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Standard analysiscolumnsOrganic SEC (GPC) columns(General Analysis) : THF, chloroformFeaturesKF-800, K-800Standard organic solvent SEC (GPC) columnSupports a wide range of applications from low to high-molecular-weightcompoundsPreparativeColumnsp.86, 87Standard columns52Organic SEC (GPC) columns (General Analysis) : THF, chloroformKF-800 series : Shipping solvent tetrahydrofuran(THF)Product CodeF6028010F6028020F6028025F6028030F6027030F6028040F6027040F6028050F6027050F6028060F6028090F6027060F6028070F6027070F6700300F6709350F6028110F6028120F6028125F6028130F6028194F6028140F6028195F6028150F6028196F6028160F6028190F6028197F6028170F6028198F6700401F6709450Product NameGPC KF-801GPC KF-802GPC KF-802.5GPC KF-803GPC KF-803LGPC KF-804GPC KF-804LGPC KF-805GPC KF-805LGPC KF-806GPC KF-806MGPC KF-806LGPC KF-807GPC KF-807LGPC KF-GGPC KF-800DK-800 series : Shipping solvent chloroformProduct CodeProduct NameGPC K-801GPC K-802GPC K-802.5GPC K-803GPC K-803LGPC K-804GPC K-804LGPC K-805GPC K-805LGPC K-806GPC K-806MGPC K-806LGPC K-807GPC K-807LGPC K-GGPC K-800DPlate Number(TP/column)≥ 18,000≥ 18,000≥ 18,000≥ 18,000≥ 18,000≥ 18,000≥ 18,000≥ 11,000≥ 11,000≥ 11,000≥ 13,000≥ 11,000≥ 6,000≥ 6,000(guard column)(solvent-peak separation column)Plate Number(TP/column)≥ 18,000≥ 18,000≥ 18,000≥ 18,000≥ 18,000≥ 18,000≥ 18,000≥ 11,000≥ 11,000≥ 11,000≥ 13,000≥ 11,000≥ 6,000≥ 6,000(guard column)(solvent-peak separation column)Exclusion Limit(PS)1,5005,00020,00070,00070,000400,000400,0004,000,0004,000,000(20,000,000)*(20,000,000)*(20,000,000)*(200,000,000)*(200,000,000)*−−Exclusion Limit(PS)1,5005,00020,00070,00070,000400,000400,0004,000,0004,000,000(20,000,000)*(20,000,000)*(20,000,000)*(200,000,000)*(200,000,000)*−−Particle Size(μm)666667710101010101818810Particle Size(μm)666667710101010101818810* See page 54 for details of the solvent-peak separation columns. The columns with ‘L’or ‘M’ at the end of the column name aremixed-gel columns capable of a wide molecular weight distribution range of samples.MaximumPore SizeColumn Size(Å) (mm) I.D. x L50 8.0 × 300150 8.0 × 300300 8.0 × 300500 8.0 × 300500 8.0 × 3001,500 8.0 × 3001,500 8.0 × 3005,000 8.0 × 3005,000 8.0 × 30010,000 8.0 × 30010,000 8.0 × 30010,000 8.0 × 30020,000 8.0 × 30020,000 8.0 × 300−4.6 × 10−8.0 × 100*( )Estimated valueMaximumPore Size(Å)501503005005001,5001,5005,0005,00010,00010,00010,00020,00020,000−−Column Size(mm) I.D. x L8.0 × 3008.0 × 3008.0 × 3008.0 × 3008.0 × 3008.0 × 3008.0 × 3008.0 × 3008.0 × 3008.0 × 3008.0 × 3008.0 × 3008.0 × 3008.0 × 3004.6 × 108.0 × 100*( )Estimated valueMolecular weight range with polystyrene (eluent KF-800 series : THF, K-800 series : chloroform)Molecular weight (Polystyrene)10 10 2 10 3 10 4 10 5 10 6 10 7 10 8 10 9KF-, K-801KF-, K-802KF-, K-802.5KF-, K-803KF-, K-804KF-, K-805KF-, K-806KF-, K-807Molecular weight (Polystyrene)10 10 2 10 3 10 4 10 5 10 6 10 7 10 8 10 9KF-, K-803LKF-, K-804LKF-, K-805LKF-, K-806MKF-, K-806LKF-, K-807L*Contact Shodex or our distributors near you for customized columns.
Calibration curves for KF-800 seriesusing PS standardMolecular weight (Polystyrene)10 610 510 410 3KF-802KF-801KF-806KF-804KF-803KF-802.5KF-807KF-805KF-806MCalibration curves for KF-800L (linear type)series using PS standardMolecular weight (Polystyrene)10 810 610 510 410 3KF-807LKF-806LKF-805LKF-804LKF-803LPolycarbonate resinSample : Polycarbonate resin 0.1%, 100μLCH3O C O CCH3 O nStandard analysiscolumns10 210 21010 8 25 min10 7 Elution volume (mL)5 6 7 8 9 10 11 12 131010 7 Elution volume (mL)5 6 7 8 9 10 11 121315 20 30minColumn : Shodex GPC KF-800 seriesEluent : THFFlow rate : 1.0mL/minDetector : RIColumn temp. : Room temp.Silicon oilSample : Silicone oil 0.1%, 200μLSilicone oil101520Column : Shodex GPC K-806M x 2Eluent : TolueneFlow rate : 1.0mL/minDetector : RIColumn temp. : 45˚CPhenoxy resinColumn : Shodex GPC KF-800L seriesEluent : THFFlow rate : 1.0mL/minDetector : RIColumn temp. : Room temp.Styrene isoprene ABA block copolymerSample : Styrene isoprene ABA block copolymer15 20 25 minColumn : Shodex GPC KF-806M x 2Eluent : THFFlow rate : 1.0mL/minDetector : RIColumn temp. : 30˚CColumn : Shodex GPC KF-806L x 2Eluent : THFFlow rate : 1.0mL/minDetector : RIColumn temp. : 40˚CBionolle TM (Polybutylene succinate/adipate)Sample : 100μLPolybutylene succinate/adipate 0.2%15 20 25 30 minColumn : Shodex GPC K-806M x 2 + K-801Eluent : ChloroformFlow rate : 1.0mL/minDetector : RIColumn temp. : 40˚CRecycling fractionation of lauryl stearyl thiodipropionate53Organic SEC (GPC) columns (General Analysis) : THF, chloroformSample : Phenoxy resin 0.1%, 100μLSample : 5%, 500μL1. Distearyl thiodipropionate2. Lauryl stearyl thiodipropionate3. Dilauryl thiodipropionateCH3O C OCH2 CHCH2CH3 OHnCYCLE1CYCLE2 CYCLE6 CYCLE1021310 15 20 25 min010 20Column : Shodex GPC KF-806L x 2Eluent : THFFlow rate : 1.0mL/minDetector : RIColumn temp. : 40˚CColumn : Shodex GPC K-LG + K-2001Eluent : ChloroformFlow rate : 3.0mL/minDetector : RIColumn temp. : 50˚C
Page 1 and 2:
Capture the EssenceHPLC Columns and
Page 3 and 4: ContentsColumn selectionSample pret
Page 5 and 6: HPLC Separation ModesLiquid chromat
Page 7 and 8: FoodsNutritionalingredientsFood saf
Page 9 and 10: Preparation of Test Samples Used in
Page 11 and 12: Systems diagram for column switchin
Page 13 and 14: Polymer-based Packed Columns for Re
Page 15 and 16: Polymer-based Packed columns forHyd
Page 17 and 18: Comparison between ODP2 HP and ODP-
Page 19 and 20: Hydantoins3214RONONHSample :Hydanto
Page 21 and 22: 0Saccharides analysis using corona-
Page 23 and 24: Hippuric acids in urineStandards123
Page 25 and 26: Medicinal chemicalssampleAlprenolol
Page 27 and 28: Protein separation using QA-8251234
Page 29 and 30: Protein separation using cation exc
Page 31 and 32: ApplicationProduct NameAFpak AAB-89
Page 33 and 34: Column Trouble ShootingCommon cause
Page 35 and 36: FeaturesDC-613,SC1211,SZ5532Separat
Page 37 and 38: 6 78Saccharides in wood12Sample : 5
Page 39 and 40: Maltooligosuccharides, organic acid
Page 41 and 42: Anion analysis with non-suppressor
Page 43 and 44: Standard cations (YS-50 and YK-421)
Page 45 and 46: Precautions for polar polymer analy
Page 47 and 48: Calibration curves for KW400 series
Page 49 and 50: Calibration curves for SB400 series
Page 51 and 52: Calibration curves for GS-HQ series
Page 53: Calibration curves for GF-HQ series
Page 57 and 58: Calibration curves for KD-800 serie
Page 59 and 60: Calibration curves for KF-600 serie
Page 61 and 62: Calibration curve for LF-804 usingP
Page 63 and 64: Calibration curves for HFIP-800 ser
Page 65 and 66: Calibration Standards for SEC[Polys
Page 67 and 68: FoodsNutritional ingredientsColumn
Page 69 and 70: BiotechnologyColumn list for Biotec
Page 71 and 72: USP(United States Pharmacopeia) Col
Page 73 and 74: I.D.2.0mm1.0mm0.8mm0.5mm0.3mm2.0mm1
Page 75 and 76: AFpak AAB-894 semi-micro and micro
Page 77 and 78: AFpak ALC-894 semi-micro and micro
Page 79 and 80: KW402.5 semi-micro and micro typeBa
Page 81 and 82: I.D.4.6mm2.0mm1.0mm0.8mm0.5mm0.3mmL
Page 83 and 84: Asahipak GF-310 HQ semi-micro and m
Page 85 and 86: Preparative columnsPolymer-based Pa
Page 87 and 88: Columns for Ligand Exchange Chromat
Page 89 and 90: GPC K-800 series Preparative typePr
Page 91 and 92: General precautions for column hand
Page 93 and 94: Refractive Index DetectorShodex RI
Page 95 and 96: Instable baseline valuesSTARTColumn
Page 97 and 98: II-524A, IA-GJJJ-50KK-801~807, K-80
Page 99 and 100: Useful Information Regarding Shodex
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