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Barbieri Thesis - BioMedical Materials program (BMM)

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Counts on total (%)<br />

1<br />

0.9<br />

0.8<br />

0.7<br />

0.6<br />

0.5<br />

0.4<br />

0.3<br />

0.2<br />

0.1<br />

Chapter 5 – Alkali surface treatment effects<br />

M0<br />

M1<br />

M2<br />

0<br />

-550 -50<br />

Heights (nm)<br />

450<br />

Figure 4. The distribution of recorded heights as compared to the zero–plane shows that stronger alkali<br />

surface treatment leads to larger variability in the surface heights.<br />

Table 5. Surface roughness parameters as measured with AFM. Statistical comparison is expressed in<br />

terms of p–values and is reported in the text.<br />

Ra Rq Rz<br />

[nm] [nm] [nm]<br />

M0 27.1±3.8 33.7±5.0 258.3±47.9<br />

M1 58.2±4.1 72.3±4.8 541.5±89.3<br />

M2 105.7±6.3 130.6±7.8 997.3±138.3<br />

Table 6. Calcium and phosphate cumulative ion concentration, mass loss and fluid uptake after 12<br />

weeks in vitro degradation in SPS.<br />

Calcium release Phosphate release Mass loss Fluid uptake<br />

[M]<br />

[M]<br />

[%] [%]<br />

M0 492±75 157±2 10.1±0.2 2.4±0.2<br />

M1 710±120 174±11 10.8±0.1 7.5±0.2<br />

M2<br />

p, ANOVA<br />

645±54 175±3 10.6±0.1 7.3±0.3<br />

M0–M1

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