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William Angerer - Department of Physics and Astronomy - University ...

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77<br />

sample was mounted on a goniometer, which had an accuracy <strong>of</strong> 0.010 in the angle<br />

<strong>of</strong> incidence. A laser beam was aligned with the center <strong>of</strong> the goniometer, optically<br />

chopped at 2kHz, <strong>and</strong> p-polarized with a Newport Glan-Thompson calcite polarizer<br />

model 10GT04AR.14. The reflected light was detected by a Thor Labs silicon photodiode<br />

model FDSIOO <strong>and</strong> measured by a Stanford Research Systems lock-in amplifier<br />

model 530. The absolute reflection coefficient was determined by measuring the light<br />

transmitted through the optical system without the sample, mounting the sample on<br />

the goniometer, measuring the light reflected from the sample as a function <strong>of</strong> angle.<br />

<strong>and</strong> calculating the ratio <strong>of</strong> the reflected light to transmitted light. ~ote, the effect <strong>of</strong><br />

temporal fluctuations on the intensity <strong>of</strong> reflected light was removed by measuring a<br />

fraction <strong>of</strong> the incident beam <strong>and</strong> the light reflected from the sample simultaneously.<br />

The angular spectrum was then renormalized to remove temporal fluctuations.<br />

There are two experimental difficulties in measuring the thickness <strong>of</strong> a ,...., 1 pm<br />

GaN film grown on a sapphire substrate. First, the effective film thickness. nd. where<br />

n is the index <strong>of</strong> refraction <strong>and</strong> d is the film thickness, is several times the incident<br />

wavelength. In theory, a reflection measurement can unambiguously determine a film<br />

thickness only if the effective thickness is less than the wavelength <strong>of</strong> incident light.<br />

The measured intensity is produced by the interference <strong>of</strong> a wave that is reflected <strong>of</strong>f <strong>of</strong><br />

the front surface <strong>and</strong> a wave that is transmitted into the thin film where it undergoes<br />

a series <strong>of</strong> reflections <strong>and</strong> is partially transmitted out <strong>of</strong> the film. If the effective<br />

Reproduced with permission <strong>of</strong> the copyright owner. Further reproduction prohibited without permission.

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