Kinetic Analysis and Characterization of Epoxy Resins ... - FedOA

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Acknowledgments I thank my supervisor Prof. Ing. Domenico Acierno, who always supported me with interesting scientific discussions and for giving me the possibility to attend various conferences on microwave engineering. I gratefully thank my supervisor Prof. Dr. Eugenio Amendola for his precious teachings and above all for his strong support in every moment of my research activity during these three years. It has been always challenging, but also very pleasant working together. I hope that this is only the starting point of future collaborations in dielectric heating of thermosetting resins. I thank Ing. Aniello Cammarano for his very useful help during this work. I thank Mr. Giovanni Napolitano for his contribution to analysis and elaboration of calorimetric and kinetic data. I thank Mr. Luigi Lisbo, Mr. Mario De Angioletti, Mr. Massimo Lombardo and Mrs. Mariarosaria Marcedula for their technical very precious support. I thank Ing. Claudio Mazzon for his useful assistance about microwave plant. I thank Dr. Marida Fasano and Mr. Antonio Capone for their useful support for bibliographic research.
3 I thank all the lecturers of PhD Industrial Engineering School for their competent and qualified contributions to our postgraduate education. I thank my colleagues Valeria Caggiano, Gabriella Callegaro and Anna Maria Scamardella. During these three years, we really supported one another in every moment. I gratefully thank my girlfriend Dora for her very precious moral support. I thank my mother for the patience, who has showed me during this work. 3
Page 1: UNIVERSITA’ DEGLI STUDI DI NAPOLI
Page 5 and 6: 5 Microwaves are electromagnetic ra
Page 7 and 8: CONTENTS 7 1.8.1 DielectricProperti
Page 9 and 10: CONTENTS 9 4 Conclusions and Outloo
Page 11 and 12: LIST OF TABLES 11 3.2 Average value
Page 13 and 14: List of Figures 1.1 Diglycidylether
Page 15 and 16: LIST OF FIGURES 15 2.23 Onset tempe
Page 17 and 18: LIST OF FIGURES 17 3.38 Comparison
Page 19 and 20: Introduction 19 cannot be melted an
Page 21 and 22: Introduction 21 • bismaleimides;
Page 23 and 24: Introduction 23 cold solders, casti
Page 25 and 26: Introduction 25 Average Properties
Page 27 and 28: Introduction 27 In Figure 1.4 n can
Page 29 and 30: Introduction 29 ducts and it genera
Page 31 and 32: Introduction 31 tween current-carry
Page 33 and 34: Introduction 33 that describe the p
Page 35 and 36: Introduction 35 1.3.5 Lorentz Force
Page 37 and 38: Introduction 37 Figure 1.11: Electr
Page 39 and 40: Introduction 39 Even microwaves can
Page 41 and 42: Introduction 41 production requirem
Page 43 and 44: Introduction 43 fect of the electro
Page 45 and 46: Introduction 45 following different
Page 47 and 48: Introduction 47 Debye equations bas
Page 49 and 50: Introduction 49 Although these mode
Page 51 and 52: Introduction 51 materials that have
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Chapter 2 Experimental In this chap
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Experimental 55 Characteristic Note
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Experimental 57 If the oven is used
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Experimental 59 In monomodal applic
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Experimental 61 Figure 2.5: Right s
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Experimental 63 Figure 2.8: Front v
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Experimental 65 regardless of the a
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Experimental 67 • The number of t
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Experimental 69 Figure 2.11: Surfac
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Experimental 71 Figure 2.12: Repeti
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Experimental 73 From the Figure 2.1
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Experimental 75 in the centre of th
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Experimental 77 not read the water
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Experimental 79 Test number 1 2 3 4
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Experimental 81 Figure 2.19: Plot o
Page 83 and 84:
Experimental 83 2.5 Datalogger This
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Experimental 85 same reason a wood
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Experimental 87 Material Behaviour
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Experimental 89 in function of the
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Experimental 91 2.6.3 Influence of
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Chapter 3 Results and Discussion Th
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Results and Discussion 95 There is
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Results and Discussion 97 Figure 3.
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Results and Discussion 99 Parameter
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Results and Discussion 101 After pr
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Results and Discussion 103 of insta
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Results and Discussion 105 1. Mecha
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Results and Discussion 107 where k
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Results and Discussion 109 Kinetic
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Results and Discussion 111 Figure 3
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Results and Discussion 113 3.3 Comp
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Results and Discussion 115 pedestal
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Results and Discussion 117 Tables 3
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Page 121 and 122:
Page 123 and 124:
Results and Discussion 123 t MW [s]
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Results and Discussion 125 simulate
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Page 129 and 130:
Results and Discussion 129 t DSC [s
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Page 133 and 134:
Results and Discussion 133 Using th
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Results and Discussion 135 forward
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Page 139 and 140:
Page 141 and 142:
Results and Discussion 141 than the
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Results and Discussion 143 Since ev
Page 145 and 146:
Results and Discussion 145 ditions.
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Results and Discussion 147 3.23 and
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Results and Discussion 149 The T g
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Results and Discussion 151 3.6.1 St
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Results and Discussion 153 Flexural
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Results and Discussion 155 3.7.2 FT
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Results and Discussion 157 identifi
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Results and Discussion 159 This eff
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Results and Discussion 161 Also in
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Conclusions and Outlook 163 degree
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Appendix A A Brief History of Micro
Page 167 and 168:
A Brief History of Microwave Oven 1
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Bibliography [1] W. Callister, “M
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BIBLIOGRAPHY 171 [19] P. I. Karkana
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BIBLIOGRAPHY 173 [34] K. D. V. Pras
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Kinetic Analysis and Characterization of Epoxy Resins ... - FedOA

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