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Using Polymer Modified Asphalt Emulsions in Surface Treatments A ...

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stra<strong>in</strong>-controlled tests <strong>in</strong>dicate that softer mixes are more fatigue resistant (16).<br />

Moreover, because polymer modified asphalt b<strong>in</strong>ders are used as th<strong>in</strong>ly-applied surface<br />

treatments, the physical parameters used to characterize the performance of HMA<br />

mixes (such as the PG specification) may not always be applicable.<br />

The search for physical parameters and related laboratory tests which can be used to<br />

accurately characterize the performance of PME is on-go<strong>in</strong>g. The follow<strong>in</strong>g section<br />

discusses some of the <strong>in</strong>formation obta<strong>in</strong>ed from the literature review which perta<strong>in</strong>s to<br />

the use and adaptation of various <strong>in</strong>novative and rout<strong>in</strong>e test<strong>in</strong>g protocols that have<br />

been, or which may be utilized for the analysis of PME residue performance.<br />

2.4.2 Test<strong>in</strong>g Protocols and Considerations<br />

Analysis of asphalt emulsion properties may be accomplished by directly collect<strong>in</strong>g a<br />

sample of the non-emulsified b<strong>in</strong>der, or by extract<strong>in</strong>g the properly cured residue from a<br />

prepared emulsion sample. Typical residue extraction techniques <strong>in</strong>clude:<br />

• Stirred Can Method – A commonly utilized extraction technique, it <strong>in</strong>volves<br />

constantly stirr<strong>in</strong>g a sample of the emulsion for 170 m<strong>in</strong>utes at a temperature of<br />

163º C. to drive-off the water. A blanket of nitrogen gas is used to dampen the<br />

effects of oxidation. Although this method yields abundant quantities of testable<br />

residue <strong>in</strong> fairly short-order, it has been criticized as not accurately represent<strong>in</strong>g<br />

actual field conditions due to the high cont<strong>in</strong>uous temperatures which are used<br />

(59).<br />

• RTFO Method – This methodology described by Takamura (2000) is a variation<br />

on the RFTO test used to simulate ag<strong>in</strong>g (60). Samples of the emulsion are<br />

rolled <strong>in</strong> bottles <strong>in</strong> a temperature-controlled environment at 85º C. for 75 m<strong>in</strong>utes<br />

with a stream of heated nitrogen gas jetted over the emulsion film to facilitate<br />

water evaporation. This method has also received criticism because it can lead<br />

to <strong>in</strong>complete water evaporation <strong>in</strong> certa<strong>in</strong> asphalt emulsions such as CRS-P2,<br />

produc<strong>in</strong>g <strong>in</strong>consistent follow-up test results (59). However, some suggest that<br />

this method may be useful for quality control purposes at emulsion production<br />

sites s<strong>in</strong>ce it permits for the rapid extraction of testable quantities of residue (60).<br />

45

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