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feedstocks were sub-sampled <strong>and</strong> freeze-thawed under ambient temperature for loading<br />

into the reactor. The simulations were also characterized in different time intervals during<br />

the long time storage. The average total <strong>solid</strong> (TS), volatile <strong>solid</strong> (VS) <strong>and</strong> ca rbon (C)<br />

contents <strong>of</strong> the Feedstocks 1 & 2, <strong>and</strong> Feedstock 3 were 20.2%, 85%TS, 51.5%TS <strong>and</strong><br />

17%, 86%TS, 51%TS respectively.<br />

3.2 Experimental Set-up<br />

3.2.1 Experimental set-up for gas formation potential test<br />

Gas formation potential test (also called GP21 test) was conducted for Feedstock 1 <strong>and</strong> 2.<br />

The experimental set-up for it has been shown in Figure 3.2. Laboratory glass bottle <strong>of</strong> 500<br />

mL with a thick Teflon/silicon (0.01”/0.05”) septum in its arms were used as reaction<br />

vessels for <strong>waste</strong>. The reaction vessel was connected to a long cylindrical approximately<br />

1L glass tube called eudiometer by plastic tube that was used for measurement <strong>of</strong> volume<br />

<strong>of</strong> biogas produced. The eudiometer had barrier solution that was free to move by the<br />

pressure <strong>of</strong> produced biogas to another 1L plastic bottle (called reservoir tank) connected<br />

to the other end <strong>of</strong> eudiometer. The reaction vessel was placed in a water bath to attain the<br />

required temperature <strong>of</strong> 35 ºC (Heerenklage <strong>and</strong> Stegmann, 2005).<br />

3<br />

4<br />

5<br />

2<br />

1<br />

79 cm<br />

4 cm<br />

Figure 3.2 Experimental set-up for gas formation potential test<br />

3.2.2 Experimental set-up for pilot-scale experiments<br />

6<br />

8<br />

7<br />

A stainless steel inclined thermophilic <strong>dry</strong> <strong>anaerobic</strong> <strong>digestion</strong> system (ITDAR) was<br />

designed with the total <strong>and</strong> working volume <strong>of</strong> 0.69 <strong>and</strong> 0.55 m 3 , respectively. The internal<br />

diameter <strong>of</strong> the reactor was 0.6 m <strong>and</strong> the total height was 2.4 m. It was placed in an<br />

inclination <strong>of</strong> about 30 o from the ground level to facilitate easy flow <strong>of</strong> the <strong>waste</strong> as shown<br />

in Figure 3.3. The ITDAR was externally connected with the <strong>waste</strong> feeding hopper, screw<br />

46<br />

9<br />

GC<br />

1. Sample + inoculum<br />

2. Reaction vessel, 500 mL<br />

3. Water bath<br />

4. Liquid sampling<br />

5. Plastic tube<br />

6. Gas collection tube<br />

(Eudiometer tube ~ 1L)<br />

7. Gas sampling<br />

8. Barrier solution<br />

9. Reservoir tank, 1L

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