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Proceedings e report - Firenze University Press

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RESEARCH ON THE AGING OF WOOD IN RISH<br />

thermal (TG, DSC) and chemical (chemical components, FT-IR spectroscopy, X-ray diffractometry)<br />

properties are being valuated. Fig. 3 shows the process flow of the property evaluation.<br />

Selection of samples Xylarium・Dr. Kohara collections<br />

Dating of samples Dendrochronology (RICPN)<br />

Radiocarbon dating (MJH)<br />

Morphological observation<br />

Photography Xylarium<br />

Annual ring width Xylarium<br />

Color Lab Xylarium<br />

Spectral reflectance<br />

Tissue observation Xylarium Mechanical Properties<br />

(permanent preparation) 3~5 specimens in each condition<br />

Bending test MOR<br />

Making samples MOE<br />

Bending test 2mm(T)×10mm(R)×60mm(L) :longitudinal direction Fracture toughness<br />

2mm(L)×10mm(T)×60mm(R) :radial direction Fracture deformation<br />

DMS 0.8mm(L)×2mm(T)×40mm(R) :radial direction (Brinnell hardness)<br />

Dielectric property 3mm(L)×40mm(T)×40mm(R) :end grain Cutting ability (Cutting force)<br />

(Chip shape)<br />

Fundamental properties<br />

(non-distractive)<br />

Chemical Properties<br />

Density Air dry using the specimens after bending test<br />

Oven dry<br />

Color Lab Thermal property DSC、TG<br />

Spectral reflectance TMA、DMS<br />

Infrared absorption Pyrolysis property<br />

Dynamic property Air dry Component<br />

Oven dry Crystallinity X-ray analysis<br />

Dielectric property Various MC Lignin Quantitative analysis<br />

Fig. 3 Process flow for evaluating the naturally aging wood from the cultural properties and historical buildings.<br />

As a part of the results from the physical and mechanical properties, Fig. 4 shows the age of the<br />

naturally aging wood samples determined by the dendrochronological dating and their equilibrium<br />

moisture contents. The wood substances of aging wood were less accessible to moisture and the<br />

equilibrium moisture content of the naturally aging wood decreased with an increase of the aging<br />

period, as shown in the figure.<br />

Fig. 5 shows the typical stress-strain curves of the aging wood of hinoki samples in the longitudinal<br />

direction. The naturally aging wood samples showed somewhat higher strength and stiffness but less<br />

toughness than those of control. It seems that the bending strength in the longitudinal direction of the<br />

naturally aging wood samples does not change so much through the aging period over 1600 years,<br />

though the values are scattered.<br />

54

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