TECHNICAL PROGRAM - American Chemical Society Publications

170. Convenient one-pot synthesis of 4-substituted-2,6-dihalopyridines:
Valuable
building blocks for medicinally active heterocycles.
V. Neelagiri, P. Salgaonkar,
D. Sethumadhavan, M. Neelagiri,
V. Rajur, H. Kim, R. Rajur, R. Reddy,
K. Vines, S. Gadamasetty, C. Moon
171. Intermolecular aza Diels-Alder reactions
of iminoacetonitriles.A[4� 2 ] cycloaddition
route to substituted tetrahydropyridines.
S. Tumidajski, K. M. Maloney,
R. L. Danheiser
172. Toward [8]circulene. R. Bhola,
B. T. King
173. Short synthesis of benzo[1,2,5]triazepin-
4-ones via intramolecular S NAr substitution.
S. Jin, O. St-Jean, V. Santhakumar,
M. J. Tomaszewski
174. X-ray, NMR, FTIR and DFT structural
study of enaminketone derivatives of the
Fisher base. O. F. Vazquez-Vuelvas,
D. Morales-Morales, Z. Gomez-Sandoval,
M. Tlenkopatchev, A. Pineda-Contreras
175. New photolabile linkers for the solidphase
synthesis of NH-1,2,3-triazoles,
homoserine lactones, and other heterocycles.
K. Qvortrup, T. E. Nielsen
176. Microwave-assisted soluble polymer
supported synthesis of quinoxalines,
benzodiazepines, and benzimidazoles.
F. S. Fouad
177. Total synthesis of cyclooroidin and
studies towards some oroidin dimers.
S. Mukherjee, C. J. Lovely
178. Modified synthesis and direct borylation
of corannulene. M. N. Eliseeva,
L. T. Scott
179. Peculiarities of the reaction between
sodium hydroxide and syn- and anti-isomers
of 5-substituted 2-(4-chlorobutyryl)aminobenzophenones
oximes.
O. V. Kulikov, L. K. Minacheva,
A. V. Mazepa
180. Interactions of �-conjugated chains in
stacked oligo(phenylene ethynylene)s.
S. P. Jagtap, G. Brizius, W. Komorner,
D. M. Collard
181. Mild and efficient �-alkynylation of
butenolides: Short synthesis of fugomycins.
N. Bruneau-Latour, J. Boukouvalas
182. Diels-Alder strategy for constructing
�-benzoyl-�-arylbutenolides: Expedient
synthesis of cadiolides. C. Thibault,
J. Boukouvalas
183. Troubleshooting a synthesis: Optimization
of a synthetic route to cyclic hydroxamic
acids. B. M. Bechle,A.B.Dounay,
X. Gan, S. Ghosh, J. Kim, L. McAllister,
V. Parikh, J. Tuttle, P. Verhoest
184. Reactivity and regioselectivity of nitroalkenes
with unsymmetrical münchnones.
J. M. Lopchuk,G.W.Gribble
185. Progress toward the asymmetric synthesis
of cyclic hydroxamic acids: Route
design and optimization. S. Ghosh,
A. B. Dounay, X. Gan, B. M. Bechle,
J. Kim, L. McAllister, V. Parikh,
J. B. Tuttle, P. R. Verhoest
186. Formal olefination and acylaziridination
of imidazolones. X. Dai, M. W. Miller,
A. W. Stamford
187. Picolinamide derivatives as ligand in
aryl-aryl Ullmann type couplings at RT.
F. Damkaci, E. Altay
188. Synthesis and characterization of 1,8dithia-4,11-diazacyclotetradecane.
T. L. Walker, M. J. Taschner, W. Malasi,
S. Bhide, T. Parker
189. Synthesis and alkali metal reduction of
cyclooctatetraenyl isocyanate. J. R. Klen,
S. J. Peters
190. Superelectrophilic chemistry of nitriles.
D. A. Klumpp,E.K.Raja
191. Direct continuous flow synthesis of
highly substituted pyrrole-3-carboxylic
acids via in situ hydrolysis of tert-butyl
esters. A. Herath,N.D.Cosford
192. Rapid multistep continuous flow synthesis
of novel 3,4-dihydropyrimidin-
2(1H)-ones (DHPMs): Tandem heterocycle
formation/three component reaction
in a single continuous microreactor sequence.
N. Pagano, A. Herath,
N. D. Cosford
193. Charge migration across aryl groups in
superelectrophiles. D. A. Klumpp,
R. R. Naredia, K. J. Boblak,
M. J. O’Connor
194. New methods for the quaternization of
benzothiazoles. L. Chen
195. Protio-defluorination chemistry.
D. A. Klumpp, A. Kethe
196. Synthesis of chiral amino acid based
pyrrolidine thioethers. A. M. Lineberry,
M. J. Taschner
197. Synthesis and conjugation of chlorins to
iron oxide nanoparticles for diagnoses
and treatment of atherosclerotic vascular
disease. S. Erdem, R. Weissleder,
J. McCarthy*
198. Synthesis of novel 6,12-disubstituted
derivatives of Tröger’s base. E. Ascic,
J. Artacho, K. Månsson, J. Karlsson,
M. Harmata, V. Snieckus, K. Wärnmark
199. Withdrawn
200. Direct aziridination of 1,3-dioxenones:
Applications in the synthesis �-amino
acids. M. Fletcher, J. Falla,
E. C. McLaughlin
201. Application of hetero-Michael pathways
for the synthesis of sultam libraries.
Q. Zang, S. Javed, P. K. Maity,
J. J. Hasting, P. R. Hanson
202. Design and synthesis of a Lewis acid
functionalized room-temperature ionic
liquid for use as a gas capture material.
B. R. Wiesenauer, J. E. Bara,
R. D. Noble, D. L. Gin
203. Synthesis and biological evaluation of
macrocyclic bifunctional ligands for cancer
therapy. X. Sun, H. Song, M. Dadwal,
C. Kang, A. Dai, H. Chong
204. Synthesis of �-substituted porpholactones
as novel chromophores for optical
high pH sensing. J. Worlinsky, G. Zarate,
P. Daddario, M. Ghandehari, G. Khalil,
C. Brückner
205. Synthesis of (�)-2-aryl- and (�)-2-alkylsubstituted2,3-dihydro-4(1H)-quinazolinones
from 2-nitro- and 2-aminobenzamide.
R. A. Bunce, B. Nammalwar
206. [Azeteochlorinato]Ni(II), a pyrrole ringcontracted
chlorin analog. M. A. Hyland,
S. Banerjee, C. Brückner
207. Oxazolochlorins: Stable chlorin-type
chromophores. J. Ogikubo,
L. Samankumara, C. Brückner
208. Formation of bridged and fused bicyclic
diazenium salts from aryl hydrazone precursors.
J. Wyman, M. I. Javed,
M. Brewer
209. Reactions of 2-alkynylcarboxylic acids
and terminal alkynes. D. E. Mendes,
A. M. Schoffstall
210. Investigations of heterocyclic sulfones
as medicinal compounds. K. N. Barrett,
J. McKee, M. Zanger
211. Toward a library-optimized approach to
synthetic ergolines. M. A. Parker,
J. Hwang, D. Schmit, J. Almazan,
M. Farmer, J. Duensing, M. B. Bergdahl
212. Solid state aldol synthesis of novel anticancer
chalcones. J. K. Rugutt
213. Gold(I)-catalyzed intermolecular amination
of allylic alcohols with cyclic ureas
and related nucleophiles. P. Mukherjee,
R. A. Widenhoefer
214. Synthesis of pyrroles and furans via
Au(I)-catalyzed Claisen rearrangement.
A. Saito, T. Konishi, Y. Hanzawa
215. TiCl 4-activated selective nucleophilic
substitutions of t-butyl alcohol and benzyl
alcohols with pi-donating substituents.
C. Tsai, R. Sung, K. Sung
216. Copper-catalyzed formations of sulfurnitrogen
bonds using thiols. N. Taniguchi
217. Highly chemoselective nickel-catalyzed
three-component cross-trimerization of
three distinct alkynes leading to 1,3-dien-
5-ynes. K. Ogata, Y. Atsuumi,
S. Fukuzawa
218. Pd(II)-catalyzed arylation of cyclic
enaminones using boronic acids via C–H
functionalization. Y. KIM, G. I. Georg
219. Zirconium mediated three component
reaction with carbon dioxide. D. Castillo,
J. Padilla,S.Oda,S.Mito
220. Highly diastereoselective synthesis of
both (E)-and (Z)-trisubstituted alkenes via
organoboranes. N. G. Bhat, L. Reyna
221. Novel diastereoselective synthesis of
(Z)-disubstituted alkenes containing a
4-methylbenzyl moiety via organoboranes.
N. G. Bhat, R. Cavazos
222. Tandem catalysis: Highly functionalized
lactones through a ruthenium-catalyzed
ring closing metathesis/hetero-Pauson-
Khand reaction sequence.
D. F. Finnegan,M.L.Snapper
223. Development of a new generation of
C-C bond forming reactions through C-H
activation. M. Wasa
224. Synthesis of oxindoles using copper
mediated radical cyclisation. H. Parekh
225. Intramolecular C-C formation via oxidative
coupling reactions. K. C. Pereira,
A. Kantak, B. DeBoef
226. Csp 3 -Csp 3 bond formation by nickelcatalyzed
reductive coupling of alkyl halides.
M. R. Prinsell,D.J.Weix
227. Isolated polyacetylene chains in a urea
inclusion complex. A. Lashua,
B. S. Hudson, M. B. Sponsler
228. Pd-Pd bridged complexes: Synthesis
and reactivity. R. Rios, M. Viciano,
A. Moyano
229. Rh(I)-catalyzed diasterselective and
enantioselecive diboration of internal
alkenes. M. Tsai
230. Synthesis of new radiopharmaceuticals
for PET imaging by “click chemistry”.
J. Sims-Mourtada, I. Tworowska
231. In search of a universal Suzuki-Miyaura
reaction. C. Stanciu, S. Berritt,
S. D. Dreher
232. Synthesis of 5-7-5 fused tricyclic lactones
via Rh(I)-catalyzed [2�2�2�1] cycloaddition
of enediynes with carbon
monoxide. J. J. Kaloko,G.Y.Teng,
S. Pavel, I. Ojima, A. A. Athan
233. Rh-catalyzed intramolecular cycloadditions
of 1,6-diene-11-ynes and 6-ene-
1,11-diynes. A. A. Athan,J.J.Kaloko,
G. Y. Teng, I. Ojima
234. Rh(I)-catalyzed [2�2�2�1] cycloaddition
of triynes for rapid access to cholchicinoids.
G. Y. Teng,J.Kaloko,I.Ojima
235. Transition metal-catalyzed addition reactions
of arylboronic acids with alkyl
2-formylbenzoates: Efficient access to
chiral 3-substituted phthalides. Y. Liao,
C. Xing, P. He, Q. Hu
236. Formation of novel 5-7-5-5 fused tetracyclic
skeletons through Rh(I)-catalyzed
[2�2�2�1] cycloaddition of cyclopentene-diynes
with carbon monoxide.
J. J. Kaloko, G. Y. Teng, A. A. Athan,
I. Ojima
237. Oxidative addition of malonates to tetrahydrofurans
via ferrocenium hexafluorophosphate.
C. R. Stephenson,
B. S. Matsuura
238. Selective reduction of �, �-unsaturated
carbonyl compounds using Bu 3SnH.
D. V. Vidhani, M. E. Krafft, J. W. Cran
239. Mechanistic studies of a Pd-catalyzed
olefin dioxygenation. S. R. Neufeldt,
M. S. Sanford
240. Development of a palladium-catalyzed
arylfunctionalization of alkenes.
A. Kubota, A. D. Satterfield,
M. S. Sanford
241. Development of novel cationic Diels-Alder
dienophiles stabilized by cobaltalkyne
complexes. M. Torres,K.M.Shea
242. Diels-Alder dienes activated by cobaltcomplexed
alkynes. S. J. Perlmutter,
K. M. Shea
243. Group 4 metal mediated reactions with
carbon dioxide. S. Oda,S.Mito
244. Lithium 2-pyridyltrihydroxyborate salts:
Stable, isolable, and scalable boronates
for Suzuki-Miyaura coupling reactions.
K. Chen, R. Peterson, S. K. Math,
J. LaMunyon, C. Testa
245. Hydrogen-bonding scaffolds and their
application to Henry reactions in nitrosugar
syntheses. A. J. Metrano,
B. R. Linton
246. New fluorescent gelators derived from
1,3,5-benzenetricarboxamide: Synthesis
and gel preparation. Y. Chen, C. Huang,
P. P. Lee, Y. Wang, H. Wang, J. H. Xin,
K. K. Cheuk
247. Study on self-assembly of novel 1,3,5benzenetricarboxamide-basedorganogel.
Y. Chen, C. Huang, P. P. Lee,
Y. Wang, H. Wang, J. H. Xin, K. K. Cheuk
248. Low molecular weight organogel based
on pyrene derivative. C. Huang, Y. Chen,
P. P. Lee, Y. Wang, H. Wang, J. H. Xin,
K. K. Cheuk
249. Towards lanthanide-based responsive
luminescent probes for the detection of
reactive oxygen species. J. Laakso,
K. E. Borbas
250. Disassembly of amphiphilic macromolecules
based-nanocontainers with enzyme
as stimulus. F. Wang,
M. A. Azagarsamy, S. Thayumanavan
251. Resolution of pharmaceuticals via crystallization
self-assembled monolayers.
P. S. Navare, J. C. MacDonald
252. Crystal engineering of sulfoxides: A
multiple synthon approach in the formation
of sulfa drug-based co-crystals.
E. Elacqua, D. Bucar, R. F. Henry,
G. G. Zhang, L. R. MacGillivray
253. Localization of self-assembled molecular
nanofiber on endoplasmic reticulum
inside live cells. Y. Gao, Y. Kuang, B. Xu
254. N-alkyl-DABCOnium trihalozincates:
Privileged scaffolds for the preparation of
noncentrosymmetric solids. A. D. Finke,
D. L. Gray, J. S. Moore
255. Effects of halogenation on the self-assembly
and hydrogelation of a small molecule.
D. M. Ryan, S. B. Anderson,
B. L. Nilsson
256. Synthesis and characterization of novel
macrocycles based on chenodeoxycholic
acid (CDCA) as potent drug delivery system.
X. Bai, X. Chen, J. R. Dias
257. Sugar-responsive organoboron block
copolymers. J. N. Cambre,D.Roy,
B. S. Sumerlin
258. Colorimetric detection of iodide ions.
I. Ahn, J. Choi, D. Cho
259. Encapsulation and isolation of flavin–
polymer conjugates using dendritic guest
moieties via molecular recognition.
C. Subramani, G. Yesilbag, B. J. Jordan,
X. Li, G. Cooke, A. Sanyal, V. M. Rotello
260. Cell-surface and lysate based identification
of cell types and cancer states using
gold nanoparticle-GFP supramolecular
complexes. S. Rana, A. Bajaj,
O. R. Miranda, J. C. Yawe, D. J. Jerry,
U. H. Bunz
261. Semiconductor co-crystals based on
carboxylic acids. K. M. Kester,
J. C. Sumrak, L. R. MacGillivray
262. Design of ruthenium and osmium containing
coiled-coil peptide dimers: Studies
in energy transfer. D. J. Wilger,
M. L. Waters
263. Synthesis and self-assembly of membrane-active
cationic molecules.
M. J. Razumov, J. S. Carter, H. Patel,
G. J. Gabriel
264. Aqueous self-assembly of porphyrin
nanowires: Synthesis, characterization
and energy transfer studies. M. Fathalla,
A. Neuberger, S. Li, R. Schmehl,
U. Diebold, J. Jayawickramarajah
265. Coordination-driven selective self-assembly
of multicomponent supramolecules.
Y. Zheng, M. Wang, Z. Zhao,
J. B. Pollock, K. Ghosh
266. Tripodal binding groups for the noncovalent
functionalization of graphene
sheets. J. A. Mann,W.R.Dichtel
267. Synthesis and studies of assembled
structures of porphyrins bearing rigid hydrogen
bonding motifs. S. Singh,
C. M. Drain
268. Traveling wave ion mobility mass spectrometry
analysis of self-assembled terpyridine-based
Ru(II)-Fe(II) macrocycles.
X. Li, Y. Chan, G. Newkome,
C. Wesdemiotis
269. Enhancing molecular gelation using
functionalized polymers for sensing applications.
Y. Adhia,T.H.Lent,J.Chen,
M. T. Perez, A. J. McNeil
The official technical program
for the 240th National Meeting
is available at:
www.acs.org/boston2010
ORGN
TECH–87