Analysis of the extended defects in 3C-SiC.pdf - Nelson Mandela ...
Analysis of the extended defects in 3C-SiC.pdf - Nelson Mandela ...
Analysis of the extended defects in 3C-SiC.pdf - Nelson Mandela ...
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4.2.5. Two-Beam Scatter<strong>in</strong>g Matrix 44<br />
4.2.6. Crystal Defects and Displacement Fields 45<br />
4.3. Image Contrast for Selected Defects 47<br />
4.3.1. L<strong>in</strong>e Defects 47<br />
4.3.2. Stack<strong>in</strong>g Faults 47<br />
4.3.3. Fr<strong>in</strong>ge Contrast Observed from Tw<strong>in</strong>n<strong>in</strong>g 51<br />
Chapter 5: LITERATURE REVIEW OF <strong>SiC</strong> 53<br />
5.1. Introduction 53<br />
5.2. CVD Growth <strong>of</strong> β-<strong>SiC</strong> on Si 53<br />
5.3. Crystal Defects <strong>in</strong> β-<strong>SiC</strong> 56<br />
5.3.1. Introduction 56<br />
5.3.2. Accommodation <strong>of</strong> Misfit and Interfacial Tw<strong>in</strong>n<strong>in</strong>g 57<br />
5.3.3. Mechanisms for <strong>the</strong> Formation <strong>of</strong> Stack<strong>in</strong>g Faults 58<br />
5.3.4. Stack<strong>in</strong>g Fault Energy <strong>in</strong> β-<strong>SiC</strong> 61<br />
5.4. Ion Implantation and Radiation Damage <strong>in</strong> β-<strong>SiC</strong> 61<br />
Chapter 6: EXPERIMENTAL DETAILS 64<br />
6.1. Introduction 64<br />
6.2. CVD Growth <strong>of</strong> β-<strong>SiC</strong> 64<br />
6.3. Proton Implantation <strong>in</strong> β-<strong>SiC</strong> 64<br />
6.3.1. Ion Ranges and Defect Production 65<br />
6.4. Anneal<strong>in</strong>g Procedure 67<br />
6.5. Sample Preparation 68<br />
Chapter 7: RESULTS AND DISCUSSION 69<br />
7.1. Introduction 69<br />
7.2. Extended Defects <strong>in</strong> β-<strong>SiC</strong> Grown by CVD on (001) Si 69<br />
7.2.1. Crystal Structure and <strong>the</strong> <strong>SiC</strong>/Si Interface 70<br />
7.2.2. Stack<strong>in</strong>g Faults and Partial Dislocations 74<br />
7.2.3. Tw<strong>in</strong>n<strong>in</strong>g 82<br />
7.3. Hydrogen Implanted β-<strong>SiC</strong> 83<br />
7.3.1. Unannealed 83<br />
7.3.2. Annealed at 1300°C 84<br />
7.3.3. Annealed at 1600°C 85<br />
7.4. Reassessment <strong>of</strong> Unimplanted Sample 94<br />
7.4.1. Overview <strong>of</strong> Investigation 94<br />
7.4.2. Results 95<br />
Chapter 8: CONCLUSION 96<br />
8.1. Introduction 96<br />
8.2. TEM <strong>Analysis</strong> <strong>of</strong> β-<strong>SiC</strong> Grown on (001) Si by CVD 96<br />
8.3. TEM <strong>Analysis</strong> <strong>of</strong> β-<strong>SiC</strong> Proton Bombarded and Annealed 97<br />
β-<strong>SiC</strong><br />
References 99