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Physical Principles of Electron Microscopy: An Introduction to TEM ...

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14<br />

Chapter 1<br />

Figure 1-10. JEOL transmission electron microscopes: (a) model 100B and (b) model 2010.<br />

The <strong>TEM</strong> has proved invaluable for examining the ultrastructure <strong>of</strong><br />

metals. For example, crystalline defects known as dislocations were first<br />

predicted by theorists <strong>to</strong> account for the fact that metals deform under much<br />

lower forces than calculated for perfect crystalline array <strong>of</strong> a<strong>to</strong>ms. They were<br />

first seen directly in <strong>TEM</strong> images <strong>of</strong> aluminum; one <strong>of</strong> M.J. Whelan’s<br />

original micrographs is reproduced in Fig. 1-11. Note the increase in<br />

resolution compared <strong>to</strong> the light-microscope image <strong>of</strong> Fig. 1-5; detail can<br />

now be seen within each metal crystallite. With a modern <strong>TEM</strong> (resolution �<br />

0.2 nm), it is even possible <strong>to</strong> image individual a<strong>to</strong>mic planes or columns <strong>of</strong><br />

a<strong>to</strong>ms, as we will discuss in Chapter 4.<br />

Figure 1-11. <strong>TEM</strong> diffraction-contrast image (M � 10,000) <strong>of</strong> polycrystalline aluminum.<br />

Individual crystallites (grains) show up with different brightness levels; low-angle boundaries<br />

and dislocations are visible as dark lines within each crystallite. Circular fringes (<strong>to</strong>p-right)<br />

represent local changes in specimen thickness. Courtsey <strong>of</strong> M.J. Whelan, Oxford University.

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