CHEM02200704003 Nilamadhab Pandhy - Homi Bhabha National ...

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Chapter 6 (55.18°) respectively, which are the characteristics peak of anatase phase. The surface morphological analysis of the TiO 2 coated 304L SS using AFM is shown in Fig. 6.8a-d. Figure. 6.8a represents the morphology of TiO 2 coated 304L SS. The morphology showed well organized, evenly spaced, and compact arrangement of particles covering the surface. The histogram for size distribution of the particles as a function of frequency of formation is shown in Fig. 6.8b. The particle size ranges from, 1.5×10 -1 µm 2 to 1.12 µm 2 . However, because of agglomeration the size of the particle increases up to 2.5 µm 2 . The exact location, and morphology of the pores on the coated surface is shown in Fig. 6.8c. The size of the pores ranges from, 3×10 -3 µm 2 to 450 ×10 -3 µm 2 (Fig. 6.8d). The root mean square roughness (R q ) on the surface was 10 nm. Fig. 6.8a-d: (a) Morphology of TiO 2 coated 304L SS, (b) histogram for the particle size distribution, (c) morphology of the pores and (d) histogram for the size distribution of the pores.
Chapter 6 6.2.2.2 Open circuit potential vs. time measurement The OCP of uncoated, and TiO 2 coated 304L SS specimens in both 1 M and 8 M nitric acid medium are shown in Fig. 6.9a-b. Fig. 6.9a: OCP vs. time measurement for TiO 2 coated 304L SS in 1 M HNO 3 [22]. Fig. 6.9b: OCP vs. time measurement for TiO 2 coated 304L SS in 8 M HNO 3 [22].
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2.3 Effect of alloying elements on
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4 C H A P T E R 4 73 # $%&' 4.1 In
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6.2.3.2 Open circuit potential vs.
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eprocessing can be recovered, and c
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The ex-situ study of passive film w
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Fig.3.10: Schematic of electrical e
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Fig.6.11: Polarization study of unc
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AISI: American Institute of Steel I
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Chapter 1 C H A P T E R 1 Spent Nuc
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Chapter 1 1.3 Challenges in spent n
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Chapter 1 corrosion resistance. The
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Chapter 1 choice of zirconium is du
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C H A P T E R2
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Chapter 2 temperature, (c) higher i
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Chapter 2 Chromium in excess of 12
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Chapter 2 2. 3 Effect of alloying e
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Chapter 2 The twins are identified
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Chapter 2 and at temperature around
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Chapter 2 of adsorption of oxygen o
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Chapter 2 transpassive dissolution
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Chapter 2 healing chromium oxide fi
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Chapter 2 their segregation to the
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Chapter 2 is intimately related to
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Chapter 2 in nature because the dis
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C H A P T E R3
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Chapter 3 3.1.1.2 Specimen preparat
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Chapter 3 ionized. However, differe
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Chapter 3 various industrial applic
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Chapter 3 In the present investigat
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Chapter 3 3.1.3.2 Atomic force micr
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Chapter 3 present on the surface fo
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Chapter 3 necessary condition is th
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Chapter 3 Y m is the sputter yield.
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Chapter 3 Fig. 3.7: Schematic of X-
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Chapter 3 rate of 10Å/min using 5
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Chapter 3 different doses of nitrog
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Chapter 3 The modulus of electroche
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Chapter 3 equivalent circuit as sho
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Chapter 3 reference electrode with
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Chapter 3 for understanding the pas
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C H A P T E R4
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Chapter 4 encountered by all materi
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Chapter 4 pitting, and intergranula
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Chapter 4 The ridged structure, and
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Chapter 4 nitric acid is that the b
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Chapter 4 Potential (V) Vs Ag/AgCl
Page 100 and 101: Chapter 4 4.2.3 In-situ electrochem
Page 102 and 103: Chapter 4 The surface morphologies
Page 104 and 105: Chapter 4 a b c d Opening up of gra
Page 106 and 107: Chapter 4 Intensity (Arbitrary unit
Page 108 and 109: Chapter 4 The chromium, and oxygen
Page 110 and 111: Chapter 4 Intensity (Arbitrary unit
Page 112 and 113: C H A P T E R5
Page 114 and 115: Chapter 5 elements, and often impar
Page 116 and 117: Chapter 5 5.2 Results and discussi
Page 118 and 119: Chapter 5 Presence of oxygen is due
Page 120 and 121: Chapter 5 was an increase in marten
Page 122 and 123: Chapter 5 formation of Cr 2 N was a
Page 124 and 125: Chapter 5 electrochemical environme
Page 126 and 127: Chapter 5 N + Dose E corr (mV vs. A
Page 128 and 129: Chapter 5 layer capacitance (C dl )
Page 130 and 131: Chapter 5 correlation between surfa
Page 132 and 133: Chapter 5 boundary dissolution was
Page 134 and 135: Chapter 6 C H A P T E R 6
Page 136 and 137: Chapter 6 193]. As a single phase c
Page 138 and 139: Chapter 6 particles range from 8×1
Page 140 and 141: Chapter 6 Results revealed that in
Page 142 and 143: Chapter 6 The change over from capa
Page 144 and 145: Chapter 6 The impedance parameters
Page 146 and 147: Chapter 6 Conc. Substrate condition
Page 148 and 149: Chapter 6 6.6a-d. The uncoated spec
Page 152 and 153: Chapter 6 OCP shifted in noble dire
Page 154 and 155: Chapter 6 The high phase angle over
Page 156 and 157: Chapter 6 Fig. 6.10d: Log f vs. Log
Page 158 and 159: Chapter 6 Fig. 6.11b: Polarization
Page 160 and 161: Chapter 6 Covalent aspect of lattic
Page 162 and 163: Chapter 6 As compared to uncoated s
Page 164 and 165: Chapter 6 6.2.3.2 Open circuit pote
Page 166 and 167: Chapter 6 Similarly, the plots for
Page 168 and 169: Chapter 6 for the duplex coating, a
Page 170 and 171: Chapter 6 Fig.6.16b: Polarization s
Page 172 and 173: Chapter 6 6.2.3.5 Morphological exa
Page 174 and 175: Chapter 7 C H A P T E R 7 The cha
Page 176 and 177: Chapter 7 1. Surface morphology exa
Page 178 and 179: Chapter 7 6 Duplex Ti-TiO 2 coated
Page 180 and 181: Chapter 7 EC-SPM study on effect
Page 183 and 184: [1] Baldev Raj, U. Kamachi Mudali,
Page 185 and 186: [37] G. Okamoto, T. Shibata, Corros
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Page 196 and 197: [19] H. H. Uhlig, Corros Sci, 19 (1
Page 198 and 199: [57] J. F. Ziegler, J. P. Biersack,
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[97] I. Betova, M. Bojinov, V. Kara
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[139] V. Ashworth, R. P. M. Procter
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[176] G. Frankel, G. Grundmeier, H.
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List of publications 1. Referred
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CHEM02200704003 Nilamadhab Pandhy - Homi Bhabha National ...

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