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Complete Report - University of New South Wales

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Figure 4.3.2.25: Properly deglazed pits with palladium<br />

activation: a) PCD and b) BCD.<br />

(a)<br />

(b)<br />

The palladium activated pit samples were sintered at<br />

350°C for 10 minutes and the un-reacted nickel was<br />

removed. Figure 4.3.2.26 shows a much improved<br />

interface in the BCD pits with palladium activation, and the roughening <strong>of</strong> the surface indicates<br />

that a thin, fairly uniform layer <strong>of</strong> silicide has been formed at the interface. The morphology <strong>of</strong><br />

the PCD interface is also improved by the inclusion <strong>of</strong> the palladium activation process.<br />

Figure 4.3.2.26: Pits on the same sample as that shown<br />

in Figure 4.3.2.23 after sintering and nickel removal.<br />

(a)<br />

(b)<br />

49

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