TECHNICAL PROGRAM - American Chemical Society Publications

971. Practical synthesis of 6-carboalkoxy-
13-cycloalkyl-5H-indolo[2,1-a] [2] benzazepine-10-carboxylic
acid derivatives.
P. Hewawasam, Y. Tu, T. Hudyma,
R. Gentles, N. Meanwell, J. Kadow
972. Pd/C catalyzed reductive formylation of
indoles and quinolines. R. Gianatassio,
A. Kulkarni,B.Török
973. Synthetic studies toward the cytotoxic
marine peptide lucentamycin A.
S. Ranatunga,U.Pal,J. R. Del Valle
974. Makeover of the halogen/lithium exchange:
Continuous reactor studies.
D. W. Slocum, D. Kusmic, J. C. Raber,
P. E. Whitley
975. Studies towards the synthesis and
structure determination of palmerolide C.
J. Wlochal, S. Eadie, G. J. Florence
976. Preparation of 2,5-disubstituted pyrazolo[4,3-c]cinnolin-3-ones.
D. R. Pitts,
R. M. DiPardo, A. W. Johnson, V. Cofre,
D. C. Beshore
977. Development of aromatic thiol-catalysts
for intramolecular Morita-Baylis-Hillman
and Rauhut-Currier reactions. P. S. Selig,
S. J. Miller
978. Studies towards the synthesis of palmerolide
A. S. Eadie, R. Murray,
G. J. Florence
979. Iron(III) tosylate catalyzed deprotection
of acetals and tetrahydropyranyl ethers.
M. V. Chiodo, P. R. Lazzara, M. E. Olson,
V. V. Angeles, R. S. Mohan
980. Direct asymmetric synthesis of
�-butenolides by bifunctional thiourea
catalyzed coupling of 2-(3H)-furanones to
aldehydes. S. J. Howard,P.D.Bloom
981. Synthetic studies towards the aplyronines:
Potent anticancer marine macrolides
isolated from Aplysia kurodai.
S. J. Fink, L. Y. Lee, I. Paterson
982. Thermal rearrangement of cyclobutadiene
cycloadducts: A novel approach to
5-7-5(6) ring system. J. He,
M. L. Snapper
983. Fluorous benzaldehyde-based multicomponent
reactions for heterocycles.
B. Piqani, S. Ding, T. Xu, W. Zhang
984. Synthesis of quaternary carbon centers
via hydroformylation using a scaffolding
ligand. X. Sun, K. Frimpong,
T. E. Lightburn, K. L. Tan
985. Chlorination of metalated nitriles and
enolates. B. R. Pitta, F. F. Fleming
986. Progress toward antiproliferative agent
popolohuanone E: A general approach to
complex cis-fused decalins featuring catalytic
carbon insertion methodology.
H. Z. Kaplan, J. S. Kingsbury
987. Total synthesis of flinderoles A-C by
gold(I)-catalyzed hydroarylation of indole.
R. M. Zeldin,F.Toste
988. Synthetic studies of tamandarin B side
chain analogs. J. Lee, K. M. Lassen,
M. M. Joullie
989. New designs of polyphenylene dendrimers
for full-color light-emitting diodes.
T. Qin,K.Müllen
990. New C-H functionalization route to heterocycles.
M. Yagoubi, M. C. Willis,
P. Nichols
991. Synthesis of heterobifunctional linkers
for nanomedicinal chemistry.
R. N. Hanson, K. Dao, T. Dunstan,
A. Kozhushuyan, J. A. Hendricks,
H. Pham, V. Ronga
992. Diastereoselective 2-aza-Cope rearrangements
and their applications in diversity-oriented
synthesis.
B. M. Ibbeson, D. T. Blackwell,
D. R. Spring
993. Application of in situ silver-imidazolylidene
complexes in ionic liquid mediated
glycosidation reactions. V. Kumar,
I. J. Talisman, S. V. Malhotra
994. Dual role of ionic liquids as phase transfer
catalysts and solvents for O-glycosidation
reactions. V. Kumar,
I. J. Talisman, S. V. Malhotra
995. Ligand-assisted, copper-catalyzed intramolecular
amination. D. N. Barman
996. Microwave-based methodology for the
preparation of organoselenium compounds.
M. Marques, I. L. Martins,
C. Charneira, A. J. Vieira, A. M. Antunes
997. Total synthesis of spinosyn analogs.
N. Schützenmeister, L. F. Tietze
998. Synthetic studies toward the synthesis
of Bromophycolides. H. Lin, I. Krauss
999. Insertion reactions of titanacyclobutanes.
G. Liu, I. Krauss
1000. Reductive substitution of aromatic
substituted acetonitriles with lithium
naphthalenide and electrophiles. I. Chen,
J. Tsao, T. Tsai, H. Liu, J. Zhu
1001. Synthesis of functionally diverse iodonium
salts via in-situ generated [hydroxy-
(tosyloxy)iodo]arenes as precursors to
18 F-labeling agents. J. Chun,V.W.Pike
1002. Progress toward the synthesis of
marineosins A and B. X. Cai,B.B.Snider
1003. Progress toward the synthesis of 7-hydroxylycopodine
and sauroine. H. Lin,
B. B. Snider
1004. Triphenylphosphine/brominating
agent: An efficient reagent for the preparation
of allylic bromides from allylic alcohols.
P. Taboonpong, W. Chavasiri
1005. New and efficient protocol for the synthesis
of bromosilane using Br 3CCOOEt/
PdCl 2. P. Srithanakit, W. Chavasiri
1006. Electron transfer induced [2�2] cycloaddition
reactions and cycloreversion
reactions of cyclobutane ring. Y. Okada,
K. Chiba
1007. Progress toward the total synthesis of
Brasilicardin A. S. Yi, C. Regan,
M. E. Jung
1008. Multi-drug resistance reversal agents:
Update on the synthesis of euphosalicin.
C. Aichinger, C. R. Lentsch, U. Rinner
1009. Catalytic scaffolding ligands: An efficient
method for directing reactions.
T. E. Lightburn, M. T. Dombrowski,
K. L. Tan*
1010. Approaches to the synthesis of isaindigotidione.
M. Hellal,G.D.Cuny
1011. Nickel-catalyzed cross-couplings of
secondary alkyl nucleophiles with aryl halides.
A. Joshi-Pangu, M. Ganesh,
M. Biscoe
1012. Quick access to the tetracycle of
strychnose alkaloids: Concise racemic
and asymmetric total syntheses of
akuammicine, strychnine. G. Sirasani,
R. B. Andrade
1013. Allyl and crotyl transfer by allyldioxazaborolidines.
M. K. Reilly,
S. D. Rychnovsky
1014. Synthesis and characterization of ferrocenyl
chalcones: Potential compounds
against some diseases.
M. R. Otaño-Vega,
N. Lafontaine-Vargas,
R. Cardona-Couvertier,
I. Montes-González,
A. R. Guadalupe-Quiñones
1015. Intramolecular, thermal [2 � 2] cycloaddition
reactions of allene-ynes: Exploring
the scope, mechanism, and application
to natural product synthesis.
K. M. Brummond, J. M. Osbourn
1016. Intramolecular 1,4-addition of nitrogen
nucleophile and halogen to conjugated
enyne. J. B. Werness, W. Tang, N. Liu
1017. Synthetic studies toward pseudotabersonine
and 5-epi-pseudotabersonine.
B. Cheng, J. D. Sunderhaus,
S. F. Martin
1018. Synthesis of p-benzoquinone methides
via benzannulated enediynyl alcohols.
B. Wen, J. L. Petersen, K. K. Wang
1019. Synthesis of lipophilic dodecyl bis(cycloSaligenyl)
nucleoside monophosphate
triesters. Y. Ahmadibeni, B. Carroll,
G. F. Doncel, K. Parang
1020. Synthesis of branched lipophilic thymidine
�-triphosphate triester conjugates
of anti-HIV nucleosides. Y. Ahmadibeni,
K. Parang
1021. Direct, HF free, synthesis of tetrabutylammonium
organotrifluoroborates.
G. Prakash, F. Pertusati,G.A.Olah
1022. Lewis-acid catalyzed [5�2]-annulation
toward stereoselective formation of functionalized
azapines. J. Woo
1023. Domino reactions based upon the Ruthenium-catalyzed
redox isomerization.
A. W. Franz, B. M. Trost
1024. New highly enantioselective organocatalytic
N-acyliminium cyclization cascades.
M. E. Muratore, C. A. Holloway,
D. J. Dixon
1025. Homoaporphine synthesis via microwave-assisted
direct arylation.
S. Chaudhary, W. W. Harding
1026. Development of a 2-aza-Cope-[3�2]
dipolar cycloaddition strategy for the synthesis
of quaternary proline scaffolds.
M. P. McCormack, S. P. Waters
1027. Practical synthesis of tert-butyl
amides from nitriles. J. C. Baum,
J. E. Milne, J. A. Murry, O. R. Thiel
1028. Metalated nitriles: Preferential S N2 cyclizations
of allylic chlorides. W. Liu,
P. Lu, P. C. Ravikumar,F.F.Fleming
1029. Development of a new method for Rucatalyzed
tandem ring-closing metathesis/hydroacylation.
Y. Nam,
M. L. Snapper
1030. Copper-catalyzed click reactions of
C-6 azidopurine nucleosides.
M. K. Singh, M. K. Lakshman
1031. Diastereoselective routes to �-aryl and
�-alkyl lactones: Mechanistic insights and
model synthetic studies toward highly oxidized
marine diterpenoids.
A. G. Macabeo, A. Kreuzer, O. Reiser
1032. Synthesis of O-vinyl oxime ethers by
iridium-catalyzed isomerization of O-allyl
oxime ethers: Reactivity, Control of stereochemistry,
and application to the synthesis
of pyrroles. H. Wang, L. Anderson
1033. Total synthesis of the indole alkaloid
(�)-subincanadine F. X. Cheng,
S. P. Waters
1034. Asymmetric synthesis of substituted
piperidines via aziridinium intermediates.
S. Jarvis, A. Charette
1035. New ligand for Ullmann type aryl halide
couplings. F. Damkaci, E. Altay
1036. Studies on the regioselectivity of catalytic
carbon insertion. A. F. Kornahrens,
J. A. Dabrowski, J. S. Kingsbury
1037. Bismuth salt-initiated epoxide rearrangement
and addition reactions toward
2,6-disubstituted dihydropyrans: What is
the role of bismuth? R. F. Lambert,
S. E. Ammann, L. C. Speight, Y. Lian,
J. Liu
1038. Factors affecting the rate of Diels-Alder
reactions involving 2-trialkylsilyloxy
furans. N. A. Setterholm, N. D. Serratore,
A. M. Franey, S. K. Bur
1039. Palladium-catalyzed asymmetric difunctionalization
of substituted vinyl phenols.
T. P. Pathak,K.H.Jensen,
M. S. Sigman
1040. Novel AlMe 3-promoted formation of
amides from acids and amines. J. Li,
D. Smith, K. Subramaniam, J. J. Li,
G. D. Vite, B. Chen
1041. Synthesis of regiospecifically fluorinated
vinyl triazoles. R. Kumar,B.Zajc
1042. Rh(I)/diene-catalyzed addition reactions
of aryl/alkenylboronic acids with aldehydes.
C. Xing
1043. Use of transition metal-catalyzed intramolecular
cyclization reactions in the
total synthesis of oroidin-derived alkaloids.
M. R. Bhandari, C. J. Lovely
1044. First total synthesis and structural
confirmation of fluvirucinine A 2 via an iterative
ring expansion. Y. Lee, J. Jung,
H. Yun, S. Lee, Y. Suh
1045. Concise total synthesis of (�)-tetrabenazine
and (�)-�-dihydrotetrabenazine.
S. Paek, N. Kim, H. Moon,Y.Suh
1046. Intermolecular [3�3] cycloadditions of
azides with the Nazarov intermediate.
O. Scadeng,F.G.West
1047. One-pot preparation of alkyl halides
from alkyl diphenylphosphinites.
K. Ruchamanee, W. Chavasiri
1048. Synthesis of succinate diesters as internal
donor for isotactic polypropylene
production process.
N. Sittichokwongkamol, W. Chavasiri
1049. Modular synthetic approach to Amicetin
derivatives. C. M. Serrano,
R. E. Looper
1050. Synthesis of aryl 1,3-butadienes from
the haloallylation of aryl aldehydes using
boron trihalide and subsequent elimination
with DBU. M. Quinn,M.Yao,
G. Kabalka
1051. Copper-catalyzed chlorination of functionalized
arylboronic acids. H. Wu,
J. Hynes
1052. Progress toward the asymmetric total
synthesis of Iriomoteolide 1A.
A. R. Dechert,M.T.Crimmins
1053. Utilizing the nitroso-ene reaction for
the synthesis of hydroxamic acid-based
natural products. R. Banerjee,S.B.King
1054. Minimizing the cost of organic chemistry
experimentation: Low-barrier microscale
high-throughput experimentation.
S. Berritt, S. D. Goble, M. T. Tudge,
D. Conway, S. D. Dreher
1055. Toward the synthesis of Thapsigargin.
C. Huang, K. Brummond
1056. Chiral phosphoramidic acids catalyzed
Mannich reaction. D. Ramella,
S. E. Schaus
1057. Studies directed toward the synthesis
of montamine. E. A. Colby Davie,
M. A. Dion, G. J. Dugas, J. M. St. Louis,
L. E. Lupien
1058. Formation of decahydroquinoline ring
systems from 2-acyl-5-amino-oxazolium
ions. C. H. Basch,S.A.Habay
1059. One-flask synthesis of benzyl phosphonates
from benzylic alcohols mediated
by ZnI 2. R. M. Richardson,
R. J. Barney, D. F. Wiemer
1060. Progress toward the synthesis of embedded
tetrahydrofuranyl isosteres.
C. M. Spencer,C.K.Zercher
1061. Studies toward the synthesis of (5R)polyandrane.
V. A. Cwynar,
M. G. Donahue, S. J. Fretz, D. J. Hart,
G. Mbogo, D. Yang
1062. Withdrawn
1063. Lewis acid catalyzed homo-Nazarov
cyclization of donor-acceptor substituted
cyclopropanes. D. V. Patil,S.A.France
1064. Development of a divergent synthesis
for the modular assembly of the zoanthamine
alkaloids. L. H. Phun,
S. A. France
1065. Radical cyclizations and atom-transfer
radical cyclizations enabled by visible
light photoredox catalysis. J. D. Nguyen,
J. W. Tucker, J. M. Narayanam,
C. R. Stephenson
1066. Photoactivation and photopassivation
of pristine and modified carbonaceous
materials as catalysts for benzylic oxidation.
V. Rajpara, G. Sereda
1067. Regioselective synthesis of tert-allylic
ethers via Gold (I) catalysis.
M. S. Hadfield
1068. Novel Lamellarin alkaloid-inspired libraries
via cycloisomerization/dipolar cycloaddition.
S. Bhagwanth,S.E.Schaus,
J. A. Porco, Jr.
1069. Using chiral, strained olefins to rapidly
assemble complex molecules.
M. T. Taylor,J.M.Fox
1070. Synthesis of trisubstituted-1,2,4-triazoles
as somatostatin subtype-4 receptor
ligands. I. Daryaei, M. Crider
1071. Chemical conversion of cellulose biomass
to biofuels. S. F. Panos, J. Kenny,
K. C. Pereira, J. Hegner, B. DeBoef,
B. Lucht
1072. Progress towards the synthesis of isatisine
A. J. D. Mighion,J.L.Moore,
E. J. Sorensen
1073. Synthesis of new rigidified manganese(III)-bis-salicylimine
peroxynitrite decomposition
catalysts for the treatment of
chronic pain. M. Ghaffari, B. Neumann
1074. Asymmetric synthesis of the enantiomer
and six diastereomers of the trisaccharide
portion of PI-080 and Vineomycin
C. Q. Chen, Y. Zhong, G. A. O’ Doherty
The official technical program
for the 240th National Meeting
is available at:
www.acs.org/boston2010
ORGN
TECH–97