting<br />

The schematic equilibrium phase diagram provi<strong>des</strong> qualitative indications about the origin of the as-<br />

cast microstructures, see Figure I.5. From the liquid, the alloy solidifies into δ-ferrite (Figure I.5.a).<br />

During cooling, the austenite precipitates by a nucleation and growth mechanism. Allotriomorphic aus-<br />

tenite (γ-allotriomorphic) nucleates at existing δ-ferrite grain boundaries (Figure I.5.b). Widmanstätten<br />

austenite laths nucleate from the allotriomorphic austenite with an orientation relationship with the<br />

ferrite close to that of Kurdjumov-Sachs.<br />

γ<br />

L+δ+γ<br />

c)<br />

a)<br />

b)<br />

δ+γ<br />

L<br />

δ<br />

L+δ<br />

a)<br />

δ primary<br />

b)<br />

δ primary<br />

δ primary<br />

δ primary<br />

γ 1-allotriomorphic<br />

c)<br />

δ primary<br />

δ primary<br />

γ 1-allotriomorphic<br />

γ 2-Widmanstätten<br />

Figure I.5. Origin of the as-cast microstructure in duplex stainless steel; a) at high temperature<br />

duplex stainless steel is entirely ferritic; during cooling, the austenite precipitates b) at existing ferrite<br />

grain boundaries and c) inside the ferrite matrix with a lath morphology; thermal history explains<br />

the as-cast microstructure.

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