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ANP PROJECT QUARTERLY PROGRESS REPORT<br />

MATERIAL<br />

4<br />

a<br />

Fig. 11.9. Type 316 stainless steel from Spinner Test with sodium at 816OC<br />

for 100 hr at a Speed of 400 ft/min. 250X.<br />

Inconel<br />

Type 316 stainless steel<br />

Type 347 stainless steel<br />

Type 446 stainless steel<br />

TIME OF<br />

TEST (hr)<br />

72<br />

100<br />

Ceramic Materials in Sodium. A<br />

series of static corrosion tests of<br />

various ceramic materials received<br />

from <strong>the</strong> Ceramic laboratory has been<br />

run in sodium at 816°C for 100 hr in<br />

Inconel tubing. The results are<br />

tabulated in Table 11.11 for <strong>the</strong><br />

materials that did not disintegrate<br />

during test. Only two of <strong>the</strong> specimens<br />

were intact after testing (A1,0, and<br />

146<br />

74<br />

53<br />

METALLOGRAPHIC NOTFS<br />

Surface layer of 0.5 mil with 0.5 mil of inter-<br />

granular voids beneath<br />

Intergranular attack, 1 to 2 mils deep on lead-<br />

ing edge and 0.5 to 1 mil deep on trailing<br />

edge<br />

Intergranular attack, to 2 mils<br />

Slight intergranular attack, less than 0.5 mil<br />

Spinel). It is possible that if <strong>the</strong><br />

specimens that broke up during testing<br />

had been thicker (specimens were<br />

approximately 0,020 in, thick), some<br />

of <strong>the</strong>m would have remained intact.<br />

The specimens that disintegrated into<br />

fine powder during <strong>the</strong> testing included<br />

porcelain (A1-576), mica, titanium<br />

dioxide (A1-192), SiO,, barium titanate<br />

(Al-T-106), A1,0, (single crystal ), lead<br />

8

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