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CEL# 10-17749<br />
Source: Sem Materials<br />
Material: Ralumac verification testing<br />
CTM 331: Residue by Evaporation T59: Residue by Distillation<br />
Tested By:lh Tested By:cg<br />
EMULSION TEST RESULTS FOR EMULSIONS E1<br />
tare identification 1 2 3 A'=Initial sample wt, g: 199.9 or 200.0 or 200.1 not tested<br />
B: tare wt (beaker+rod), g 64.9 64 64.7 B'=Tare wt,g (still, lid, clamp, therm's, gasket) 0<br />
emulsion weight, g 40 40 40 C=Average start time: end time: total time:<br />
A: final total dry weight, g 90.6 89.2 90.8 Residue,% D'=Total final wt,g (tare & distilled sample) 0<br />
Res, % 64.3 63.0 65.3 64.2 E'=Final sample wt, g=(D'-B') 0.0<br />
emulsion weight = 39.9g or 40.0g or 40.1g C'=Residue, %= (E'/A')100 C'= #VALUE!<br />
residue, % = 2.5[A-B] start time @ 118°C: 6:15 1. distillation time: 60 +/- 15 min<br />
@30m, increase temp to 138°C: 6:45<br />
after 1.5h, stir and return to oven: 8:15<br />
complete after add'l 1.0h: 9:15<br />
187<br />
T49: Penetration of Bituminous Materials<br />
T53: Ring & Ball Softening Point<br />
Tested By:LH Test temp, °C: 25 Tested By: LH Liquid Bath Used: Boiled Distilled Water<br />
Time, s: 5 Left side Right Side<br />
Cup#1 Load, g: 100 °C: 61 °C: 61.5<br />
Trial #1: 46<br />
Trial #2: 48 Softening Point to Report, °C: 61.3<br />
Trial #3: 47<br />
AVERAGE: 47 1. Heat sample no more than 110°C above expected softening point within 2 hr max.<br />
Report to the nearest whole unit the average of 3 penetrations 2. Pour sample into heated rings. Total time from this point not to exceed 240 min.<br />
whose values do not differ by more than the following: 3. Cool, at ambient, for 30min. Trim excess w/heated spatula.<br />
Pen range: 0-49 50-149 4. Assemble apparatus (w/steel balls at bottom); fill w/water to 105mm depth; return to refrig<br />
Max difference between 2 4 or ice bath for 15 min<br />
highest & lowest penetration result 5. Apply heat at 5°C/min. After first 3min, max. variation is +/-0.5°C<br />
6. If the difference between the two temperatures exceeds 1°C (2°F), repeat the test.<br />
7. When using a 15C or 15F thermometer (low temp range), then report to nearest 0.2°C (0.5°F)