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<strong><strong>ALU</strong>MINIUM</strong> SMELTING INDUSTRY<br />

Meeting of the ISO Committee for analysis of<br />

materials for primary aluminium in Switzerland<br />

L. P. Lossius, Norsk Hydro; J.-C. Fischer, R&D Carbon<br />

The Swiss standardisation authority SNV<br />

and R&D Carbon Ltd hosted the 6 th Plenary<br />

Meeting of ISO Technical Committee<br />

226 ‘Materials for the production of<br />

primary aluminium’ in Sierre early in October<br />

2012. The participation was good,<br />

with 16 delegates and eight of the twelve<br />

P-member countries attending.<br />

Highlights of the meeting were the progress on<br />

four new alumina standards and the harmonisation<br />

of three anode / cathode standards on<br />

mechanical strength; details for each material<br />

type below are given below.<br />

Two new convenors were confirmed: Mr<br />

Wu Lin of Do-Fluorides (China) for smelter<br />

grade fluorides and Mr Jean-Claude Fischer<br />

of R&D Carbon (Switzerland) for petroleum<br />

coke.<br />

The Technical Committee 226 is responsible<br />

for 110 ISO standards on the sampling<br />

and analysis of materials for the electrolytic<br />

production of aluminium, covering the material<br />

groups Smelter grade alumina, Smelter<br />

grade fluorides, Pitch, Petroleum coke and<br />

Carbon electrodes. The main work is maintenance<br />

and development of standards, with a<br />

dedicated work group (WG) for each material.<br />

After the Sierre meeting, the Work Group<br />

Convenors are:<br />

• Nigel Turner of Koppers EU, UK; WG1 on<br />

Pitch<br />

• Professor Harald A. Øye of NTNU, Norway;<br />

WG2 on Carbon electrodes<br />

• Ray Brown of Alcoa, Australia; WG3 on<br />

Smelter grade alumina<br />

• Wu Lin of Do-Fluoride Chemicals Co., Ltd,<br />

China; WG4 on Smelter grade fluorides<br />

• Jean-Claude Fischer, R&D Carbon Ltd,<br />

Switzerland; WG6 on Petroleum coke.<br />

The Plenary Meeting reconfirmed 17 standards<br />

and confirmed the development of 11<br />

new standards. This makes a fairly large<br />

number of standards, but current development<br />

work mostly replaces out-of-date methods<br />

with new and improved methods, and aims to<br />

later withdraw the out-of-date standards.<br />

For Smelter grade alumina there are four<br />

standards in development, based on the muchused<br />

Australian standards: elemental analysis<br />

by XRF, bulk density, flow time, and α-alumina<br />

content. In addition to the informal work<br />

in WG3, the following ISO technical experts<br />

are nominated for this work: Ray Brown (Alcoa<br />

Australia, SA), Flor Campa (Alcoa, for<br />

AENOR), Kjell Hamberg (Hydro, for SN) and<br />

Josef Lovcican (Slovalco, for SUTN).<br />

For Smelter grade fluorides the new standard<br />

ISO 12926 for elemental analysis by XRF<br />

From the tour of the R&D Carbon facilities in Sierre, from the left: Ray Brown (Alcoa, Convenor alumina),<br />

in front Erwin Smits (Aluchemie), Petter Lossius (Hydro, Committee Chair), Nigel Turner (Koppers EU, Convenor<br />

Pitch), Ma Cunzhen (SAC), Yu Yiru (JN Carbon), Xue Xujin (Do-Fluorides) and Jean-Claude Fischer<br />

(R&D Carbon, Convenor Petroleum coke).<br />

will be ready for publication in 2013. Work<br />

is also on-going in the fluoride field to review<br />

or replace several old fluoride methods; ISO<br />

technical experts are Xujin Xue (Do-Fluorides,<br />

for SAC); Wu Lin (Do-Fluorides, for SAC);<br />

Oscar Pérez (Derivados del Flúor, for AENOR)<br />

and L.P. Lossius (Hydro, for SN).<br />

For Pitch, a critical issue today is the determination<br />

of Quinoline insoluble. TC 226 expresses<br />

high concern for the continued availability<br />

of Quinoline because REACH regulations<br />

could ban it, but Quinoline is vital and<br />

critical to an important raw materials test. The<br />

committee therefore recommends interested<br />

organisations, if they are surveyed, to state<br />

that they wish to retain Quinoline.<br />

In the Solid carbon bodies the next published<br />

standard will be the dynamic modulus<br />

of elasticity by the resonance method, which<br />

goes to the final vote this autumn. Work is also<br />

on-going to harmonise existing standards, and<br />

Andreas Schnittker (SGL Carbon, for DIN) has<br />

harmonised the existing standards for 3-and<br />

4-point flexural strength, as well as the crushing<br />

strength standard; these will be republished<br />

in 2013. ISO technical experts are Harald A.<br />

Øye (NTNU, for SN), Jean-Claude Fischer<br />

(R&D Carbon, for SNV), Erwin Smits (Aluchemie,<br />

for NEN), Yu Yiru (JN Carbon, for SAC)<br />

and Nigel Turner (Koppers EU, for BSI).<br />

For Petroleum coke there is a revision to<br />

specific electrical resistivity to add measurement<br />

of the 1.4-1.0 mm fraction, harmonising<br />

the sample preparation for the routine coke<br />

analysis.<br />

For information on the work in TC226,<br />

please contact the Secretary Knut Aune at<br />

kau@standard.no or the Committee Chair<br />

Lorentz Petter Lossius, Hydro Aluminium,<br />

Norway at lorentz.petter.lossius@hydro.com.<br />

Stéphane Sauvage is the Technical Programme<br />

manager for TC226 on behalf of the<br />

ISO Central Secretariat, Geneva. Note that<br />

the standards in the TC226 programme are<br />

available in the ISO Store as a CD made specifically<br />

for ‘Materials for the production of<br />

primary aluminium’.<br />

The Committee thanks R&D Carbon, Hydro<br />

Aluminium and Sør-Norge Aluminium<br />

for sponsoring the 2012 Plenary Meeting and<br />

TC226. The plenary meetings are held every<br />

18 months, and the next plenary meeting will<br />

be hosted by DIN and SGL Carbon, in Wiesbaden,<br />

Germany, on 8-9 May 2014. In September<br />

2015, a plenary meeting will be hosted<br />

by SAC and Do-Fluorides Chemicals, in China.<br />

Authors<br />

Dr.-Ing. Lorentz Petter Lossius is principal engineer<br />

for primary metal technology at Norsk Hydro ASA,<br />

based in Øvre Årdal, Norway.<br />

Jean-Claude Fischer is director of R&D Carbon Ltd,<br />

based in Chalais, Switzerland.<br />

86 <strong><strong>ALU</strong>MINIUM</strong> · 1-2/2013

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