30.11.2012 Views

Physical Principles of Electron Microscopy: An Introduction to TEM ...

Physical Principles of Electron Microscopy: An Introduction to TEM ...

Physical Principles of Electron Microscopy: An Introduction to TEM ...

SHOW MORE
SHOW LESS

You also want an ePaper? Increase the reach of your titles

YUMPU automatically turns print PDFs into web optimized ePapers that Google loves.

70 Chapter 3<br />

where G is a large amplification fac<strong>to</strong>r (or gain), dependent on the design <strong>of</strong><br />

the oscilla<strong>to</strong>r and <strong>of</strong> the step-up transformer. Changing Vi (by altering the<br />

reference voltage V+ in Fig. 3-6) allows V0 <strong>to</strong> be intentionally changed (for<br />

example, from 100 kV <strong>to</strong> 200 kV). However, V0 could drift from its original<br />

value as a result <strong>of</strong> a slow change in G caused by drift in the oscilla<strong>to</strong>r or<br />

diode circuitry, or a change in the emission current Ie for example. Such HV<br />

instability would lead <strong>to</strong> chromatic changes in focusing and is generally<br />

unwanted. To stabilize the high voltage, a feedback resis<strong>to</strong>r R f is connected<br />

between the HV output and the oscilla<strong>to</strong>r input, as in Fig. 3-6. If G were <strong>to</strong><br />

increase slightly, V0 would change in proportion but the increase in feedback<br />

current I f would drive the input <strong>of</strong> the oscilla<strong>to</strong>r more negative, opposing the<br />

change in G. In this way, the high voltage is stabilized by negative feedback,<br />

in<br />

a similar way <strong>to</strong> stabilization <strong>of</strong> the emission current by the bias resis<strong>to</strong>r.<br />

To provide adequate insulation <strong>of</strong> the high-voltage components in the HV<br />

genera<strong>to</strong>r, they are immersed in transformer oil (used in HV power<br />

transformers) or in a gas such as sulfur hexafluoride (SF6) at a few<br />

atmospheres pressure. The high-voltage “tank” also contains the bias resis<strong>to</strong>r<br />

Rb and a transformer that supplies the heating current for a thermionic or<br />

Schottky source. Because the source is operating at high voltage, this second<br />

transformer must also have good insulation between its primary and<br />

secondary windings. Its primary is driven by a second voltage-controlled<br />

oscilla<strong>to</strong>r, whose input is controlled by a potentiometer that the <strong>TEM</strong><br />

opera<strong>to</strong>r turns <strong>to</strong> adjust the filament temperature; see Fig. 3-6.<br />

Although the electric field accelerating the electrons is primarily along<br />

the optic axis, the electric-field lines curve in the vicinity <strong>of</strong> the hole in the<br />

Wehnelt control electrode; see Fig. 3-7. This curvature arises because the<br />

electron source (just above the hole) is less negative than the electrode, by an<br />

amount equal <strong>to</strong> the Wehnelt bias. The curvature results in an electrostatic<br />

lens action that is equivalent <strong>to</strong> a weak convex lens, bringing the electrons <strong>to</strong><br />

a focus (crossover) just below the Wehnelt. Similarly, electric field lines<br />

curve above the hole in the anode plate, giving the equivalent <strong>of</strong> a concave<br />

lens and a diverging effect on the electron beam. As a result, electrons<br />

entering the lens column appear <strong>to</strong> come from a virtual source, whose<br />

diameter is typically 40 �m and divergence semi-angle �1 (relative <strong>to</strong> the<br />

optic axis) about 1 mrad (0.06 degree) in the case <strong>of</strong> a thermionic source.<br />

3.3 Condenser-Lens System<br />

The <strong>TEM</strong> may be required <strong>to</strong> produce a highly magnified (e.g, M = 10 5 )<br />

image <strong>of</strong> a specimen on a fluorescent screen, <strong>of</strong> diameter typically 15 cm. To<br />

ensure that the screen image is not <strong>to</strong>o dim, most <strong>of</strong> the electrons that pass

Hooray! Your file is uploaded and ready to be published.

Saved successfully!

Ooh no, something went wrong!