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Characterization and control of the fiber-matrix interface in ceramic ...

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10<br />

lay-ups or filaiiients wound <strong>in</strong>to cyl<strong>in</strong>drical shdpes <strong>and</strong> densified,<br />

usually hy hpt press<strong>in</strong>g.<br />

The object <strong>of</strong> consolidation is to produce a dense material while<br />

<strong>in</strong>flict<strong>in</strong>g m<strong>in</strong>imal damage to <strong>the</strong> <strong>fiber</strong> or whisker re<strong>in</strong>forcement.<br />

The<br />

majority <strong>of</strong> densification processes employ high temperatures <strong>and</strong> some,<br />

such as hot press<strong>in</strong>g, utilize elevated temperature comb<strong>in</strong>ed with extreme<br />

pressui-e.<br />

These condi t i o m nay have detrimental effects on <strong>the</strong><br />

propertie4 <strong>of</strong> <strong>the</strong> re<strong>in</strong>forc<strong>in</strong>g component.<br />

3.2 Hot Press<strong>in</strong>g<br />

The <strong>in</strong>ost widely used technique ~ O K produc<strong>in</strong>g <strong>ceramic</strong> <strong>matrix</strong><br />

co<strong>in</strong>posi tes is hot press<strong>in</strong>g.<br />

Hot press<strong>in</strong>g has been used to fabricate<br />

composites from a large selection <strong>of</strong> polycrystall<strong>in</strong>e <strong>ceramic</strong> matvices<br />

(21,32,35). The properties <strong>of</strong> <strong>the</strong> composites depend on fabrication<br />

parameters such as <strong>the</strong> particle size distribution <strong>of</strong> <strong>the</strong> powders <strong>and</strong> <strong>the</strong><br />

temperatures <strong>and</strong> pressures employed.<br />

These pdrameters <strong>control</strong> <strong>the</strong><br />

porosity OL <strong>the</strong> <strong>matrix</strong> <strong>and</strong> <strong>the</strong> damage <strong>in</strong>troduced <strong>in</strong>to <strong>the</strong> <strong>fiber</strong>s <strong>and</strong> can<br />

affect f iber-<strong>matrix</strong> bond strength.<br />

Hot press<strong>in</strong>g has yieldpd <strong>fiber</strong>-<br />

re<strong>in</strong>forced <strong>ceramic</strong> composites with reproducible properties, <strong>and</strong> <strong>the</strong><br />

materials <strong>and</strong> process<strong>in</strong>g conditions have been studied <strong>in</strong> depth.<br />

However,<br />

<strong>the</strong> tcmper,?tures <strong>and</strong> pressores necessary to atta<strong>in</strong> <strong>the</strong> required densities<br />

<strong>in</strong> <strong>the</strong> matrices severely damage many <strong>of</strong> <strong>the</strong> available <strong>fiber</strong>s.<br />

An advantage <strong>of</strong> hot press<strong>in</strong>g is that <strong>the</strong> procedure does not require<br />

b<strong>in</strong>ders 1-0<br />

stiffen preforms prior to densification; thus, components can<br />

be fabricated with close dimensional tIolerances,<br />

The technique is<br />

restricted to relatively simple shapes but a similar process, hot

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