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Standard analysiscolumnsOrganic SEC (GPC) columns : HFIP solvent typeFeaturesHFIP-800 Columns exclusively for use with hexafluoroisopropanol (HFIP)HFIP-600Rapid analysis, solvent-saving typeStandard columnsHFIP-800 series60Organic SEC (GPC) columns : HFIP solvent typeProduct CodeF6028530F6028540F6028550F6028560F6028590F6028570F6700500F6021030F6021040F6021050F6021060F6021080F6021070F6700511Product NameGPC HFIP-803GPC HFIP-804GPC HFIP-805GPC HFIP-806GPC HFIP-806MGPC HFIP-807GPC HFIP-LGGPC HFIP-603GPC HFIP-604GPC HFIP-605GPC HFIP-606GPC HFIP-606MGPC HFIP-607GPC HFIP-GPlate Number(TP/column)≥ 12,000≥ 12,000≥ 10,000≥ 10,000≥ 10,000≥ 4,000(guard column)≥ 12,000≥ 12,000≥ 5,000≥ 5,000≥ 6,000≥ 3,000(guard column)Exclusion Limit(PMMA)*30,000100,0001,000,000(10,000,000)**(10,000,000)**(100,000,000)**−* The columns with ‘M’ at the end of the column name are mixed-gel columns capable of awide molecular weight distribution range of samples.Rapid analysis downsized columnsHFIP-600 seriesProduct CodeProduct NamePlate Number(TP/column)Exclusion Limit(PMMA)*30,000100,0001,000,000(10,000,000)**(10,000,000)**(100,000,000)**−ParticleSize(μm)1071010101815ParticleSize(μm)33101010188MaximumPore Size(Å)5001,5005,00010,00010,00020,000−MaximumPore Size(Å)5001,5005,00010,00010,00020,000−Column Size(mm)I.D. x L8.0 × 3008.0 × 3008.0 × 3008.0 × 3008.0 × 3008.0 × 3008.0 × 50Shipping solvent : hexafluoroisopropanol (HFIP)*PMMA : polymethylmethacrylate**( )Estimated valueUse of the HFIP-600 series with semi-micro type devices is recommended.Column Size(mm)I.D. x L6.0 × 1506.0 × 1506.0 × 1506.0 × 1506.0 × 1506.0 × 1504.6 × 10* The columns with ‘M’ at the end of the column name are mixed-gel columns capable of awide molecular weight distribution range of samples.Shipping solvent : hexafluoroisopropanol (HFIP)*PMMA : polymethylmethacrylate**( )Estimated valueMolecular weight range with PMMA (eluent : HFIP)Molecular weight (PMMA)10 2 10 3 10 4 10 5 10 6 10 7 10 8 10 9HEIP-803, 603HEIP-804, 604HEIP-805, 605HEIP-806, 606HEIP-807, 607HEIP-806M, 606M*Contact Shodex or our distributors near you for customized columns.
Calibration curves for HFIP-800 seriesusing polymethylmethacrylate (PMMA)Molecular weight (PMMA)10 7 110 62310 545610 47810 310 29105 6 7 8 9 10 11 12Elution volume (mL)HFIP-805HFIP-806MHFIP-804HFIP-803HFIP-806Calibration curves for HFIP-600 seriesusing polymethylmethacrylate (PMMA)Molecular weight (PMMA)10 610 510 410 310 2HFIP-605HFIP-606MHFIP-604HFIP-603HFIP-6061.0 1.5 2.0 2.5 3.0 3.5 4.0Polyethylene terephthalate (PET)Sample : PET 0.2%, 20μLMw=19,3000 5 1015minStandard analysiscolumnsElution volume (mL)Column : Shodex GPC HFIP-800 seriesEluent : HFIPFlow rate : 1.0mL/minDetector : RIColumn temp. : Room temp.Polyamide (effect of salt addition)HFIP5mM CF3COONa/HFIP10 15 20 2530 minColumn : Shodex GPC HFIP-600 seriesEluent : 5mM CF 3COONa in HFIPDetector : RI(small cell volume)Column temp. : 40˚CSample : Polycaprolactum (Nylon TM 6)In SEC analysis using HFIP some samplesmay yield abnormal peaks as a result ofelectrostatic interaction. In this case, theimpact of electrostatic interaction can beremoved by adding sodium trifluoroacetateto HFIP.Column : Shodex GPC HFIP-606M x 2Eluent : 5mM CF 3COONa in HFIPFlow rate : 0.6mL/minDetector : RI(small cell volume)Column temp. : 40˚CPolybutylene terephthalate (PBT)Sample : PBT 0.05%, 500μL1520 30 min61Organic SEC (GPC) columns : HFIP solvent typeColumn : Shodex GPC HFIP-806M x 2Eluent : HFIP(solid line), 5mM CF 3 COONa in HFIP(broken line)Flow rate : 1.0mL/minDetector : RIColumn temp. : 40˚CColumn : Shodex GPC HFIP-805 + HFIP-803Eluent : 5mM CF 3 COONa in HFIPFlow rate : 1.0mL/minDetector : RIColumn temp. : 40˚CPolyamides (Nylon 6/10 and Nylon 6)PolyacetalSample : Nylon TM 6/10 0.2%, 20μL Sample : Nylon TM 6 0.2%, 20μL Sample : Polyacetal 0.2%, 20μLMw=29,300 Mw=38,100 Mw=176,0000 5 1015min0 5 10150 5 10 15minminColumn : Shodex GPC HFIP-606M x 2Eluent : 5mM CF 3 COONa in HFIPFlow rate : 0.6mL/minDetector : RI(small cell volume)Column temp. : 40˚CColumn : Shodex GPC HFIP-606M x 2Eluent : 5mM CF 3 COONa in HFIPFlow rate : 0.6mL/minDetector : RI(small cell volume)Column temp. : 40˚C
Page 1 and 2:
Capture the EssenceHPLC Columns and
Page 3 and 4:
ContentsColumn selectionSample pret
Page 5 and 6:
HPLC Separation ModesLiquid chromat
Page 7 and 8:
FoodsNutritionalingredientsFood saf
Page 9 and 10:
Preparation of Test Samples Used in
Page 11 and 12: Systems diagram for column switchin
Page 13 and 14: Polymer-based Packed Columns for Re
Page 15 and 16: Polymer-based Packed columns forHyd
Page 17 and 18: Comparison between ODP2 HP and ODP-
Page 19 and 20: Hydantoins3214RONONHSample :Hydanto
Page 21 and 22: 0Saccharides analysis using corona-
Page 23 and 24: Hippuric acids in urineStandards123
Page 25 and 26: Medicinal chemicalssampleAlprenolol
Page 27 and 28: Protein separation using QA-8251234
Page 29 and 30: Protein separation using cation exc
Page 31 and 32: ApplicationProduct NameAFpak AAB-89
Page 33 and 34: Column Trouble ShootingCommon cause
Page 35 and 36: FeaturesDC-613,SC1211,SZ5532Separat
Page 37 and 38: 6 78Saccharides in wood12Sample : 5
Page 39 and 40: Maltooligosuccharides, organic acid
Page 41 and 42: Anion analysis with non-suppressor
Page 43 and 44: Standard cations (YS-50 and YK-421)
Page 45 and 46: Precautions for polar polymer analy
Page 47 and 48: Calibration curves for KW400 series
Page 49 and 50: Calibration curves for SB400 series
Page 51 and 52: Calibration curves for GS-HQ series
Page 53 and 54: Calibration curves for GF-HQ series
Page 55 and 56: Calibration curves for KF-800 serie
Page 57 and 58: Calibration curves for KD-800 serie
Page 59 and 60: Calibration curves for KF-600 serie
Page 61: Calibration curve for LF-804 usingP
Page 65 and 66: Calibration Standards for SEC[Polys
Page 67 and 68: FoodsNutritional ingredientsColumn
Page 69 and 70: BiotechnologyColumn list for Biotec
Page 71 and 72: USP(United States Pharmacopeia) Col
Page 73 and 74: I.D.2.0mm1.0mm0.8mm0.5mm0.3mm2.0mm1
Page 75 and 76: AFpak AAB-894 semi-micro and micro
Page 77 and 78: AFpak ALC-894 semi-micro and micro
Page 79 and 80: KW402.5 semi-micro and micro typeBa
Page 81 and 82: I.D.4.6mm2.0mm1.0mm0.8mm0.5mm0.3mmL
Page 83 and 84: Asahipak GF-310 HQ semi-micro and m
Page 85 and 86: Preparative columnsPolymer-based Pa
Page 87 and 88: Columns for Ligand Exchange Chromat
Page 89 and 90: GPC K-800 series Preparative typePr
Page 91 and 92: General precautions for column hand
Page 93 and 94: Refractive Index DetectorShodex RI
Page 95 and 96: Instable baseline valuesSTARTColumn
Page 97 and 98: II-524A, IA-GJJJ-50KK-801~807, K-80
Page 99 and 100: Useful Information Regarding Shodex
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