rok 2007 - Fakulta chemickej a potravinÃ¡rskej technolÃ³gie

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VEGA project No 1/2469/05 Study of stereoselective transformations of non proteinogenic oxoaminocarboxylic acids (Dušan Berkeš) Synthesis of enantiomerically pure, conformationally restricted derivatives of homophenylalanine and of its heteroanalogs by crystallization induced asymmetric transformation (CIAT) coupled with the aza-Michael addition and electrophilic lactonization. Study of simultaneous CIAT taking place at two stereogenic centers. Synthesis and stereoselective transformations of bicyclic tetramic acid derivatives. Utilization of such asymmetric transformation in the synthesis of natural polysubstituted amino acids and their derivatives. Preparation of 5 aryl¬substituted 3 amino-2-hydroxytetrahydrofurans and study of their conversion to optically pure substituted C- aryl amino¬furanosides. Project duration: from 01.01.2005 to 31.12.2007 VEGA project No 1/248/05 Polyazaheterocycles and their oxygen analogues. Ecologically more suitable syntheses, supramolecular structure, biological – physical properties (Viktor Milata) The project aims at preparation of novel aromatic polyazaheterocycles on the bases of triazines, dihydropyridines, pyrimidines, quinolines and quinazolines, having additional fused aromatic or saturated ring. In the early stages of the project we shall concentrate on preparation of precursors to the above heterocycles by modern, more ecological methods. Next the precursors will be used in cyclization and cyclocondensation reaction leading to target compounds. Prepared heterocycles will be modified to enhance their hydrophilicity and hence bioactivity by attaching a sugar or other hydrophilic moiety. Our attention will concentrate on physicochemical and spectral characteristics, combined with xray analysis, supramolecular chemistry and quantum chemical calculations. Project duration: from 01.01.2005 to 31.12.2007 APVV Project No. 20-007304 Synthesis and properties of the pharmacologically potentially active nitrogen heterocycles (Viktor Milata) Study and optimisation of the new synthetic methods for preparation of analogues of natural condensed aromatic polyazaheterocyclic compounds with fused aromatic or saturated ring containing O, S, Se or N atoms. Preparation of precursors of cited heterocycles and their nitro- and aminoderivatives, imidoylchlorides, imidoyl and amidinoylisothiocyanates. Exploitation of new precursors in cyclisation and cyclocondesation reactions for preparation of target compounds. Derivatisation of newly prepared heterocyclic compounds by introduction of carbohydrate or other hydrophylic part aiming to higher solubility of prepared compounds allowing their more effective biological application. Study of physico-chemical properties and spectral characteristics of final derivatives in relation to their X-ray structural analysis, supramolecular chemistry using quantum-chemical calculations. Project duration: from 01.01.2005 to 31.12.2007 APVT Project No. 20-000904 Asymmetric Pd(II)-catalysed reactions as a methodology for the preparation of chiral bulding blocks for the synthesis of biologically active natural compounds (Peter Szolcsányi) The main aim of the project is to develop a new and efficient methodology of asymmetric palladium-catalysed intramolecular and intermolecular aminocarbonylations and halocyclisations for the enantioselective preparation of optically pure building blocks. These valuable intermediates will serve as suitable chiral precursors for targeted total syntheses of biologically active natural compounds and/or their analogues with their potential use in human medicine. The sub-objectives of the project involve the development of a simple and rapid preparation of necessary aminoalkenitols as starting substrates in multi-gram quantities and required purity, as well as an effective synthesis of enantiomerically pure chiral Pd-catalysts essential for key asymmetric transformations. Project duration: from 01.01.2005 to 31.12.2007 VI. COOPERATION A. Cooperation in Slovakia Institution Type of cooperation Responsible person Duration 168
Synkola, Bratislava Duslo, Šaľa Slovak Academy of Sciences, Bratislava Slovak Academy of Sciences, Bratislava Tau-Chem, Bratislava Institute of Drugs Research, Modra Tatra Trade, Prievidza Georganics, Bratislava CMS, Bratislava Zentiva a.s., Hlohovec Seminars and conferences The synthesis of heterocyclic compounds. The synthesis of heterocyclic compounds. The synthesis of heterocyclic compounds. The synthesis of heterocyclic compounds. The synthesis of heterocyclic compounds. The synthesis of heterocyclic compounds. The synthesis of heterocyclic compounds. The synthesis of heterocyclic compounds. Research and teaching Karvaš Milan, director, Mlynská dolina, 842 15 Bratislava 4 Lehocký Peter, director, Duslo, a. s. 927 03 Šaľa Tvaroška Igor, director, Dubravská cesta 9, 841 04 Bratislava 4 Šoltés Ladislav, UEF, Dubravská cesta 9, 841 04 Bratislava 4 Žvak Vladimír, director, Nobelova 34, 836 05 Bratislava 3 Šmahovský Vendelín, director, Horná 36, 900 01 Modra Klínovský Ján, director, Matice slovenskej 10, 971 01 Prievidza Ďuriš Juraj, director, Koreničova 1, 811 03 Bratislava 1 Toman Jaromír, director, Nobelova 34, 836 03 Bratislava 3 Chylik Jaroslav Dr., API prod. manager, Nitrianska cesta 100, 920 27 Hlohovec 01.01.1992- 01.01.1990- 01.01.1970 01. 01.1997- 01.01.1996 01.01.1980- 01.01.2000- 01.01.2000- 01.01.2000- 01.07.2003- B. International Cooperation Institution Type of cooperation Responsible person Duration Inst. für Angewandte Synthese Chemie TU Vienna, Austria Inst. für Organische Chemie Univ. Stuttgart, Germany Max Plank Institute, Stuttgart, Germany Inst. für Organische Chemie Univ. Berlin, Germany Inst. de Chimie Moleculaire d´Orsay, France Inst. de Chimie Moleculaire d´Orsay, France Institute de Chimie Moleculaire, Orsay, Univ. Paris-Sud, France URCOM, Univ. Le Havre, France Inst. für Festkörperphysik der Univ. Vienna, Austria The synthesis of heterocyclic compounds Stereoselective dipolar cycloaddition and oxycarbonylation reactions The synthesis of heterocyclic compounds for nanotubes Stereoselective reactions of chiral nitrones Resau formation recherche Resau formation recherche NMR study of chiral compounds and cooperation in exchange of students The synthesis of condensed heterocyclic compounds New materials for microelectronics Fröhlich Hannes, dean, professor, Getreide Markt 9, A-1060 Vienna, Austria Jäger Volker, professor, Pfaffenwaldring 55, D-70569 Stuttgart, Germany Roth Siegmar, Dr., Helsenbergerstr. 1, D-70569 Stuttgart, Germany Reissig Hans-Ulrich, professor, Takustr. 3, D-14195 Berlin, Germany Basch E. H., professor, IUT d'Orsay Université de Paris-Sud (XI) Département Chimie Plateau du Moulon 91400 ORSAY, France Fiaud, J. C., professor, IUT d'Orsay Université de Paris-Sud (XI) Département Chimie Plateau du Moulon 91400 ORSAY, France Loupy, A. , professor, Institut of Molecular Chemistry, ICMO, University Paris – South, Orsay, France DECROIX B., DAICH A., professors Laboratoire de Chimie URCOM, EA 3221 Faculté des Sciences et Techniques Université du Havre 25, r Kauffmann H. F. professor, University of Vienna, Intitut fur Physikalische chemie, Währingerstrasse 42, Wien, Austria. 01. 01. 1991- 01. 01. 1989- 01.01.2002- 01. 01. 2002- 01.01.1976- 01.05. 2007- 01.01.2000- 01.01.1990 01.010.2001- 169
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ANNUAL REPORT 2007 Faculty of Chemi
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DEPARTMENT OF ANALYTICAL CHEMISTRY
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IV. CURRENT RESEARCH PROJECTS A. VE
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I. APVV Project -20-035205: Develop
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B. International Cooperation Instit
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Zapadlo, M. Palacky University, Olo
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Lehotay, J. Pharmaceutical Faculty
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Bratislava, Slovak Republic : 27th
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In: Acta Crystallographica Section
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[30] Hroboňová, K., Lehotay, J.,
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Slovak Republic, 2007, A10. ISBN 98
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prístupov. In: Syntéza a analýza
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DEPARTMENT OF NMR SPECTROSCOPY AND
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Duslo Šaľa ZoD Ing. J.Uhlár, PhD
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INSTITUTE OF INORGANIC CHEMISTRY, T
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1. semester (MSc) Laboratory Practi
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APVT Project APVT-20-005504 Synthes
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F. Visits of Staff Members and Post
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[2] Bienko, A., Klak, J., Mrozinski
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konference Vodárenská biologie 20
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IV. CURRENT RESEARCH PROJECTS VEGA
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J. Híveš Slovak Chemical Society
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In 59. Zjazd chemických spoločnos
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Technology of ceramics 2/0/0 Smrčk
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F. Visits of Staff Members and Post
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978-80-8073-806-8 - Hutnícka fakul
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DEPARTMENT OF BIOCHEMISTRY AND MICR
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IV. CURRENT RESEARCH PROJECTS APVT
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Laubertová, Inhibition of Human Le
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[15] Kaliňák, M., Lakatoš, B., P
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value of produced foods. This is cl
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E. Hybenová Member of Committee of
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Šramková Z. Implementation of nut
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Zborník príspevkov. - ISBN 978-80
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DEPARTMENT OF BIOCHEMICAL TECHNOLOG
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IV. CURRENT RESEARCH PROJECTS A. VE
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Project ojectives: To find optimal
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Czech Academic of Sciences Microbio
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Nádaský P. Mendel University of A
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VIII. PUBLICATIONS Chapter or pages
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[19]. Dercová, K. Čičmanová, J.
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[61]. Šulák, M., Šmogrovičová,
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Terminal Work 0/0/9 All members of
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VI. COOPERATION A. Cooperation in S
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Dandár,A. Slovak Soc. Of Agricultu
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Kollárová, L. Oxidative Stability
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slowackiej. In Zywność a choroby
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mäsových výrobkov. . In Zborník
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DEPARTMENT OF PHYSICAL CHEMISTRY He
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industry and nuclear power plants.
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IFW Dresden, Germany scientific P.
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VII. THESES AND DISSERTATIONS A. Gr
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B. PhD Study: Biophysics I 2/0/0 Va
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VII. THESES AND DISSERTATIONS B. Gr
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Seminar. pp. 26-27, 2007. [17] Luke
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E. Visitors from abroad Name Organi
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Baran, D. Olejník, P. Kajanová J.
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[14] KAJANOVÁ, J.: Moderné príst
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Chapter or pages in book [1] Lauren
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