rok 2007 - Fakulta chemickej a potravinÃ¡rskej technolÃ³gie

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Organic Chemistry Laboratory 0/0/4 Lásiková, Wiesenganger, Šafař, Štibrányi 4. semester (Bc) (Pt) Organic Chemistry 1/1/0 Gracza, Stankovský, Považanec Organic Chemistry Laboratory 0/0/4 Lásiková, Wiesenganger, Žáková, Petro 5. semester (Bc) Chemical Information 1/1/0 Zálupský, 6. semester (Bc) Chemical Specialities 2/2/0 Mravec, Štibrányi Semestral Project 0/0/4 Fišera, Šafář, Lásiková, Gracza, Szolcsányi, Milata, Végh 1. semester (MSc) Organometallic Compounds 1/1/0 Gracza Mechanisms of Organic Reactions I 3/1/0 Fišera Bioorganic Chemistry 2/0/0 Berkeš Laboratory Project I 0/0/10 Milata, Szolcsányi, Gracza, Lásiková, Šafář 1. semester (MSc) Organic Chemistry III 1/1/0 Považanec 2. semester (MSc) Organic Synthesis 2/1/0 Marchalín Asymmetric Synthesis 2/1/0 Gracza Stereochemistry 0/2/0 Štibrányi Spectroscopic Methods in the Control of Technology 2/2/0 Milata, Segľa 2. semester (MSc) Laboratory Project II 0/0/6 Berkeš, Koreňová Training at Industrial Production Floor 15 d Berkeš, Koreňová 3. semester (MSc) Mechanisms of Organic Reactions II 1/1/0 Marchalín Applied Organic Synthesis 1/1/0 Považanec Physical Organic Chemistry I 0/2/0 Milata Physical Organic Chemistry II 2/0/0 Kolarovič Chemistry of Natural Substances and Drugs 2/0/0 Berkeš Chemical Information Systems 2/0/0 Zálupský 3. semester (MSc) Laboratory Project 0/0/10 Berkeš, Koreňová 4. semester (MSc) Diploma Seminar Považanec Diploma Thesis Project Milata, Szolcsányi, Gracza, Lásiková, Považanec, Fišera, Marchalín C. Doctoral Study: 1. semester (PhD) Advanced Organic Chemistry 2/0/0 Gracza 1. semester (PhD) Advanced Stereochemistry 2/0/0 Fišera 2. semester (PhD) Structure Reactivity Relationship 2/0/0 Marchalín 3. semester (PhD) Advanced Organic Chemistry 2/0/0 Milata 3. semester (PhD) Chemistry of Heterocyclic Compounds 2/0/0 Végh IV. CURRENT RESEARCH PROJECTS VEGA project No 1/3549/2006 Asymmetric and Stereoselective Reactions. Dipolar Cycloadditions, Sm(II)-Induced Additions, Cyclizations and Oxycarbonylations in the Total Syntheses of Natural Products and Its Analogues (Lubor Fišera) The Sm(II) induced diastereoselective reductive coupling of sugar derived nitrones with ethyl acrylate will provide access to a variety of functionalized amino acids directly, or to amino acids as constituents of small peptides. The stereoselective synthesis of optically active polysubstituted pyrrolidin-2-ones and piperidine-2-ones from chiral amino acids which are promising precursors for the synthesis of several pyrrolizidine, pyrrolidine, indolizidine and piperidine alkaloids. The synthesis of non-proteinogenic amino acids derived nitrones, isoxazolidinyl nucleosides, spironucleosides and azanucleosides. The study of the effect of Lewis acids to influence diastereoselectivity of nitrone cycloaddition reactions. Asymmetric palladium(II)-catalyzed oxy-/aminocarbonylation and oxa-/aminobicyclization of unsaturated polyols and aminopolyols. Catalyst design using the calculation of the model for transition state. Correlation of enantioselectivity with calculated models of the transition states for prediction of the reaction stereoselectivity and stereochemistry of the products. The application of these reactions as the asymmetric key-steps in the total syntheses of natural compounds. Project duration: from 01.01.2006 to 31.12.2008 166
APVV project LPP-0238-06 Asymmetric synthesis based on a template for crystallizationinduced asymmetric transformation (CIAT) (Lubor Fišera) Detailed information on application of acylacrylic subunit as a template for crystallization-induced asymmetric transformation (CIAT). Marking out the boundaiy for effective asymmetric synthesis by this method. Acquisition of information essential for next shift from acylacrylic template towards crystallization auxiliaries, making accessible future synthetic options. Simplification of existing synthetic procedures leading to chiral amino and hydroxyamino acids, respectively. 1.3-DCA of prepared alkenes with subsequent transformation to corresponding aminohydroxy acids and derivatives. Utilization of prepared chiral hydroxyamino acids in synthesis of selected target compounds containing piperidine or pyrrolidine skeleton. Project duration: from 01.12.2006 to 30.11.2009 APVV project No 20-000305 New strategies for stereoselective and asymmetric syntheses of biologically active natural compounds (Tibor Gracza) Development of the new stereoselective and asymmetric strategies for funcionalization of C=C double bond of alkenes with introduction of O- and/or N-functions. Asymmetric Pd(II)-catalyzed oxy-/aminocarbonylations of unsaturated polyols and amino polyols. Catalyst design using X-ray and electron density analysis and QM method. Theoretical calculations of TS-models for prediction of stereochemical outcome (ee%) of the reactions. Their application in the syntheses of natural compounds and biologically interesting compounds. Stereoselective synthesis of optically active polysubstituted pyrrolidin-2-ones and piperidin-2-ones from chiral g-aminoacids - precursors for preparation of polyhydroxylated pyrrolidines, piperidines, pyrrolizidines and indolizines. The synthesis of non-proteinogenic amino acids derived nitrones, isoxazolidinyl nucleosides, spironucleosides and azanucleosides. The study of the effect of Lewis acids to influence diastereoselectivity of nitrone cycloaddition reactions. Project duration: from 01.03.2006 to 28.02.2009 VEGA project No 1/2456/05 Stereoselective Syntheses of Chiral 1,4-Dihydropyridines and Analogs of Indolizine type Alkaloids (Štefan Marchalín) The principal goal of the project is to investigate posible utilization of 2-formyl- dihydropyridines in the synthesis of novel chiral nonracemic 2-substituted dihydropyridines, bi- and tricyclic heterocycles respectively, containing a 1,4-dihydropyridine ring. Preparation and characterrization of coordination compounds of both transition and non transition metals carrying 1,4-dihydropyridine based ligands, examination of their composition, structure, and investigation of their catalytic activity. The project aims at preparation of carefully designed substituted indolizines and indolizidines - compounds with possible bioactivity. Practical application of regio-, chemo- and stereoselective reactions making use of novel features of organic synthesis. Elaboration of novel, simple, and generally applicable stereocontrolled syntheses of pure analogs of indolizine type alkaloids, utilizing chiral synthons based on hetero[f]indolizidinediones. Project duration: from 01. 01. 2005 to 31.12.<strong>2007</strong> VEGA 1/4453/07 Syntheses directed towards novel π-conjugated heterocyclic compounds such that show opto-electronic properties, specific bioactivity, and apoptosis (Daniel Végh). Design of syntheses, supported by theoretical studies, of novel heterocyclic compounds. Research into novel synthetic procedures, reactions and catalysts, structure elucidation of prepared target compounds and reaction mechanisms involved. Synthesis of derivatives of novel π-conjugated heterocycles of the thiophene, pyrrole, furan imidazole, pyrazine, fluorene and anthrone derivatives series as well as of their bioactivity. Study of controlled dimerization and trimerization of the synthesized π-conjugated heterocyclic compounds for preparation of molecular and supramolecular functional units and nanostructures. Synthesis of thiophene oligomers in the channels of synthetic zeolite and at the surface of inorganic conductor TiO2 aiming at preparation of anisotropic photoactive system organic compounds-inorganic substrate. Characterization of the prepared heterogeneous composite as to its structure, spectral and magnetic properties. Modeling of novel supramolecular units and potential π-conjugated antenna systems pro molecular recognition and self-assembly by utilizing theoretical calculations and combination of various building blocks. Synthesis and utilization of perfluoroaromatics for molecular recognition. Synthesis and modelling of structure of compounds active against cancer and launching apoptosis. Project duration: from 01. 01. <strong>2007</strong> to 31. 12. 2009 167
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ANNUAL REPORT 2007 Faculty of Chemi
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DEPARTMENT OF ANALYTICAL CHEMISTRY
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IV. CURRENT RESEARCH PROJECTS A. VE
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I. APVV Project -20-035205: Develop
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B. International Cooperation Instit
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Zapadlo, M. Palacky University, Olo
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Lehotay, J. Pharmaceutical Faculty
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Bratislava, Slovak Republic : 27th
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In: Acta Crystallographica Section
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[30] Hroboňová, K., Lehotay, J.,
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Slovak Republic, 2007, A10. ISBN 98
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prístupov. In: Syntéza a analýza
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DEPARTMENT OF NMR SPECTROSCOPY AND
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Duslo Šaľa ZoD Ing. J.Uhlár, PhD
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INSTITUTE OF INORGANIC CHEMISTRY, T
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1. semester (MSc) Laboratory Practi
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APVT Project APVT-20-005504 Synthes
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F. Visits of Staff Members and Post
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[2] Bienko, A., Klak, J., Mrozinski
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konference Vodárenská biologie 20
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IV. CURRENT RESEARCH PROJECTS VEGA
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J. Híveš Slovak Chemical Society
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In 59. Zjazd chemických spoločnos
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Technology of ceramics 2/0/0 Smrčk
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F. Visits of Staff Members and Post
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978-80-8073-806-8 - Hutnícka fakul
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DEPARTMENT OF BIOCHEMISTRY AND MICR
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IV. CURRENT RESEARCH PROJECTS APVT
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Laubertová, Inhibition of Human Le
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[15] Kaliňák, M., Lakatoš, B., P
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DEPARTMENT OF NUTRITION AND FOOD AS
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value of produced foods. This is cl
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E. Hybenová Member of Committee of
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Šramková Z. Implementation of nut
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Zborník príspevkov. - ISBN 978-80
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DEPARTMENT OF BIOCHEMICAL TECHNOLOG
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IV. CURRENT RESEARCH PROJECTS A. VE
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Project ojectives: To find optimal
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Czech Academic of Sciences Microbio
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Nádaský P. Mendel University of A
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VIII. PUBLICATIONS Chapter or pages
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[19]. Dercová, K. Čičmanová, J.
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[61]. Šulák, M., Šmogrovičová,
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Terminal Work 0/0/9 All members of
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VI. COOPERATION A. Cooperation in S
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Dandár,A. Slovak Soc. Of Agricultu
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Kollárová, L. Oxidative Stability
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slowackiej. In Zywność a choroby
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mäsových výrobkov. . In Zborník
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DEPARTMENT OF PHYSICAL CHEMISTRY He
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industry and nuclear power plants.
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IFW Dresden, Germany scientific P.
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VII. THESES AND DISSERTATIONS A. Gr
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B. PhD Study: Biophysics I 2/0/0 Va
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VII. THESES AND DISSERTATIONS B. Gr
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DEPARTMENT OF MANAGEMENT Head of De
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E. Visitors from abroad Name Organi
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Baran, D. Olejník, P. Kajanová J.
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[14] KAJANOVÁ, J.: Moderné príst
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DEPARTMENT OF LANGUAGES Head of Dep
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Chapter or pages in book [1] Lauren
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