Kinetic Analysis and Characterization of Epoxy Resins ... - FedOA

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Conclusions and Outlook 164 a direct comparison between DSC and MW curing reactions can be carried out. Moreover a more complete investigation of the final properties of the epoxy system cured in both the way can be accomplished through the dielectric characterization. 164
Appendix A A Brief History of Microwave Oven Like many great inventions in history, the microwave oven was also a product of past technology. It was during a radar-related research project around 1946 that Dr. Percy Spencer, a self-taught engineer with the Raytheon Corporation, noticed something very unusual. He was testing a new vacuum tube called magnetron, when he discovered that the chocolate bar in his pocket had melted. This interested Dr. Spencer, so he tried another experiment. This time he placed some popcorn kernels near the tube and watched as popcorn sputtered, cracked and popped all over his laboratory. Another experiment, that he conducted, involved an egg, which he placed near the magnetron tube. That time, he asked his colleague to accompany him so that they can both see the phenomena. Because of the elevated pressure, the egg began to tremor. The temperature inside the egg got so high, that the egg exploded. Hot yolk splattered all over his 165
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UNIVERSITA’ DEGLI STUDI DI NAPOLI
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3 I thank all the lecturers of PhD
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5 Microwaves are electromagnetic ra
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CONTENTS 7 1.8.1 DielectricProperti
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CONTENTS 9 4 Conclusions and Outloo
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LIST OF TABLES 11 3.2 Average value
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List of Figures 1.1 Diglycidylether
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LIST OF FIGURES 15 2.23 Onset tempe
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LIST OF FIGURES 17 3.38 Comparison
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Introduction 19 cannot be melted an
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Introduction 21 • bismaleimides;
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Introduction 23 cold solders, casti
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Introduction 25 Average Properties
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Introduction 27 In Figure 1.4 n can
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Introduction 29 ducts and it genera
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Introduction 31 tween current-carry
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Introduction 33 that describe the p
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Introduction 35 1.3.5 Lorentz Force
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Introduction 37 Figure 1.11: Electr
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Introduction 39 Even microwaves can
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Introduction 41 production requirem
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Introduction 43 fect of the electro
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Introduction 45 following different
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Introduction 47 Debye equations bas
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Introduction 49 Although these mode
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Introduction 51 materials that have
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Chapter 2 Experimental In this chap
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Experimental 55 Characteristic Note
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Experimental 57 If the oven is used
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Experimental 59 In monomodal applic
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Experimental 61 Figure 2.5: Right s
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Experimental 63 Figure 2.8: Front v
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Experimental 65 regardless of the a
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Experimental 67 • The number of t
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Experimental 69 Figure 2.11: Surfac
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Experimental 71 Figure 2.12: Repeti
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Experimental 73 From the Figure 2.1
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Experimental 75 in the centre of th
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Experimental 77 not read the water
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Experimental 79 Test number 1 2 3 4
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Experimental 81 Figure 2.19: Plot o
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Experimental 83 2.5 Datalogger This
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Experimental 85 same reason a wood
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Experimental 87 Material Behaviour
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Experimental 89 in function of the
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Experimental 91 2.6.3 Influence of
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Chapter 3 Results and Discussion Th
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Results and Discussion 95 There is
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Results and Discussion 97 Figure 3.
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Results and Discussion 99 Parameter
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Results and Discussion 101 After pr
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Results and Discussion 103 of insta
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Results and Discussion 105 1. Mecha
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Results and Discussion 107 where k
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Results and Discussion 109 Kinetic
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Results and Discussion 111 Figure 3
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Page 117 and 118: Results and Discussion 117 Tables 3
Page 119 and 120: Results and Discussion 119 Figure 3
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Page 129 and 130: Results and Discussion 129 t DSC [s
Page 133 and 134: Results and Discussion 133 Using th
Page 135 and 136: Results and Discussion 135 forward
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Page 143 and 144: Results and Discussion 143 Since ev
Page 145 and 146: Results and Discussion 145 ditions.
Page 147 and 148: Results and Discussion 147 3.23 and
Page 149 and 150: Results and Discussion 149 The T g
Page 151 and 152: Results and Discussion 151 3.6.1 St
Page 153 and 154: Results and Discussion 153 Flexural
Page 155 and 156: Results and Discussion 155 3.7.2 FT
Page 157 and 158: Results and Discussion 157 identifi
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Page 161 and 162: Results and Discussion 161 Also in
Page 163: Conclusions and Outlook 163 degree
Page 167 and 168: A Brief History of Microwave Oven 1
Page 169 and 170: Bibliography [1] W. Callister, “M
Page 171 and 172: BIBLIOGRAPHY 171 [19] P. I. Karkana
Page 173: BIBLIOGRAPHY 173 [34] K. D. V. Pras
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