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ANP PROJECT QUARTERLY PROGRESS REPORT<br />

14. RADIATION DAMAGE<br />

D. S. Billington, Solid State Division<br />

A. J. Miller,<br />

Radiation-damage studies of ma-<br />

terials exposed in <strong>the</strong> ORNE graphite<br />

reactor, <strong>the</strong> LITR, and <strong>the</strong> 86-in.<br />

cyclotron have continued. A sample of<br />

a zirconium-bearing fused fluoride<br />

fuel has been irradiated with a high<br />

flux in <strong>the</strong> MTR, but examination of<br />

<strong>the</strong> irradiated capsule and its con-<br />

tents has, not yet been made. A sodium-<br />

filled loop was operated in <strong>the</strong> LITR<br />

at about 1200”F, but it was shut down<br />

after seven days because of a flow<br />

s t oppage .<br />

Additional irradiations of fuel<br />

have been carried out in <strong>the</strong> LITR at<br />

ARE fission rates for extended periods<br />

of time. High power dissipations, in<br />

<strong>the</strong> range that would occur in an air-<br />

craft reactor, were achieved for long<br />

periods of time in fuels by using 22-<br />

Mev protons from <strong>the</strong> cyclotron, and<br />

<strong>the</strong>re was some indication, but no<br />

positive evidence, of radiation damage<br />

or radiation-induced corrosion.<br />

In-reactor cantilever creep measure-<br />

ments on Inconel in an air atmosphere<br />

were continued in both <strong>the</strong> graphite<br />

reactor and <strong>the</strong> LITR. Frorn <strong>the</strong>se more<br />

recent measurements, it appears that<br />

<strong>the</strong> radiation has only a small effect<br />

on <strong>the</strong> creep strength. Examination of<br />

some of <strong>the</strong> older test rigs showed<br />

that <strong>the</strong> decrease in creep strength<br />

previous 1 y reported cou Id pos s i bl y<br />

have been due to defective extensometer<br />

devi.ces. Apparatus is being con-<br />

structed for creep measuremenLs #in <strong>the</strong><br />

MTR.<br />

These radiation damage studies are<br />

described in <strong>the</strong> following. Additional<br />

information is contained in <strong>the</strong> So 1 id<br />

State Division Quarterly Progress<br />

Report for <strong>the</strong> Period Ending November<br />

lo-, 1952.<br />

186<br />

ANP Dhvision<br />

IRRADIATION OF FUSED HATERIALS<br />

G. W. Keillioltz D. F. Weeks<br />

J. G. Morgan M. T. Robinson<br />

11. E. Robertson D. D. Davies<br />

C. C. <strong>Web</strong>ster A. Richt<br />

P. R. Klein W. J. Sturm<br />

M. J. Feldman<br />

Solid State Division<br />

R. J. Jones R. I,. Knight<br />

Electromagnetic Research Division<br />

B. 1‘. Kinyon<br />

OHNL Engineering Division<br />

The installation in <strong>the</strong> MTR of <strong>the</strong><br />

testing facility for fused salts was<br />

completed. The guide tube extends<br />

from a 1 3/8-in. hole in a beryllium<br />

“A” piece through a specially designed<br />

flange in <strong>the</strong> north-tank access hole.<br />

In <strong>the</strong> first run, a 1-in. column of<br />

salt was contained in a 0.1-in.-ID<br />

Inconel capsule. The capsule ternpcra-<br />

ture was maintained at 1500°F by means<br />

of a controlled flow of cooling air.<br />

The flux at <strong>the</strong> capsule position was<br />

determined by means of cobal t wire with<br />

<strong>the</strong> MTR operating at 19 and at, 25<br />

megawatts. The estimated <strong>the</strong>rmal flux<br />

for <strong>the</strong> first capsule run at 30 mega-<br />

watts was 2.1 x ioi4.<br />

The capsule contained a fuel with<br />

<strong>the</strong> composi tion NaF-ZrF4 -UF, (50.0-<br />

46.2-3.8 mole X). It was maintained<br />

at 1500°F for 116 hr at full flux, and<br />

<strong>the</strong>re was an estimated power dissipation<br />

of 1900 watts/cm3 in <strong>the</strong> fused salt.<br />

This approaches <strong>the</strong> power density<br />

expected in an aircraft reactor,<br />

Examinations of <strong>the</strong> irradiated capsule<br />

and <strong>the</strong> salt are now being made. In<br />

addition, two capsules containing <strong>the</strong><br />

fuel have been irradiated in <strong>the</strong> LITR<br />

at 140 watts/cm3 for 565 hr, and two<br />

more have been placed in <strong>the</strong> LITR for<br />

1000-hr tests. Examinations of <strong>the</strong>

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